CN105994441A - Non-toxic pesticide synthetizing technology - Google Patents
Non-toxic pesticide synthetizing technology Download PDFInfo
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- CN105994441A CN105994441A CN201610441514.XA CN201610441514A CN105994441A CN 105994441 A CN105994441 A CN 105994441A CN 201610441514 A CN201610441514 A CN 201610441514A CN 105994441 A CN105994441 A CN 105994441A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
- A01N55/02—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur containing metal atoms
- A01N55/04—Tin
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Agronomy & Crop Science (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Pest Control & Pesticides (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Virology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a non-toxic pesticide synthetizing technology. The technology mainly comprises the following steps that A, lemon-scented gum, Buddleja lindleyana Fortune, castor seeds, Drosera indica L., common andrographis herb, pyrethrum and lemongrass are placed into a stirrer, and pig's bile and neochamaejasmine; B, dibutyltin dilaurate and acetyl tributyl citrate are added into the mixture obtained in the step A; C, the mixture obtained in the step B is placed into a reaction kettle, meanwhile, a surface active agent and nano-silver ion powder are added for heating stirring, and finally the non-toxic pesticide is obtained. The technology is simple, the manufacturing process is environmentally friendly and free of pollution in the overall process, and the obtained pesticide has the efficient sterilization and disinsection effect, generates no environmental pollution or residues, and has the good economic value and social value.
Description
Technical field
The present invention relates to pesticide fabricating technology field, the synthesis technique of a kind of non-poisonous pesticides.
Background technology
Along with improving constantly of people's living standard, the consumption idea of urban and rural residents has had bigger transformation, people are no longer satisfied with eating one's fill and wearing warm clothes, not only be particular about nutrition at the aspect eaten but also more focus on nontoxic, but, the currently used pesticide more than 60% of China is chemicals, and the chemical residual in agricultural byproducts, it is mainly derived from fertilizer and pesticide, more than 50% chemical pesticide contains carcinogen, due to chemical pesticide residual quantity severe overweight, agricultural subjects the erosion of harmful pesticide to varying degrees, serious destruction is suffered in ecological environment, biological life is on the hazard, simultaneously, bring harm also can to its own existence of the mankind, existing inorganic and organic insecticide, antibacterial not only pollutes environment, and destroy ecology, poison the mankind, so it is a kind of nontoxic to need development badly, pollution-free, the environment-protection pesticide having no side effect.
Summary of the invention
It is an object of the invention to provide the synthesis technique of a kind of non-poisonous pesticides, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme: the synthesis technique of a kind of non-poisonous pesticides, mainly comprises the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 1500-2000 rev/min, and mixing time 10min-20min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 55 DEG C-75 DEG C, and heat time heating time is 20min-30min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
Preferably, in step A, component includes eucalyptus citriodora 10-15 part, Radix seu Caulis Derridis Trifoliatae grass 7-12 part, castor bean 7-15 part, shichongcao 8-15 part, Herba Andrographis 10-20 part, Pyrethrum 10-20 part, Herba Cymbopogonis Citrari 15-20 part, Fel Sus domestica 10-20 part and chamaejasmine 5-12 part by weight.
Preferably, in step B, component includes dibutyl tin laurate 10-20 part and tributyl 2-acetylcitrate 10-15 part by weight.
Preferably, in step C, component includes surfactant 15-25 part and nano-silver ionic powder 2-8 part by weight.
Preferably, the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Compared with prior art, the invention has the beneficial effects as follows: present invention process is simple, manufacturing process is omnidistance environment friendly and pollution-free, use eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari as raw material, the pesticide prepared has efficient disinfection and deinsectization effect, environmentally safe, noresidue, have good economic worth and social value；The present invention is additionally additionally added a certain amount of nano-silver ionic powder, it is possible to rotten after preventing pesticide oxidation.
Detailed description of the invention
Below the technical scheme in the embodiment of the present invention is clearly and completely described; obviously; described embodiment is only a part of embodiment of the present invention; rather than whole embodiments; based on the embodiment in the present invention; the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly falls into the scope of protection of the invention.
Embodiment one:
The present invention provides a kind of technical scheme: the synthesis technique of a kind of non-poisonous pesticides, mainly comprises the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 1500 revs/min, and mixing time 10min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 55 DEG C, and heat time heating time is 20min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
In the present embodiment, in step A, component includes eucalyptus citriodora 10 parts, Radix seu Caulis Derridis Trifoliatae grass 7 parts, castor bean 7 parts, shichongcao 8 parts, Herba Andrographis 10 parts, Pyrethrum 10 parts, Herba Cymbopogonis Citrari 15 parts, Fel Sus domestica 10 parts and chamaejasmine 5 parts by weight.
In the present embodiment, in step B, component includes dibutyl tin laurate 10 parts and tributyl 2-acetylcitrate 10 parts by weight.
In the present embodiment, in step C, component includes 15 parts of surfactant and 2 parts of nano-silver ionic powder by weight.
In the present embodiment, the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Embodiment two:
The present invention provides a kind of technical scheme: the synthesis technique of a kind of non-poisonous pesticides, mainly comprises the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 2000 revs/min, and mixing time 20min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 75 DEG C, and heat time heating time is 30min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
In the present embodiment, in step A, component includes eucalyptus citriodora 15 parts, Radix seu Caulis Derridis Trifoliatae grass 12 parts, castor bean 15 parts, shichongcao 15 parts, Herba Andrographis 20 parts, Pyrethrum 20 parts, Herba Cymbopogonis Citrari 20 parts, Fel Sus domestica 20 parts and chamaejasmine 12 parts by weight.
In the present embodiment, in step B, component includes dibutyl tin laurate 20 parts and tributyl 2-acetylcitrate 15 parts by weight.
In the present embodiment, in step C, component includes 25 parts of surfactant and 8 parts of nano-silver ionic powder by weight.
In the present embodiment, the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Embodiment three:
The present invention provides a kind of technical scheme: the synthesis technique of a kind of non-poisonous pesticides, mainly comprises the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 1900 revs/min, and mixing time 18min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 70 DEG C, and heat time heating time is 28min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
In the present embodiment, in step A, component includes eucalyptus citriodora 14 parts, Radix seu Caulis Derridis Trifoliatae grass 11 parts, castor bean 14 parts, shichongcao 14 parts, Herba Andrographis 18 parts, Pyrethrum 18 parts, Herba Cymbopogonis Citrari 19 parts, Fel Sus domestica 18 parts and chamaejasmine 11 parts by weight.
In the present embodiment, in step B, component includes dibutyl tin laurate 18 parts and tributyl 2-acetylcitrate 14 parts by weight.
In the present embodiment, in step C, component includes 23 parts of surfactant and 7 parts of nano-silver ionic powder by weight.
In the present embodiment, the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Embodiment four:
The present invention provides a kind of technical scheme: the synthesis technique of a kind of non-poisonous pesticides, mainly comprises the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 1800 revs/min, and mixing time 15min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 65 DEG C, and heat time heating time is 25min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
In the present embodiment, in step A, component includes eucalyptus citriodora 12 parts, Radix seu Caulis Derridis Trifoliatae grass 10 parts, castor bean 11 parts, shichongcao 12 parts, Herba Andrographis 15 parts, Pyrethrum 15 parts, Herba Cymbopogonis Citrari 17 parts, Fel Sus domestica 15 parts and chamaejasmine 8 parts by weight.
In the present embodiment, in step B, component includes dibutyl tin laurate 15 parts and tributyl 2-acetylcitrate 12 parts by weight.
In the present embodiment, in step C, component includes 20 parts of surfactant and 5 parts of nano-silver ionic powder by weight.
In the present embodiment, the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Using method: join 8 kg of water mixture by every mu of 100mg medicinal liquid and crops are sprayed, after half an hour, most of insect of crop surface is dead, after two hours, the insect almost all of crop surface is dead, detection crop surface pesticide residues two days later, testing result pesticide is wholly absent, and agricultural leaf does not has any damage.
Present invention process is simple, manufacturing process is omnidistance environment friendly and pollution-free, use eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari as raw material, the pesticide prepared has efficient disinfection and deinsectization effect, environmentally safe, noresidue, have good economic worth and social value；The present invention is additionally additionally added a certain amount of nano-silver ionic powder, it is possible to rotten after preventing pesticide oxidation.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, being appreciated that and these embodiments can carry out multiple change without departing from the principles and spirit of the present invention, revise, replace and modification, the scope of the present invention be defined by the appended.
Claims (5)
1. the synthesis technique of a non-poisonous pesticides, it is characterised in that: mainly comprise the steps that
A, eucalyptus citriodora, Radix seu Caulis Derridis Trifoliatae grass, castor bean, shichongcao, Herba Andrographis, Pyrethrum, Herba Cymbopogonis Citrari being put in blender and add Fel Sus domestica and chamaejasmine, blender rotating speed is 1500-2000 rev/min, and mixing time 10min-20min obtains A mixture；
B, in the A mixture that step A obtains, add dibutyl tin laurate and tributyl 2-acetylcitrate, adition process is stirred continuously, filters off impurity by sieves afterwards, obtain B mixture；
C, B mixture step B obtained are put in reactor, being simultaneously introduced surfactant and nano-silver ionic powder carries out heated and stirred, reactor heating-up temperature is 55 DEG C-75 DEG C, and heat time heating time is 20min-30min, stand after constant temperature 20min afterwards and be cooled to room temperature, obtain non-poisonous pesticides.
A kind of non-poisonous pesticides synthesis technique the most according to claim 1, it is characterised in that: in step A, component includes eucalyptus citriodora 10-15 part, Radix seu Caulis Derridis Trifoliatae grass 7-12 part, castor bean 7-15 part, shichongcao 8-15 part, Herba Andrographis 10-20 part, Pyrethrum 10-20 part, Herba Cymbopogonis Citrari 15-20 part, Fel Sus domestica 10-20 part and chamaejasmine 5-12 part by weight.
A kind of non-poisonous pesticides synthesis technique the most according to claim 1, it is characterised in that: in step B, component includes dibutyl tin laurate 10-20 part and tributyl 2-acetylcitrate 10-15 part by weight.
A kind of non-poisonous pesticides synthesis technique the most according to claim 1, it is characterised in that: in step C, component includes surfactant 15-25 part and nano-silver ionic powder 2-8 part by weight.
A kind of non-poisonous pesticides synthesis technique the most according to claim 1, it is characterised in that: the surfactant in step C includes tween 80 and sodium dodecyl sulfate mixture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610441514.XA CN105994441A (en) | 2016-06-20 | 2016-06-20 | Non-toxic pesticide synthetizing technology |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610441514.XA CN105994441A (en) | 2016-06-20 | 2016-06-20 | Non-toxic pesticide synthetizing technology |
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| CN201610441514.XA Pending CN105994441A (en) | 2016-06-20 | 2016-06-20 | Non-toxic pesticide synthetizing technology |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107410378A (en) * | 2017-06-01 | 2017-12-01 | 冯新平 | A kind of non-poisonous pesticides and its preparation technology |
| CN108353946A (en) * | 2018-04-28 | 2018-08-03 | 陈建峰 | A kind of Agrimycin and preparation method thereof |
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| CN1106213A (en) * | 1994-11-28 | 1995-08-09 | 王安邦 | Chinese medicinal insecticide |
| CN1362021A (en) * | 2002-01-25 | 2002-08-07 | 杨凌大地化工有限公司 | Chinese stellera extract pesticide |
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| CN104920507A (en) * | 2015-05-29 | 2015-09-23 | 蚌埠市乔峰农业蔬菜专业合作社 | Agent capable of effectively controlling cabbage caterpillars |
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| CN1049441A (en) * | 1989-08-13 | 1991-02-27 | 潘志荣 | Rotenone-pyrethroids insecticide |
| CN1106213A (en) * | 1994-11-28 | 1995-08-09 | 王安邦 | Chinese medicinal insecticide |
| CN1362021A (en) * | 2002-01-25 | 2002-08-07 | 杨凌大地化工有限公司 | Chinese stellera extract pesticide |
| EP1510129A2 (en) * | 2002-04-17 | 2005-03-02 | Agribiotec s.r.l. | Use of vegetable oil as an adjuvant for substances having a fungicide, bactericide, insecticide and herbicide activity |
| CN104920507A (en) * | 2015-05-29 | 2015-09-23 | 蚌埠市乔峰农业蔬菜专业合作社 | Agent capable of effectively controlling cabbage caterpillars |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107410378A (en) * | 2017-06-01 | 2017-12-01 | 冯新平 | A kind of non-poisonous pesticides and its preparation technology |
| CN108353946A (en) * | 2018-04-28 | 2018-08-03 | 陈建峰 | A kind of Agrimycin and preparation method thereof |
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Application publication date: 20161012 |