CN108354849A - A kind of oral care composition and preparation method thereof that cooperation electric toothbrush uses - Google Patents
A kind of oral care composition and preparation method thereof that cooperation electric toothbrush uses Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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Abstract
The invention belongs to the cosmetics or similar dressing preparation technical field characterized by component, and in particular to a kind of oral care composition that cooperation electric toothbrush uses.The oral care composition includes rubbing agent and polishing agent.There is the oral care composition good cleaning force, cooperation electric toothbrush to use, and can significantly reduce the abrasion to tooth, reduce the stimulation degree to oral cavity, effectively improve the glossiness and whiteness of tooth.
Description
Technical field
The invention belongs to the cosmetics or similar dressing preparation technical field characterized by component, and in particular to one
The oral care composition and preparation method thereof that kind cooperation electric toothbrush uses.
Background technology
With popularizing for oral knowledge, more and more people recognize the importance of oral care.Consumer is to whitening tooth
Tooth has strong demand, and it is the basic function brushed teeth to clean dirt and tooth stain.However, often having tea, the tooth table of smoker
One layer of dun tea stain and cigarette stain are often adsorbed in face securely, and the main reason for forming these exogenous spots is tooth table
The plaque in face and a variety of coloring matters inside tea stain and cigarette stain, by electrostatic force, Van der Waals force and it is short-range mutually
Effect is difficult to the exogenous spot removed.Traditional toothbrush is difficult to thoroughly remove plaque, along with method for brushing teeth is not proper, makes brush
The cleaning action of tooth is had a greatly reduced quality.
Electric toothbrush high speed rotation and the high-frequency vibration generated, can resolve into subtle foam moment by toothpaste, deeply clear
Clean one's teeth seam, and the trembling of bristle can promote the blood circulation in oral cavity, has preferable nursing efficacy to gingiva tissue.Numerous studies table
Bright, compared with manual toothbrush, electric toothbrush can improve 38% to the cleaning force of plaque, can effectively reduce and drink tea, drink coffee
Tooth stain caused by coffee and bad oral conditions restores the original color and luster of tooth.
With advances in technology and improvement of living standard, more and more people select to replace traditional hand with electric toothbrush
Dynamic toothbrush.Numerous studies show that electric toothbrush is safer than manual toothbrush, are safe from harm to hard and soft tissue, manual toothbrush
It is easier to cause tooth wear.Certain electric toothbrushes on the market carry strength sensor now, and prompt is had when firmly excessive,
It is excessive largely to avoid strength when brushing teeth.In addition, the rise of APP also promotes the appearance of " intelligently brushing teeth ", pass through indigo plant
Tooth is connect with the APP that brushes teeth, and electric toothbrush can show the time brushed teeth and path by mobile phone, and comment the effect after brushing teeth
Valence, to guide consumer preferably to brush teeth.
For most of oral care implement manufacturing enterprise, to develop with high cleaning power, to tooth loss compared with
Small oral care implement is very difficult, is often attended to one thing and lose sight of another.The reason is that carrying with electric toothbrush cleaning force
Height can cause the abrasion of tooth.Therefore, oral care implement of the exploitation with high cleaning power has to coordinate electric toothbrush to use
Effect reduces tooth wear, and it is necessary to reduce and cause damage to tooth and gum.
Invention content
In view of this, the purpose of the present invention is to provide a kind of oral care composition, the composition can be with electric tooth
Brush is used cooperatively, and effectively reduces tooth wear, reduces the damage to tooth and gum.
To achieve the above object, the technical scheme is that：
Oral care composition, including rubbing agent and polishing agent.
Further, the rubbing agent is the 1-4 kinds in calcium carbonate, silica, aluminium hydroxide and calcium pyrophosphate.
Further, the rubbing agent is by silica, the dentine relative attrition value of dentine relative attrition value ＜ 50
The silica and dentine relative attrition value of 180-200 is that the silica composition of 130-170 forms.
Further, the rubbing agent is by silica, the dentine relative attrition value of dentine relative attrition value ＜ 50
The silica and dentine relative attrition value of 180-200 is the silica of 130-170 according to 1:5-20:The mass ratio of 5-20
It is composed.
The dentine relative attrition value passes through according to ISO11609 Appendix B《Denfifrice pair is measured by surface profiler
The relative attrition value of enamel and dentine》The method is tested.
Further, the polishing agent is the 1-6 in Brazil wax, candelila wax, beeswax, shellac, microwax and paraffin
Kind.
Further, further include foaming agent.
Further, the foaming agent is lauryl sodium sulfate, cocounut oil acyl alanine triacetic acid ammonium, cocamidopropyl propyl amide sweet tea
Dish alkali, cocounut oil acyl glycine potassium, sodium cocoyl glycinate, sodium lauroyl sarcosine, laureth sodium sulfovinate and cocounut oil acyl
1-8 kinds in glutamic acid triethanolamine.
Further, in terms of mass parts, proportion relation is：0.1-5 parts of 22-82 parts of rubbing agent and polishing agent.
Further, the oral care composition is toothpaste.
Further, further include moisturizer and/or thickener and/or sweetener and/or essence and/or water.
Further, the moisturizer is the 1-4 kinds in sorbierite, glycerine, propylene glycol and polyethylene glycol.
Further, the thickener is sodium carboxymethylcellulose, hydroxyethyl cellulose, carbomer, carragheen, Guar
1-7 kinds in glue, xanthans and silica dioxide gel.
Further, the sweetener is saccharin sodium, Aspartame, stevioside, Sucralose, acesulfame potassium, sucrose, xylitol
With the 1-8 kinds in acetic acid sulfamic acid potassium.
Further, in terms of mass parts, proportion relation is：22-47 parts of rubbing agent, 0.1-0.6 parts of polishing agent, foaming agent do not surpass
Cross 3.0 parts, moisturizer be no more than 60 parts, thickener be no more than 2 parts, sweetener be no more than 0.5 part, essence be no more than 1.5 parts, it is remaining
Amount is water, 100 parts of total amount.
Further, in terms of mass parts, 22-47 parts of rubbing agent, 1.2-3.0 parts of foaming agent, 0.1-0.6 parts of polishing agent, moisturizing
30-60 parts of agent, 0.2-2 parts of thickener, 0.2-0.5 parts of sweetener, 0.5-1.5 parts of essence, surplus are water, and total amount is 100 parts.
Further, proportion relation is：26 parts of rubbing agent, 2.2 parts of foaming agent, 0.5 part of polishing agent, 55 parts of moisturizer, thickening
0.7 part of agent, 0.3 part of sweetener, 1 part of essence, surplus are water, and total amount is 100 parts.
Further, the oral care composition is tooth powder.
Further, further include sodium bicarbonate and/or sweetener and/or Herba Menthae powder essence and/or Natural menthol.
Further, in terms of mass parts, proportion relation is：70-82 parts of rubbing agent, 1-5 parts of polishing agent, foaming agent are no more than 12
Part, sodium bicarbonate are no more than no more than 0.8 part, Herba Menthae powder essence no more than 0.7 part, Natural menthol no more than 10 parts, sweetener
0.7 part.
Further, in terms of mass parts, proportion relation is：70-82 parts of rubbing agent, 1-5 parts of polishing agent, 8-12 parts of foaming agent,
0.2-0.8 parts of sweetener, 0.3-0.7 parts of Herba Menthae powder essence, 0.3-0.7 parts of Natural menthol, 6-10 parts of sodium bicarbonate.
Further, in terms of mass parts, proportion relation is：80 parts of rubbing agent, 10 parts of foaming agent, 4 parts of polishing agent, sweetener
0.5 part, Herba Menthae powder essence 0.4 part, 0.5 part of Natural menthol, 8 parts of sodium bicarbonate.
The present invention also aims to protect the preparation method of the oral care composition, include the following steps：
A. thickener is scattered in anhydrous moisturizer to no caking；
B. sweetener is dissolved in water, remaining moisturizer and foaming agent are added to together in the mixture of step A, and mixing is equal
It is even；
C. polishing agent and rubbing agent are stirred evenly；
D. mixture obtained by step C is added in mixture obtained by step B, is stirring evenly and then adding into essence, stirs evenly,
Vacuum outgas forms lotion.
The above glycerine, polyethylene glycol and with propylene glycol be anhydrous moisturizer.
In addition, inventor also found, if not operating in this way, it may appear that caking phenomenon, liquid charging stock dispersion is uneven,
The property sent out is bad thoroughly for lotion fragrance.
The beneficial effects of the present invention are：
The oral care composition of the present invention has good cleaning force.
The oral care composition cooperation electric toothbrush of the present invention uses, and can significantly reduce the abrasion to tooth.
Toothpaste has good stability made from the oral care composition of the present invention.
The oral care composition of the present invention can reduce the stimulation degree to oral cavity, and sudden strain of a muscle bubble property is good, gas release is big.
The oral care composition cooperation electric toothbrush of the present invention is using the glossiness that can effectively improve tooth and in vain
Degree.
Specific implementation mode
Illustrated embodiment is to preferably be illustrated to present disclosure, but is not that present disclosure only limits
In illustrated embodiment.So those skilled in the art carry out nonessential change according to foregoing invention content to embodiment
Into and adjustment, still fall within protection scope of the present invention.
Electric toothbrush in following embodiment and comparative example isCrystalline substance bores series of acoustic electric toothbrush；Ordinary toothbrush is
Luclean carbon filament times cleaning toothbrush, RDA is according to ISO11609 Appendix B《Denfifrice is measured to enamel and tooth by surface profiler
The relative attrition value of essence》The method is tested.
Embodiment 1
Toothpaste, consisting of：The silica 1 5.5g, RDA that the silica 8g, RDA that RDA is 200 are 140 are 35
Silica 1 .5g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, babassu
Wax 0.2g, titanium dioxide 0.2g, lauryl sodium sulfate 2g, cocounut oil acyl glutamic acid triethanolamine 0.1g, saccharin sodium 0.3g, essence
1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. by Brazil wax, lauryl sodium sulfate, cocounut oil acyl glutamic acid triethanolamine, titanium dioxide and silica
It is uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Embodiment 2
Toothpaste, consisting of：The silica 1 1g, RDA that the silica 1 3g, RDA that RDA is 200 are 140 are the two of 35
Silica 2.5g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, Brazil wax
0.5g, titanium dioxide 0.2g, lauryl sodium sulfate 1.7g, Cocoamidopropyl betaine 0.3g, sodium lauroyl sarcosine
0.1g, saccharin sodium 0.3g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. by Brazil wax, lauryl sodium sulfate, Cocoamidopropyl betaine, sodium lauroyl sarcosine, dioxy
Change titanium and silica is uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Embodiment 3
Toothpaste, consisting of：RDA silica, the 10g for 200, RDA silica, the 13g for 140, RDA are 35
Silica 2g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, Brazil wax
0.6g, titanium dioxide 0.2g, lauryl sodium sulfate 1.5g, Cocoamidopropyl betaine 0.6g, saccharin sodium 0.3g, essence
1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. Brazil wax, lauryl sodium sulfate, Cocoamidopropyl betaine, titanium dioxide and silica are mixed
It closes uniform；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 36min of sky forms lotion to get the toothpaste.
Embodiment 4
Toothpaste, consisting of：Silica (thickener) 3g, sorbierite 25g, glycerine 3g, calcium carbonate 40g that RDA is 35,
Sodium carboxymethylcellulose 0.8g, guar gum 0.2g, Brazil wax 0.1g, candelila wax 0.3g, titanium dioxide 0.2g, dodecane
Base sodium sulphate 1.1g, cocounut oil acyl glutamic acid triethanolamine 0.4g, sodium lauroyl sarcosine 0.6g, saccharin sodium 0.15g, Sucralose
0.2g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and guar gum are scattered in glycerine, are dispersed with stirring uniformly to no caking；
B. saccharin sodium and Sucralose is soluble in water, it is then added to together with sorbierite in mixture obtained by step A,
Stir 10min；
C. by Brazil wax, candelila wax, lauryl sodium sulfate, cocounut oil acyl glutamic acid triethanolamine, lauroyl flesh
Propylhomoserin sodium, titanium dioxide, silica and calcium carbonate are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 38min of sky forms lotion to get the toothpaste.
Embodiment 5
Toothpaste, consisting of：Sorbierite 20g, glycerine 10g, calcium pyrophosphate 39g, sodium carboxymethylcellulose 0.6g, xanthans
0.1g, candelila wax 0.4g, titanium dioxide 0.2g, lauryl sodium sulfate 0.6g, Cocoamidopropyl betaine 0.5g, bay
Acylsarcosine sodium 1g, Sucralose 0.3g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and xanthans are scattered in glycerine, are dispersed with stirring uniformly to no caking；
B. Sucralose is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirring
10min；
C. by candelila wax, lauryl sodium sulfate, Cocoamidopropyl betaine, sodium lauroyl sarcosine, titanium dioxide
Titanium and calcium pyrophosphate are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 36min of sky forms lotion to get the toothpaste.
Embodiment 6
Toothpaste, consisting of：Sorbierite 20g, aluminium hydroxide 45g, polyethylene glycol-400 10g, carragheen 0.5g, xanthan
Glue 0.2g, candelila wax 0.2g, microwax 0.2g, titanium dioxide 0.2g, lauryl sodium sulfate 0.4g, sodium lauroyl sarcosine
1.7g, Sucralose 0.2g, xylitol 0.2g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. carragheen and xanthans are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. Sucralose and xylitol is soluble in water, it is then added to together with sorbierite in mixture obtained by step A,
Stir 10min；
C. by candelila wax, microwax, lauryl sodium sulfate, sodium lauroyl sarcosine, titanium dioxide and aluminium hydroxide
It is uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 39min of sky forms lotion to get the toothpaste.
Comparative example 1
Toothpaste, consisting of：The silica 1 5g, RDA that the silica 3g, RDA that RDA is 200 are 140 are the two of 35
Silica 3g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, Brazil wax
0.5g, titanium dioxide 0.2g, lauryl sodium sulfate 1.8g, Cocoamidopropyl betaine 0.3g, saccharin sodium 0.3g, essence
1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. Brazil wax, lauryl sodium sulfate, Cocoamidopropyl betaine, titanium dioxide and silica are mixed
It closes uniform；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Comparative example 2
Toothpaste, consisting of：The silica 1 3g, RDA that the silica 1 0g, RDA that RDA is 200 are 140 are the two of 35
Silica 2g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, titanium dioxide
0.2g, lauryl sodium sulfate 1.8g, Cocoamidopropyl betaine 0.3g, saccharin sodium 0.3g, essence 1g, water surplus, altogether
100g。
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. lauryl sodium sulfate, Cocoamidopropyl betaine, titanium dioxide and silica are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 36min of sky forms lotion to get the toothpaste.
Comparative example 3
Toothpaste, consisting of：The silica 1 3g, RDA that the silica 1 0g, RDA that RDA is 200 are 140 are the two of 35
Silica 2g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, candelila wax
0.5g, titanium dioxide 0.2g, lauryl sodium sulfate 2.1g, Cocoamidopropyl betaine 0.01g, saccharin sodium 0.3g, essence
1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. candelila wax, lauryl sodium sulfate, Cocoamidopropyl betaine, titanium dioxide and silica are mixed
Uniformly；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Comparative example 4
Toothpaste, consisting of：The silica 1 3g, RDA that the silica 1 0g, RDA that RDA is 200 are 140 are the two of 35
Silica 2g, sorbierite 50g, polyethylene glycol-400 4g, sodium carboxymethylcellulose 0.3g, carragheen 0.3g, microwax 0.5g,
Titanium dioxide 0.2g, lauryl sodium sulfate 2.1g, saccharin sodium 0.3g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and carragheen are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. saccharin sodium is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. microwax, lauryl sodium sulfate, titanium dioxide and silica are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Comparative example 5
Toothpaste, consisting of：Silica 3g, the calcium carbonate 40g that RDA is 35, sorbierite 25g, glycerine 3g, carboxymethyl are fine
Dimension plain sodium 0.8g, guar gum 0.2g, Brazil wax 0.1g, candelila wax 0.3g, titanium dioxide 0.2g, lauryl sodium sulfate
2.1g, saccharin sodium 0.15g, Sucralose 0.2g, essence 1g, water surplus, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and guar gum are scattered in glycerine, are dispersed with stirring uniformly to no caking；
B. saccharin sodium and Sucralose is soluble in water, it is then added to together with sorbierite in mixture obtained by step A,
Stir 10min；
C. Brazil wax, candelila wax, lauryl sodium sulfate, titanium dioxide, silica and calcium carbonate are mixed
Uniformly；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 37min of sky forms lotion to get the toothpaste.
Comparative example 6
Toothpaste, consisting of：Calcium carbonate 2g, calcium pyrophosphate 37g, sorbierite 20g, glycerine 10g, sodium carboxymethylcellulose
0.6g, xanthans 0.1g, titanium dioxide 0.2g, lauryl sodium sulfate 2.1g, Sucralose 0.3g, essence 1g, water surplus, altogether
100g。
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and xanthans are scattered in glycerine, are dispersed with stirring uniformly to no caking；
B. Sucralose is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirring
10min；
C. lauryl sodium sulfate, titanium dioxide, calcium carbonate and calcium pyrophosphate are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 38min of sky forms lotion to get the toothpaste.
Comparative example 7
Toothpaste, consisting of：Aluminium hydroxide 45g, sorbierite 20g, polyethylene glycol-400 10g, carragheen 0.5g, xanthan
Glue 0.2g, titanium dioxide 0.2g, lauryl sodium sulfate 2.1g, Sucralose 0.2g, xylitol 0.2g, essence 1g, water surplus,
Total 100g.
The preparation method of the toothpaste is：
A. carragheen and xanthans are scattered in polyethylene glycol-400, are dispersed with stirring uniformly to no caking；
B. Sucralose and xylitol is soluble in water, it is then added to together with sorbierite in mixture obtained by step A,
Stir 10min；
C. lauryl sodium sulfate, titanium dioxide and aluminium hydroxide are uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 38min of sky forms lotion to get the toothpaste.
Comparative example 8
Toothpaste, consisting of：The silica 24g, RDA that RDA is 140 are 35 silica 2g, sorbierite 53g, are gathered
Ethylene glycol -400 2g, glycerine 2g, sodium carboxymethylcellulose 0.2g, xanthans 0.3g, Brazil wax 0.2g, microwax 0.2g,
Titanium dioxide 0.2g, lauryl sodium sulfate 1.0g, Cocoamidopropyl betaine 1.0g, xylitol 0.3g, essence 1g, more than water
Amount, total 100g.
The preparation method of the toothpaste is：
A. sodium carboxymethylcellulose and xanthans are scattered in polyethylene glycol-400 and glycerine, are dispersed with stirring uniformly to nothing
Caking；
B. xylitol is soluble in water, it is then added to together with sorbierite in mixture obtained by step A, stirs 10min；
C. by Brazil wax, microwax, lauryl sodium sulfate, Cocoamidopropyl betaine, titanium dioxide and two
Silica is uniformly mixed；
D. step C products therefroms are added in step B products therefroms, are stirred evenly, add essence, stir 10min, very
The lower high-speed stirred 40min of sky forms lotion to get the toothpaste.
Toothpaste stability experiment
Toothpaste made from embodiment 1-6 and comparative example 1-8 is placed in the refrigerator that temperature is -8 DEG C, takes out and restore after 8h
To room temperature, tests it and squeeze cream pressure, whether appearance is normal, and the results are shown in Table 1；
The test method for squeezing cream pressure is：It materialses toothpaste, first squeezing out lotion about 20mm with hand abandons it, and toothpaste nozzle is revolved
In the standard cap for entering crowded cream piezometry instrument, then standard cap is tightened in the air storage of crowded cream piezometry instrument together with toothpaste
It in cylinder, is allowed to air tight, air is pressed by compression pump slowly to air tank；When cream item is extruded 1mm-2mm, stop into
Gas, and air tank exhaust pition is opened, so that pressure gauge is restored to zero, scrapes off the lotion of extrusion with the neat hose port of pocket knife, and close
Exhaust pition is pressed again by air, and when lotion is extruded 1mm-2mm, the number pressure of immediate record pressure gauge takes maximum survey
Definite value is measurement result；It squeezes cream pressure≤30KPa and judges its qualification.
Toothpaste made from embodiment 1-6 and comparative example 1-8 is placed 3 years at room temperature, and observes steadiness, is tied
Fruit is as shown in table 1；
Toothpaste made from embodiment 1-6 and comparative example 1-8 is placed in constant incubator and carries out high temperature accelerated aging tests, is seen
Trimestral steadiness is examined, the results are shown in Table 1.
1 stability test result of table
As shown in Table 1, toothpaste made from embodiment 1-6 has good stability.Toothpaste stability made from comparative example 1 is poor,
There is grease lamination, light discolouration then occurs in toothpaste made from comparative example 5, and toothpaste occurs slight point made from comparative example 7
Oil, but do not influence to use.Thus it proves, toothpaste of the invention has good stability.Lotion of toothpaste made from comparative example 1,5 and 7
Stability it is slightly poor, the toothpaste of comparative example 2,3,4,6,8 has good stability.The crowded cream pressure of all embodiment and comparative examples exists
In acceptability limit.
Toothpaste cleaning force is tested
Recommendable biomembrane cleaning ratio is recognized using American Dental Association ADA and tests (Pellicle Cleaning
Ration, PCR) test sample the exogenous color spot of removal whitening effect, specially：Enamel is made by ox central incisor
Block simulates people's tooth dyeing circumstances, is dyed to tooth enamel mass by the approach dyed in vitro, then is normally brushed teeth by Tooth-brushing device simulation
Frequency quantitative brushing times are carried out to the tooth enamel mass of dyeing, by colorimeter to before the dyeing of tooth enamel mass and after brushing teeth
L* values are monitored；International Commission on Illumination (CIE) L*a*b* standard colorimetric systems are most common colour systems in dentistry, should
L* indicates that visual sense lightness, a*, b* indicate form and aspect and chroma in system, and for the numerical value of L* in 0-100, the big person of lightness is small close to white
Person is close to black；Analysis grouping is carried out to data using spass softwares, A groups are substantially better than B groups, have significant difference；A groups
Slightly it is better than AB groups, but there was no significant difference；B groups are substantially better than C groups, have significant difference；B groups are slightly better than BC groups, but without aobvious
Write sex differernce；The case where evaluating the removal facing staining of toothpaste made from embodiment 1-6 and comparative example 1, comparative example 8,
Toothpaste or tooth powder are assessed to the cleaning force effect of tooth, the results are shown in Table 2：
2 cleaning force test result of table
Remarks：PCR=Δs L test specimens/Δ L standard samples * 100% ,-L baselines after Δ L=L polishings, calcium pyrophosphate is standard
Sample
As shown in Table 2, the toothpaste of embodiment 1-6 either selects electric toothbrush or ordinary toothbrush, cleaning force obviously high
In the toothpaste of comparative example 1 and comparative example 8.The toothpaste of embodiment 1-6 and comparative example 1 then use the cleaning effect of electric toothbrush excellent
In ordinary toothbrush, there is no statistics difference for the electric toothbrush of comparative example 8 and ordinary toothbrush cleaning force.Thus it proves, using this
The toothpaste cleaning effect of inventive composition is good, and cooperation electric toothbrush use has more preferably cleaning force effect.
Toothpaste wear test
The abrasiveness of toothpaste made from testing example 1-6 and comparative example 1, specially：Using surface roughness method, brushing
Ra (Roughness Average) value on tooth samples surface is detected with surface roughometer before and after mill test, with brush
The difference of Ra values evaluates the degree of wear of the sample to tooth samples before and after tooth, and Ra values are not more than 5.664 μm, then the abrasiveness of toothpaste
Can be it is safe (" 3 kinds evaluation toothpaste polishing machinees methods compare ", Sun Dongfang etc., daily chemical industry, 2016 volume 46
3rd phase, the 162-166 pages, publication date on 03 31st, 2016), the results are shown in Table 3.
3 abrasion test results of table
By 3 it is found that the Ra values of toothpaste made from embodiment 1-6, comparative example 1 and comparative example 8 are respectively less than 5.664 μm.Thus
Toothpaste cooperation electric toothbrush use made from proof, embodiment 1-6 and comparative example 1 can be reduced to tooth with manual toothbrush comparison
Abrasion, the attrition value that wherein electric toothbrush of embodiment 1 and the ordinary toothbrush of comparative example 1 reach is close, but the tooth of embodiment 1
The cleaning force toothpaste with obvious effects better than comparative example 1 of cream, comparative example 8 are connect using the attrition value of electric toothbrush and ordinary toothbrush
Closely.Thus it proves, the abrasion that can be significantly reduced to tooth is used using the toothpaste cooperation electric toothbrush of the present composition.
Toothpaste foam performance is tested
Surrounding area randomly chooses 20 people where inventor, uses electric toothbrush and ordinary toothbrush to embodiment 1- respectively
The toothpaste of 6 and comparative example 3-7 carries out foam performance and brushes teeth sensory testing, and the results are shown in Table 4.
4 foam performance test result of table
Remarks：It scores 1-5 points, 1 point worst, and 5 points best
As shown in Table 4, the toothpaste of embodiment 1-6 and comparative example 3-7 is dodging bubble property, foam volume, foam sophistication and temperature
In terms of property, it is better than ordinary toothbrush using electric toothbrush effect.Electric toothbrush coordinates the toothpaste of embodiment 1-6 to use, test
Person's usage experience is preferable, and without sensation of dryness, overall assessment is higher in oral cavity after use.Thus it proves, using the present composition
Toothpaste cooperation electric toothbrush use can bring experience of preferably brushing teeth to consumer.
The assessment experiment of tooth gloss degree
It is respectively brushed teeth primary, is removed sooner or later with the toothpaste of embodiment 1-6 and comparative example 2, comparative example 5, comparative example 6 and comparative example 7
Toothpaste is different outer, and other modes are identical, the glossiness of dental surface and whiteness situation after a week is observed, as a result such as 5 institute of table
Show：
5 tooth gloss degree assessment result of table
Remarks：It scores 1-5 points, 1 point worst, and 5 points best
As shown in Table 5, no matter the toothpaste of embodiment 1-6 uses which kind of toothbrush, the glossiness of tooth to be all substantially better than
Comparative example 2 and comparative example 5-7；For identical formulation of tooth-paste, electric toothbrush has more obvious polishing action to tooth, makes
Tooth has better glossiness；In terms of whiteness, for embodiment 1-6 and comparative example 2, comparative example 5-7, all using electric toothbrush
It scores than ordinary toothbrush high.Thus it proves, can effectively be carried using the toothpaste cooperation electric toothbrush use of the present composition
The glossiness and whiteness of high tooth.
Embodiment 7
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 9.5g, Cocoamidopropyl betaine 1g, beeswax
1g, saccharin sodium 0.4g, Natural menthol 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 78.8g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. after beeswax and Cocoamidopropyl betaine being crossed 300 mesh sieve, with mixture and dodecyl sulphur obtained by step A
Sour sodium is uniformly mixed to get the tooth powder.
Embodiment 8
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 8.5g, Cocoamidopropyl betaine 2.5g, bee
Wax 2g, saccharin sodium 0.4g, Natural menthol 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 77.3g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. after beeswax and Cocoamidopropyl betaine being crossed 300 mesh sieve, with mixture and dodecyl sulphur obtained by step A
Sour sodium is uniformly mixed to get the tooth powder.
Embodiment 9
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 7.9g, Cocoamidopropyl betaine 3.6g, bee
Wax 4g, saccharin sodium 0.4g, Natural menthol 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 75g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. after beeswax and Cocoamidopropyl betaine being crossed 300 mesh sieve, with mixture and dodecyl sulphur obtained by step A
Sour sodium is uniformly mixed to get the tooth powder.
Comparative example 9
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 9.5g, Cocoamidopropyl betaine 1g, saccharin
Sodium 0.4g, Natural menthol 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 77.8g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. mixed with mixture obtained by step A and lauryl sodium sulfate after Cocoamidopropyl betaine being crossed 300 mesh sieve
It closes uniformly to get the tooth powder.
Comparative example 10
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 10g, beeswax 2g, saccharin sodium 0.4g, natural peppermint
Brain 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 79.1g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. it after beeswax being crossed 300 mesh sieve, is uniformly mixed to get institute with mixture and lauryl sodium sulfate obtained by step A
State tooth powder.
Comparative example 11
Tooth powder, consisting of：Sodium bicarbonate 8g, lauryl sodium sulfate 8g, Cocoamidopropyl betaine 3.3g, beeswax
5g, saccharin sodium 0.4g, Natural menthol 0.8g, Herba Menthae powder essence 0.5g, calcium carbonate 74g.
The preparation method of the tooth powder is：
A. first by calcium carbonate, sodium bicarbonate, saccharin sodium, Natural menthol and Herba Menthae powder lappingout grinds and the sieve of 250 mesh excessively；
B. after beeswax and Cocoamidopropyl betaine being crossed 300 mesh sieve, with mixture and dodecyl sulphur obtained by step A
Sour sodium is uniformly mixed to get the tooth powder.
Tooth powder cleaning force is tested
Recommendable biomembrane cleaning ratio is recognized using American Dental Association ADA and tests (Pellicle Cleaning
Ration, PCR) test sample the exogenous color spot of removal whitening effect, specially：Enamel is made by ox central incisor
Block simulates people's tooth dyeing circumstances, is dyed to tooth enamel mass by the approach dyed in vitro, then is normally brushed teeth by Tooth-brushing device simulation
Frequency quantitative brushing times are carried out to the tooth enamel mass of dyeing, by colorimeter to before the dyeing of tooth enamel mass and after brushing teeth
L* values are monitored；International Commission on Illumination (CIE) L*a*b* standard colorimetric systems are most common colour systems in dentistry, should
L* indicates that visual sense lightness, a*, b* indicate form and aspect and chroma in system, and for the numerical value of L* in 0-100, the big person of lightness is small close to white
Person is close to black；Analysis grouping is carried out to data using spass softwares, A groups are substantially better than B groups, have significant difference；A groups
Slightly it is better than AB groups, but there was no significant difference；B groups are slightly better than BC groups, but there was no significant difference；Evaluate embodiment 7-9 and comparative example
The case where removal facing staining of tooth powder made from 10, assesses the cleaning force effect of toothpaste or tooth powder to tooth, as a result
As shown in table 6.
6 cleaning force test result of table
As shown in Table 6, the tooth powder of embodiment 7-9 either selects electric toothbrush or ordinary toothbrush, cleaning force to be better than
The tooth powder of comparative example 11.For the tooth powder of same recipe, also it is better than ordinary toothbrush using the cleaning effect of electric toothbrush.By
This is proved, more preferable using cleaning effect using the tooth powder cooperation electric toothbrush of the present composition.
Tooth powder wear test
The abrasiveness of tooth powder made from testing example 7-9 and comparative example 11, specially：Using surface roughness method,
Ra (Roughness Average) value on tooth samples surface is detected with surface roughometer before and after brushing test, is used
The difference evaluation sample for front and back Ra values of brushing teeth is to the degree of wear of tooth samples, and Ra values are no more than 5.664 μm, then the abrasion of tooth powder
Performance be it is safe (" 3 kinds evaluation toothpaste polishing machinees methods compare ", Sun Dongfang etc., daily chemical industry, 2016 the 46th
Rolled up for the 3rd phase, the 162-166 pages, publication date on 03 31st, 2016), the results are shown in Table 7.
7 abrasion test results of table
As shown in Table 7, the Ra values of embodiment 7-9 and the tooth powder of comparative example 11 are respectively less than 5.664 μm.Thus it proves, implements
Example 7-9 and the tooth powder of comparative example 11 will not damage tooth, and the tooth powder cooperation electric toothbrush of embodiment 7-9 and comparative example 11 use
The abrasion to tooth can be reduced.
Tooth powder foam performance is tested
Surrounding area randomly chooses 20 people where inventor, uses electric toothbrush and ordinary toothbrush to embodiment 7- respectively
9 and the tooth powder of comparative example 10 carry out foam performance and brush teeth sensory testing, the results are shown in Table 8.
8 foam performance test result of table
Remarks：It scores 1-5 points, 1 point worst, and 5 points best
As shown in Table 8, embodiment 7-9 and the tooth powder of comparative example 10 are dodging bubble property, foam volume, foam sophistication and mild
Property aspect, be better than ordinary toothbrush using electric toothbrush effect；Electric toothbrush coordinates the tooth powder of embodiment 7-9 to use, tester
Usage experience is preferable, and without sensation of dryness, overall assessment is higher in oral cavity after use.Thus it proves, using the tooth of the present composition
Powder cooperation electric toothbrush use can bring experience of preferably brushing teeth to consumer.
Tooth gloss degree is tested
It is respectively brushed teeth sooner or later with embodiment 7-9 and the tooth powder of comparative example 9 primary, in addition to tooth powder is different, the complete phase of other modes
Together, the glossiness of dental surface and whiteness situation after a week are observed, the results are shown in Table 9：
9 tooth gloss degree assessment result of table
Remarks：It scores 1-5 points, 1 point worst, and 5 points best
As shown in Table 9, no matter the tooth powder of embodiment 7-9 uses which kind of toothbrush, the glossiness of tooth to be all substantially better than
Comparative example 9；For the tooth powder of same recipe, electric toothbrush has more obvious polishing action to tooth, and tooth is made to have more
Good glossiness；In terms of whiteness, the tooth powder of embodiment 7-9 and comparative example 9 are all scored than ordinary toothbrush high using electric toothbrush.
Thus it proves, the cooperation electric toothbrush of the tooth powder of the present composition uses the glossiness that can effectively improve tooth and white
Degree.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (20)
1. oral care composition, which is characterized in that including rubbing agent and polishing agent.
2. oral care composition according to claim 1, which is characterized in that the rubbing agent is calcium carbonate, titanium dioxide
1-4 kinds in silicon, aluminium hydroxide and calcium pyrophosphate.
3. oral care composition according to claim 1 or 2, which is characterized in that the rubbing agent is opposite by dentine
The silica and dentine relative attrition value that silica, the dentine relative attrition value of attrition value ＜ 50 is 180-200 is
The silica composition of 130-170 forms.
4. oral care composition according to claim 3, which is characterized in that the rubbing agent is by dentine relative wear
The silica and dentine relative attrition value that silica, the dentine relative attrition value of value ＜ 50 is 180-200 are 130-
170 silica is according to 1:5-20:The mass ratio of 5-20 is composed.
5. oral care composition according to claim 1,2,3 or 4, which is characterized in that the polishing agent is cohune
1-6 kinds in palmitic acid wax, candelila wax, beeswax, shellac, microwax and paraffin.
6. according to the oral care composition described in claim 1,2,3,4 or 5, which is characterized in that further include foaming agent.
7. oral care composition according to claim 6, which is characterized in that the foaming agent is dodecyl sulphate
Sodium, cocounut oil acyl alanine triacetic acid ammonium, Cocoamidopropyl betaine, cocounut oil acyl glycine potassium, sodium cocoyl glycinate, bay
1-8 kinds in acylsarcosine sodium, laureth sodium sulfovinate and cocounut oil acyl glutamic acid triethanolamine.
8. according to the oral care composition described in claim 1,2,3,4,5,6 or 7, which is characterized in that in terms of mass parts, match
It is than relationship：0.1-5 parts of 22-82 parts of rubbing agent and polishing agent.
9. according to the oral care composition described in claim 1,2,3,4,5,6,7 or 8, which is characterized in that the oral cavity shield
Reason composition is toothpaste.
10. oral care composition according to claim 9, which is characterized in that further include moisturizer and/or thickener
And/or sweetener and/or essence and/or water.
11. oral care composition according to claim 10, which is characterized in that the moisturizer be sorbierite, glycerine,
1-4 kinds in propylene glycol and polyethylene glycol.
12. the oral care composition according to claim 10 or 11, which is characterized in that the thickener is that carboxymethyl is fine
1-7 kinds in the plain sodium of dimension, hydroxyethyl cellulose, carbomer, carragheen, guar gum, xanthans and silica dioxide gel.
13. according to the oral care composition described in claim 10,11 or 12, which is characterized in that the sweetener is saccharin
1-8 kinds in sodium, Aspartame, stevioside, Sucralose, acesulfame potassium, sucrose, xylitol and acetic acid sulfamic acid potassium.
14. according to the oral care composition described in claim 10,11,12 or 13, which is characterized in that in terms of mass parts, match
It is than relationship：22-47 parts of rubbing agent, 0.1-0.6 parts of polishing agent, foaming agent are no more than 60 parts no more than 3.0 parts, moisturizer, increase
Thick dose is no more than 1.5 parts no more than 2 parts, sweetener no more than 0.5 part, essence, and surplus is water, 100 parts of total amount.
15. oral care composition according to claim 14, which is characterized in that in terms of mass parts, rubbing agent 22-47
Part, 0.1-0.6 parts of polishing agent, 1.2-3.0 parts of foaming agent, 30-60 parts of moisturizer, 0.2-2 parts of thickener, sweetener 0.2-0.5
Part, 0.5-1.5 parts of essence, surplus are water, and total amount is 100 parts.
16. according to the oral care composition described in claim 1,2,3,4,5,6,7 or 8, which is characterized in that the oral cavity shield
Reason composition is tooth powder.
17. oral care composition according to claim 14, which is characterized in that further include sodium bicarbonate and/or sweet taste
Agent and/or Herba Menthae powder essence and/or Natural menthol.
18. oral care composition according to claim 17, which is characterized in that in terms of mass parts, proportion relation is：
70-82 parts of rubbing agent, 1-5 parts of polishing agent, foaming agent do not surpass no more than 12 parts, sodium bicarbonate no more than 10 parts, sweetener
Cross 0.8 part, Herba Menthae powder essence be no more than 0.7 part, Natural menthol be no more than 0.7 part.
19. oral care composition according to claim 18, which is characterized in that in terms of mass parts, proportion relation is：It rubs
70-82 parts of liniment, 1-5 parts of polishing agent, 8-12 parts of foaming agent, 0.2-0.8 parts of sweetener, 0.3-0.7 parts of Herba Menthae powder essence, natural thin
0.3-0.7 parts of lotus brain, 6-10 parts of sodium bicarbonate.
20. the preparation method of any one of the claim 1-15 oral care compositions, which is characterized in that including following step
Suddenly：
A. thickener is scattered in anhydrous moisturizer to no caking；
B. sweetener is dissolved in water, remaining moisturizer and foaming agent are added to together in the mixture of step A, are uniformly mixed；
C. polishing agent and rubbing agent are stirred evenly；
D. mixture obtained by step C is added in mixture obtained by step B, is stirring evenly and then adding into essence, stirs evenly, vacuum
Degassing forms lotion.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109288731A (en) * | 2018-11-23 | 2019-02-01 | 辉达生物医药（苏州）有限公司 | A kind of oral care product |
| CN115778846A (en) * | 2022-12-16 | 2023-03-14 | 广州立白企业集团有限公司 | Toothpaste for electric toothbrush |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85109119A (en) * | 1984-12-21 | 1986-08-27 | 帝国化学工业泛美公司 | Oral hygiene composition |
| JP2001003034A (en) * | 1999-06-22 | 2001-01-09 | Kao Corp | Abrasive |
| US7270803B1 (en) * | 2006-03-23 | 2007-09-18 | J.M. Huber Corporation | High-cleaning, low abrasion, high brightness silica materials for dentrifices |
| CN101060887A (en) * | 2004-06-18 | 2007-10-24 | 吉莱特公司 | Oral care compositions |
| CN103006445A (en) * | 2012-12-28 | 2013-04-03 | 美晨集团股份有限公司 | Toothpaste for simultaneously cleaning, whitening and restoring teeth and preparation method of toothpaste |
| CN105456062A (en) * | 2015-12-08 | 2016-04-06 | 宁波高欣生物科技有限公司 | Toothpaste friction agent and preparation method thereof |
| US20160220459A1 (en) * | 2007-05-10 | 2016-08-04 | Clarkson University | Methods for Polishing a Tooth Surface Utilizing Abrasive Nanoparticles |
| CN106727056A (en) * | 2017-03-03 | 2017-05-31 | 广州纳英化工有限公司 | A kind of MC new product is brushed teeth sugar and preparation method thereof and application method |
-
2018
- 2018-05-08 CN CN201810433715.4A patent/CN108354849B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85109119A (en) * | 1984-12-21 | 1986-08-27 | 帝国化学工业泛美公司 | Oral hygiene composition |
| JP2001003034A (en) * | 1999-06-22 | 2001-01-09 | Kao Corp | Abrasive |
| CN101060887A (en) * | 2004-06-18 | 2007-10-24 | 吉莱特公司 | Oral care compositions |
| US7270803B1 (en) * | 2006-03-23 | 2007-09-18 | J.M. Huber Corporation | High-cleaning, low abrasion, high brightness silica materials for dentrifices |
| US20160220459A1 (en) * | 2007-05-10 | 2016-08-04 | Clarkson University | Methods for Polishing a Tooth Surface Utilizing Abrasive Nanoparticles |
| CN103006445A (en) * | 2012-12-28 | 2013-04-03 | 美晨集团股份有限公司 | Toothpaste for simultaneously cleaning, whitening and restoring teeth and preparation method of toothpaste |
| CN105456062A (en) * | 2015-12-08 | 2016-04-06 | 宁波高欣生物科技有限公司 | Toothpaste friction agent and preparation method thereof |
| CN106727056A (en) * | 2017-03-03 | 2017-05-31 | 广州纳英化工有限公司 | A kind of MC new product is brushed teeth sugar and preparation method thereof and application method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109288731A (en) * | 2018-11-23 | 2019-02-01 | 辉达生物医药（苏州）有限公司 | A kind of oral care product |
| CN115778846A (en) * | 2022-12-16 | 2023-03-14 | 广州立白企业集团有限公司 | Toothpaste for electric toothbrush |
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| CN108354849B (en) | 2021-03-19 |
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