CN108485501A - 一种石墨烯基水性涂料及其制备方法 - Google Patents
一种石墨烯基水性涂料及其制备方法 Download PDFInfo
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- CN108485501A CN108485501A CN201810412263.1A CN201810412263A CN108485501A CN 108485501 A CN108485501 A CN 108485501A CN 201810412263 A CN201810412263 A CN 201810412263A CN 108485501 A CN108485501 A CN 108485501A
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 67
- 239000003973 paint Substances 0.000 title claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims abstract description 56
- 239000005058 Isophorone diisocyanate Substances 0.000 claims abstract description 53
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 48
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229920000515 polycarbonate Polymers 0.000 claims abstract description 24
- 239000004417 polycarbonate Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 14
- 230000002776 aggregation Effects 0.000 claims abstract description 9
- 238000004220 aggregation Methods 0.000 claims abstract description 8
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 8
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 48
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 32
- DQFBYFPFKXHELB-UHFFFAOYSA-N Chalcone Natural products C=1C=CC=CC=1C(=O)C=CC1=CC=CC=C1 DQFBYFPFKXHELB-UHFFFAOYSA-N 0.000 claims description 26
- 235000005513 chalcones Nutrition 0.000 claims description 26
- 229960002725 isoflurane Drugs 0.000 claims description 26
- 239000003795 chemical substances by application Substances 0.000 claims description 19
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical group CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 18
- 238000010792 warming Methods 0.000 claims description 8
- 238000004945 emulsification Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 239000004575 stone Substances 0.000 claims description 3
- 238000011065 in-situ storage Methods 0.000 claims description 2
- 238000007711 solidification Methods 0.000 claims description 2
- 230000008023 solidification Effects 0.000 claims description 2
- 150000001336 alkenes Chemical class 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims 1
- 239000011248 coating agent Substances 0.000 abstract description 17
- 238000000576 coating method Methods 0.000 abstract description 17
- 239000004814 polyurethane Substances 0.000 abstract description 10
- 229920002635 polyurethane Polymers 0.000 abstract description 10
- 229920000642 polymer Polymers 0.000 abstract description 8
- 239000000853 adhesive Substances 0.000 abstract description 5
- 230000001070 adhesive effect Effects 0.000 abstract description 5
- 239000002131 composite material Substances 0.000 abstract description 5
- 229920013657 polymer matrix composite Polymers 0.000 abstract description 4
- 239000011160 polymer matrix composite Substances 0.000 abstract description 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract description 3
- 230000020477 pH reduction Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 125000004356 hydroxy functional group Chemical group O* 0.000 abstract description 2
- 239000006185 dispersion Substances 0.000 description 10
- HJOVHMDZYOCNQW-UHFFFAOYSA-N isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000011527 polyurethane coating Substances 0.000 description 6
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 3
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 description 3
- 239000000945 filler Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000003063 flame retardant Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 239000004970 Chain extender Substances 0.000 description 2
- 229920001730 Moisture cure polyurethane Polymers 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011256 inorganic filler Substances 0.000 description 2
- 229910003475 inorganic filler Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 239000005056 polyisocyanate Substances 0.000 description 2
- 229920001228 polyisocyanate Polymers 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 150000005846 sugar alcohols Polymers 0.000 description 2
- 238000002604 ultrasonography Methods 0.000 description 2
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 1
- 239000004425 Makrolon Substances 0.000 description 1
- 239000008896 Opium Substances 0.000 description 1
- 238000012644 addition polymerization Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000009435 amidation Effects 0.000 description 1
- 238000007112 amidation reaction Methods 0.000 description 1
- 238000005576 amination reaction Methods 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000002041 carbon nanotube Substances 0.000 description 1
- 229910021393 carbon nanotube Inorganic materials 0.000 description 1
- -1 carbonate diol Chemical class 0.000 description 1
- 125000005587 carbonate group Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910003472 fullerene Inorganic materials 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229960001027 opium Drugs 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000003252 repetitive effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
- C08G18/44—Polycarbonates
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/24—Electrically-conducting paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
- C08K3/042—Graphene or derivatives, e.g. graphene oxides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paints Or Removers (AREA)
Abstract
Description
S1 | S2 | S3 | S4 | D1 | D2 | |
附着力/级 | 0 | 0 | 0 | 1 | 1 | 1 |
铅笔硬度/H | 4H | 5H | 5H | 5H | 3H | 3H |
柔韧性/mm | <1 | <1 | <1 | <1 | <1 | <1 |
冲击力/cm | >50 | >50 | >50 | >50 | >50 | >50 |
盐雾实验/h | 480 | 492 | 500 | 502 | 282 | 312 |
表面电阻率/Ω | 1010 | 109 | 106 | 108 | 109 | 107 |
拉伸强度/MPa | 60 | 64 | 72 | 70 | 40 | 48 |
氧指数 | 26.8 | 27.3 | 27.7 | 28.5 | 26.6 | 27.8 |
达到最大烟密度时间/S | 170 | 191 | 210 | 218 | 161 | 211 |
Claims (10)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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CN2018102787043 | 2018-03-30 | ||
CN201810278704 | 2018-03-30 |
Publications (2)
Publication Number | Publication Date |
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CN108485501A true CN108485501A (zh) | 2018-09-04 |
CN108485501B CN108485501B (zh) | 2020-02-18 |
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Application Number | Title | Priority Date | Filing Date |
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CN201810412263.1A Active CN108485501B (zh) | 2018-03-30 | 2018-05-03 | 一种石墨烯基水性涂料及其制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN108485501B (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109575225A (zh) * | 2018-12-21 | 2019-04-05 | 广东好邦石墨烯新材料科技有限公司 | 一种氧化石墨烯改性固化剂、聚氨酯涂料及其制备方法和应用 |
CN109575782A (zh) * | 2018-11-15 | 2019-04-05 | 青岛科技大学 | 氧化石墨烯改性聚氨酯电泳树脂、聚氨酯电泳漆及其制备方法 |
CN110643016A (zh) * | 2019-10-16 | 2020-01-03 | 安徽大学 | 碳纳米管负载纳米银线改性聚氨酯抗静电乳液的制备方法 |
CN110804384A (zh) * | 2019-11-21 | 2020-02-18 | 安徽新大陆特种涂料有限责任公司 | 一种防腐蚀性能较好的水性聚氨酯涂料制备方法 |
CN115746689A (zh) * | 2022-11-11 | 2023-03-07 | 吉林大学 | 一种仿生自修复、防污、防腐多功能涂层及其制备方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103805046A (zh) * | 2014-01-26 | 2014-05-21 | 陕西科技大学 | 原位法制备含石墨烯的水性聚氨酯复合导电涂料及其方法 |
CN103805049A (zh) * | 2013-08-05 | 2014-05-21 | 江苏大学 | 基于氧化石墨烯的紫外光固化水性聚氨酯抗电磁屏蔽涂料的制备方法 |
CN104277198A (zh) * | 2014-10-25 | 2015-01-14 | 朱蕾 | 一种石墨烯基导电阻燃型水性聚氨酯涂料和胶黏剂的制备方法 |
CN104804169A (zh) * | 2015-05-22 | 2015-07-29 | 烟台大学 | 一种石墨烯改性聚氨酯导电性涂料的制备方法 |
WO2016199167A2 (en) * | 2015-06-10 | 2016-12-15 | Council Of Scientific And Industrial Research | Microcapsules modified with nanomaterial for controlled release of active agent and process for preparation thereof |
-
2018
- 2018-05-03 CN CN201810412263.1A patent/CN108485501B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103805049A (zh) * | 2013-08-05 | 2014-05-21 | 江苏大学 | 基于氧化石墨烯的紫外光固化水性聚氨酯抗电磁屏蔽涂料的制备方法 |
CN103805046A (zh) * | 2014-01-26 | 2014-05-21 | 陕西科技大学 | 原位法制备含石墨烯的水性聚氨酯复合导电涂料及其方法 |
CN104277198A (zh) * | 2014-10-25 | 2015-01-14 | 朱蕾 | 一种石墨烯基导电阻燃型水性聚氨酯涂料和胶黏剂的制备方法 |
CN104804169A (zh) * | 2015-05-22 | 2015-07-29 | 烟台大学 | 一种石墨烯改性聚氨酯导电性涂料的制备方法 |
WO2016199167A2 (en) * | 2015-06-10 | 2016-12-15 | Council Of Scientific And Industrial Research | Microcapsules modified with nanomaterial for controlled release of active agent and process for preparation thereof |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109575782A (zh) * | 2018-11-15 | 2019-04-05 | 青岛科技大学 | 氧化石墨烯改性聚氨酯电泳树脂、聚氨酯电泳漆及其制备方法 |
CN109575782B (zh) * | 2018-11-15 | 2020-11-27 | 青岛科技大学 | 氧化石墨烯改性聚氨酯电泳树脂、聚氨酯电泳漆及其制备方法 |
CN109575225A (zh) * | 2018-12-21 | 2019-04-05 | 广东好邦石墨烯新材料科技有限公司 | 一种氧化石墨烯改性固化剂、聚氨酯涂料及其制备方法和应用 |
CN109575225B (zh) * | 2018-12-21 | 2021-11-16 | 广东好邦石墨烯新材料科技有限公司 | 一种氧化石墨烯改性固化剂、聚氨酯涂料及其制备方法和应用 |
CN110643016A (zh) * | 2019-10-16 | 2020-01-03 | 安徽大学 | 碳纳米管负载纳米银线改性聚氨酯抗静电乳液的制备方法 |
CN110804384A (zh) * | 2019-11-21 | 2020-02-18 | 安徽新大陆特种涂料有限责任公司 | 一种防腐蚀性能较好的水性聚氨酯涂料制备方法 |
CN115746689A (zh) * | 2022-11-11 | 2023-03-07 | 吉林大学 | 一种仿生自修复、防污、防腐多功能涂层及其制备方法 |
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