CN106727056A

CN106727056A - A kind of MC new product is brushed teeth sugar and preparation method thereof and application method

Info

Publication number: CN106727056A
Application number: CN201710123896.6A
Authority: CN
Inventors: 邹忌; 邹长清
Original assignee: Guangzhou Naying Chemical Co Ltd
Current assignee: Guangzhou Naying Chemical Co Ltd
Priority date: 2017-03-03
Filing date: 2017-03-03
Publication date: 2017-05-31
Anticipated expiration: 2037-03-03
Also published as: CN106727056B

Abstract

Brushed teeth sugar the invention discloses a kind of MC new product.By weight percentage, the sugar of brushing teeth is made up of 60% 95% sugared core segment and 5% 40% sugar shell coatings；The sugared core segment includes component：Wetting agent 0.01 50%, rubbing agent 0.01 40%, sweetener 0.01 40%, thickener 0.01 4%, from foaming agent 0.01 15%, buffer 0.02 5%, surfactant 0.02 10% eats aromatic 0.02 4%, and other functions additive is appropriate.It is of the invention to brush teeth sugar product when in use and all make us being as cheerful as a lark after, succinctly, oral cavity is placed on somewhat to chew several seconds, fragrance discharges full oral cavity quickly, foam is also produced quickly simultaneously, at this moment the toothbrush for picking up yours at one's side first dips in little water as using toothpaste, start to brush teeth, easily can realize cleaning of teeth and healthcare function within the of short duration time, reached the technique effect for cleaning one's teeth and nursing oral cavity.

Description

A kind of MC new product is brushed teeth sugar and preparation method thereof and application method

Technical field

The present invention relates to a kind of oral care product, belong to household chemicals technical field, more particularly to a kind of oral cavity Nursing new product is brushed teeth sugar and preparation method thereof.

Background technology

In the MC daily product field of nearest decades, there is no the product appearance of new raw material and neomorph, city Product homogeneity is abnormal serious on field, and the mode in people's cleaning oral cavity is to be brushed teeth with toothpaste sooner or later in daily life, or is chewed Chewing gum.

According to the definition of national standard, toothpaste is added containing rubbing agent, aromatic, NMF, thickener and other functions Plus the product of agent and the lotion shape formed under certain process conditions.From after 19 beginnings of the century invention toothpaste, the research of toothpaste, life Product technology becomes highly developed.It is required for opening lid when but toothpaste is used every time, then extrusion one dips on toothbrush Little water starts grooming, if the product of this form is carried on airborne vehicle and using all there is inconvenient place, makes Technique is also comparatively laborious, and tourism every time is all that the toothpaste specification for carrying is bothered, because board a plane can not carry more than 100ml's Flow-like material.The free toothpaste that hotel provides is used and perceptual quality is very poor, it is impossible to satisfied.

Continuous gum base eigen is that often have pockets of matrix after chewing, and these matrixs are polymerized to a bulk of, it is impossible to disperse, Can not be washed away with water, they be easy to it is unpleasant be attached on basin bottom, wall, sole or plant, it can not replace Toothpaste is used.

The author of the present invention is devoted to oral care product research decades, it is desirable to be able to create a kind of with breakthrough MC new product.

The content of the invention

Brushed teeth sugar and its application method it is an object of the invention to provide a kind of MC new product, when using and used Afterwards all can be pleasant, succinct, it is placed on oral cavity and somewhat chews several seconds, fragrance discharges full oral cavity quickly, while foam is also very Fast to produce, the toothbrush at this moment picking up yours at one's side is first dipped in little water as using toothpaste, starts to brush teeth, can be in the of short duration time It is interior easily to realize cleaning of teeth and healthcare function, reach the technique effect for cleaning one's teeth and nursing oral cavity.

Another object of the present invention is to provide the preparation method that a kind of MC new product brushes teeth sugar, the present invention is used The product being made can also realize as needed hemostasis as toothpaste, reduce sensitivity of tooth, it is mothproof, prevent halitosis, dispel Bacterial plaque, dispel tooth stain and other effects.

The purpose of the present invention and the technical problem of solution are realized using following technical scheme.Proposed according to the present invention A kind of MC new product brush teeth sugar, by weight percentage, the sugar of brushing teeth be by 60%-95% sugared core segment and The sugar shell coatings composition of 5%-40%；The sugared core segment includes following components：

Wetting agent 0.01-50%, rubbing agent 0.01-40%, sweetener 0.01-40%, thickener 0.01-4%, from foaming Agent 0.01-15%, surfactant 0.02-10%, eat aromatic 0.02-4%, and buffer 0.02-5%, other functions add Plus appropriate agent.

MC new product of the invention is brushed teeth sugar, and the sugar shell coatings are by ground floor, the second layer and third layer group Into；

The ground floor is including but not limited to microwax or paraffin, insect wax, beeswax, Brazil wax, other edibles Wax；Or including but not limited to the sugar-coat that xylitol, mannitol, marine alga sugar alcohol, maltitol make；

The sugar that the second layer sugar coating makes including but not limited to xylitol, mannitol, marine alga sugar alcohol, maltitol Clothing；

The third layer is including but not limited to microwax or paraffin, beeswax, insect wax, Brazil wax, other edibles Wax；Or the sugar-coat made comprising xylitol, mannitol, marine alga sugar alcohol, maltitol.

MC new product of the invention is brushed teeth sugar, and the sugar shell coatings include trehalose or maltitol, sweet dew The mixing more than one or both of sugar alcohol, its percentage in sugar-coat is 50-96%, and preferred proportion is 65-95%.

MC new product of the invention is brushed teeth sugar, it is described from foaming ingredient be sodium carbonate, potassium carbonate, sodium acid carbonate, In saleratus, citric acid, disodium hydrogen phosphate, dibastic sodium phosphate any one or both more than mixing, it accounts for sugared core segment weight Amount percentage composition is 0.01-15%, preferably 0.1-12%, more preferably 0.5-10%.

MC new product of the invention is brushed teeth sugar, and the thickener is carragheen or Carbomer or pectin, Arab Mixing more than glue, the one or both of xanthans, it accounts for sugared core segment percentage for 0.05-5%, is preferably in a proportion of 0.1- 4%；The surfactant is foaming agent, including but not limited to sodium lauroyl sarcosine, lauroyl Sodium Glycinate, dodecyl Sodium sulphate, alkyl-glucoside, cocounut oil acyl CAB etc., it accounts for sugared core segment percentage for 0.02-10%, preferred proportion It is 0.1-5%.

MC new product of the invention is brushed teeth sugar, and the wetting agent is including but not limited to glycerine, D-sorbite, the third two The nontoxic polyalcohols such as alcohol, polyethylene glycol, butanediol, inositol；

The abrasive be natural stone-powder of the granularity in the range of 20-2000 mesh, winnofil, dicalcium phosphate dihydrate, Hydroxyapatite, calcium pyrophosphate, calcium phosphate dibasic anhydrous, calcium phosphate, silica, aluminium hydroxide, anhydrous sodium metaphosphate, resin, String, microcrystalline cellulose, 4-A zeolites etc.；Preferable particle size 300-800 mesh particle as rubbing agent, but for picture Mild abrasive as string, chalina, it is also possible to from granularity in 50-800 mesh scopes as friction component；

It is thin that the aromatic includes but is not limited to liquid essence, powdered flavor, menthyl lactate, menthol, borneol, acetic acid Lotus ester, menthone glycerol ketals etc. one or several can increase fragrance and the composition received of refrigerant sense.

MC new product of the invention is brushed teeth sugar, and sweetener is contained in formula：Including but not limited to glucose, sugarcane The material with sense organ sweet taste such as sugar, fructose, mannose, maltose, stevioside, erythrose, xylitol, and those synthesis Material such as saccharin, Sucralose, acesulfame potassium, honey element, Aspartame etc. of sweet multiple high；

Can also be added in component Paeonol, tranxamic acid, sodium monofluorophosphate, sodium chloride, strontium chloride, potassium nitrate, vitamin, The effects such as material, it is also possible to reuse other plant extract such as Notogineng Extract, ginseng extract, the bark of official magnolia, soapberry, hardship The extract component of ginseng, chrysanthemum indicum, honeysuckle, rattletop, rhizoma imperatae, the root of Dahurain angelica, aloe, ilex pubescens, the coptis, the root of large-flowered skullcap, the capsule of weeping forsythia etc., may be used also To use the extract of animal extracts such as donkey-hide gelatin, honey.

In addition, the present invention also proposes that a kind of MC new product is brushed teeth the preparation method of sugar, walks comprising following technique Suddenly：

1) preparation of sugared core：

In a clean container for suitable capacity uniform stirring mixed foaming agent, blowing promotor, sweetener, excipient, Rubbing agent, thickener, wetting agent, characteristic effect adding ingredient etc. are until form the cream embryo of uniform and delicate, the viscosity of cream embryo, humidity Needs are controlled in suitable scope；During need to control the humidity of whipping temp and environment, cream embryo displays certain hour slightly Afterwards, be transferred on molding machine, mould cut according to definite shape, obtain have certain humidity, spherical or block, bar-shaped of hardness Grain；

2) ground floor sugar-coat is sprayed, microwax has been melted in advance, open coating pan, control kettle temperature, will at 40-80 DEG C Particles of these shapings are transferred in coating pan, are sprayed on microwax in the rotation of coating pan above sugared slug particle and are formed the A glace；

3) spray second layer sugar-coat, in advance by maltitol or, xylitol, mannitol and water and gum arabic press According to certain proportion, infusion, into syrup, checks viscosity, color, the transparency states of syrup in sugar boiler；Shift obtained by the 2nd step In particle to coating pan, the sugar-coat is sprayed at into particle surface at 50-120 DEG C of temperature under the rotation status (if necessary must be Sprayed under spraying equipment inner pressure relief)；

4) polish, at 60-120 DEG C of temperature, Brazil wax on the 3rd step gained particle spray coating is polished (necessary When must be sprayed under spraying equipment inner pressure relief).

In addition, a kind of MC new product of the invention is brushed teeth, the application method of sugar can be expressed as：

First take the flake products being made and put into oral cavity and chew, product can bubble automatically quickly during chewing, fragrance is also quickly Release, at this moment picks up toothbrush and dips in fraction of water, to put in start in the mouth and brushes teeth, and foam in discharge oral cavity, clear with clear water after a few minutes Wash clean oral cavity.

Product of the invention has very big difference with tooth piece alleged on the market at present, and tooth piece is using microcrystalline cellulose figuration Effect is directly squeezed into dry, and its manufacture craft is with making tablet, because particle when being chewed without wetting agent tooth piece Dry, because no thickener tooth piece is difficult to bubble, foam is easy to rupture, because the essence tooth piece without liquid is almost without perfume Gas, this tooth piece greatly limit the mouthfeel of product because any fluent material such as glycerine and liquid essence can not be used And efficacy capability.Moistening easily foaming in oral cavity when product is chewed is not gone out like the present invention, fragrance release is abundant, after the completion of brushing teeth still Right lasting overflows, and the experience after use is felt and brushes teeth very similar.

By above-mentioned technical proposal, the present invention has following different advantage and beneficial effect：

1) MC new product of the invention is brushed teeth sugar, can do slabbing, it is also possible to make round bead shape, granular, can Be packaged in the scraps of paper with by them, in food bag film, in plastics or glass bottle, be put into after packaging in your trouser pocket, knapsack, The ground at arbitrary your the satisfied showplace any for being carried to the earth, uses at any time, easy as toothpaste without worrying Flow out that to make all be all over the body lotion from damaged lid, such as can be packaged in a small paper envelope with 4, it is also possible to More satisfactory it is sufficient that travelling 2-3 days outside with 6, you can also be flown using the packaging of a bottle hundreds of Everywhere ball each place, nobody does not have place to forbid, very convenient to carry.But the container for containing toothpaste must be special The plastic tube or tank of system, otherwise easily leakage is fragrant and overflows lotion.

2) can all make us being as cheerful as a lark when product of the invention is used and after using, succinctly, be placed on oral cavity and somewhat chew several Second, the inner core of its softness has been experienced immediately, fragrance discharges full oral cavity quickly, while foam is also produced quickly, picks up tooth Brush first dips in little water as using toothpaste, starts to brush teeth, and easily can realize cleaning of teeth and guarantor within the of short duration time Health-care function, has reached the technique effect for cleaning one's teeth and nursing oral cavity, certainly, if at this moment you are at one's side without toothbrush, just as in work Make state just in the white collars of office, also it doesn't matter for that, told after chewing tens seconds and gargled with clear water, oral cavity is full with regard to delicate fragrance Overflow.

3) after the completion of it is not like pellet, and chewing gum is non-foaming, cannot also be brushed teeth after the completion of chewing, and it is chewed Can remaining matrix need to spue, the sugar of brushing teeth is no matrix, and it can not bring like chewing gum unpleasant everywhere can The matrix being stained with.

4) it is not also like the product for being tooth piece for occurring recently, this product difference without core and outer layer as tablet Not, manufacture craft is also as pharmacy.It is from inside to outside homogeneous components, it is harder when chewing, it is difficult to chew, for year elder The old man of loss of tooth cannot more be chewed, and the fragment for chewing out is dried, uncomfortable.Sugared skin of brushing teeth of the invention is thin and brittle easily to chew, and core It is soft and soak comfortable a lot.

Specific embodiment

As any product innovation, new product must all bring the more preferable adventure in daily life of the mankind, convenience and comfortable pleasure Degree.The present invention proposes that a kind of new oral care product is brushed teeth sugar, and this sugar of brushing teeth is including but not limited to containing a kind of nozzle A large amount of foams are produced from foaming ingredient when chewing, during chewing, facing and mucous membrane of mouth is washed away, it provides and gives people a kind of chewing mouth perfume The impression of sugar, provides a kind of impression brushed teeth with toothpaste again.This sugar of brushing teeth is chewed after meeting water and disperseed, and can be told as toothpaste Go out and washed away without resulting in blockage with water, it is non-foaming after chewing-gum chewing, toothbrush can not be used, because not relaxing like that Clothes, but product of the invention can produce abundant foam, the grooming as toothpaste that can be very comfortable.

Drop it into and chew in the mouth, it discharges fragrance in one's mouth immediately；The product bubbles automatically after several seconds, flush with foam Tooth, with toothbrush grooming in the oral cavity, its abundant foam, rubbing agent, functional additive can be cleaned as toothpaste, protected again Reason tooth and oral cavity.

Brushed teeth sugar the invention discloses a kind of MC new product, by weight percentage, the sugar of brushing teeth is by sugared core Part and sugar shell coatings composition；Sugared core segment is included：Wetting agent 0.01-50%, rubbing agent 0.01-40%, sweetener 0.01- 40%, thickener 0.01-4%, from foaming agent 0.01-15%, the edible virtues of buffer 0.02-5% surfactants 0.02-10% Pastil 0.02-4%, other functions additive is appropriate；Sugar shell coatings：Appropriate microwax, appropriate multi-sugar alcohol, Brazil wax are fitted Amount, appropriate amount of water, appropriate gum arabic.

MC new product of the invention is brushed teeth sugar, wherein containing from foaming ingredient sodium acid carbonate (or potassium), its weight hundred It is 0.01-15% to divide than content, preferably 0.1-12%, more preferably 0.5-10%.

MC new product of the invention is brushed teeth sugar, wherein containing from foaming ingredient citric acid, its total amount degree It is 0.01-10%, preferably 0.1-5%, more preferably 0.2-2%

MC new product of the invention is brushed teeth sugar, wherein containing from foaming ingredient sodium carbonate and sodium acid carbonate (or potassium), Its weight percent content is respectively sodium carbonate (or potassium) 0.01-15%, sodium acid carbonate (or potassium) 0.01-15%, preferred proportion It is respectively sodium carbonate (or potassium) 0.1-12%, sodium acid carbonate (or potassium) 0.01-12%；More preferably ratio sodium carbonate (or potassium) 0.5- 10%th, sodium acid carbonate (or potassium) 0.5-10%；

MC new product of the invention is brushed teeth sugar, wherein containing from foaming ingredient sodium carbonate (or potassium), sodium acid carbonate (or Potassium), citric acid, its weight percent content is respectively sodium carbonate (or potassium) 0.01-15%, sodium acid carbonate (or potassium) 0.01- 15%, citric acid 0.01-15%, preferred proportion are respectively sodium carbonate (or potassium) 0.1-12%, sodium acid carbonate (or potassium) 0.1- 12%th, citric acid 0.1-12%；More preferably ratio be sodium carbonate (or potassium) 0.5-10%, sodium acid carbonate (or potassium) 0.5-10%, Citric acid 0.2-2%.

MC new product of the invention is brushed teeth sugar, and the wetting agent is including but not limited to glycerine, D-sorbite, the third two The nontoxic polyalcohols such as alcohol, polyethylene glycol, butanediol, inositol.

MC new product of the invention is brushed teeth in saccharic composition, and the rubbing agent is：Such as granularity is in 20-2000 mesh models Enclose interior natural stone-powder, winnofil, dicalcium phosphate dihydrate, hydroxyapatite, calcium pyrophosphate, calcium phosphate dibasic anhydrous, phosphoric acid Calcium, silica, aluminium hydroxide, anhydrous sodium metaphosphate, resin, string, microcrystalline cellulose, 4A zeolites etc.；Preferable particle size 300-800 mesh particle as rubbing agent, but for the mild abrasive as string, it is also possible to existed from granularity 100-800 mesh scopes are used as friction component.The use of rubbing agent can in chewing and grooming brush them and mucous membrane of mouth table Face, so as to take away the dirt on surface.

It is comprising surfactant in component：The nontoxic surface of anion, cation, nonionic or both sexes Activating agent, makes consumer produce enough foams when in use, such as：Lauryl sodium sulfate, sylvite, sodium lauroyl sarcosine, Potassium, lauroyl Sodium Glycinate, potassium, cocamidopropyl betaine, alkyl-glucoside, fatty alcohol carboxylate, fatty alcohol polyoxy The safety such as ethene phosphoric acid (carboxylic acid, sulfonic acid) ester material harmless to the human body, preferably those food grade materials or pharmaceutical grade materials.

Thickener is：Cellulose gel, sodium carboxymethylcellulose, xanthan gum, modified guar, carragheen, Carbomer, hydroxyl Ethyl cellulose, tragacanth gum, Arabic gum, konjac glucomannan, pectin, gellan gum, Prussia's polysaccharide, mineral coagulant such as lithium metasilicate magnesium, Thickening type silica, sodium alginate, microcrystalline cellulose, cellulose gel etc.；

What sweetener was generally comprised but do not limited is the saccharin sodium of pharmaceutical grade or food-grade, acesulfame potassium, Sucralose, sweet Synanthrin, Aspartame；Also include but do not limit xylitol, glucose, mannitol, trehalose, maltitol, erythrose, fruit Natural sweet taste composition such as sugar, sucrose etc..

Also include aromatic such as essence, preferably food-grade chewing gum essence in component.

Can also be added in component preservative, food coloring, deionized water, pearlizing ingredients, colour particles, titanium dioxide etc. with And some can increase the material of product feature.

Can also be added in combination Paeonol, tranxamic acid, sodium monofluorophosphate, sodium chloride, strontium chloride, potassium nitrate, vitamin, The effects such as zinc citrate material, it is also possible to reuse other plant extract such as 37 extracts, ginseng extract, the bark of official magnolia, The extract component of soapberry, kuh-seng, honeysuckle, chrysanthemum indicum, the coptis, the capsule of weeping forsythia, the root of large-flowered skullcap, Radix Angelicae Sinensis, rhizoma imperatae, the tuber of dwarf lilyturf etc., can be with Using animal extracts such as donkey-hide gelatin, honey, snake oil etc., as long as nontoxic do not damage this hair not conflicting with the present invention pharmacologically The material of bright purpose can be applied in the present invention.

Buffer in component can be material, such as the citric acid, hydrogen citrate two of the sugared core acid-base balance of any control The band hydrogen salt of sodium, dibastic sodium phosphate, disodium hydrogen phosphate etc. Multiple Weak Acid.

Used as a preferred embodiment, sugar of brushing teeth of the invention includes sugared sandwich layer and sugar-coat, and the sugarcoating layer is applied by first Layer wax coating, second coating sugar coating, the 3rd coating wax coating is constituted, and its sugared sandwich layer ratio is：Wetting agent 0.01-50% (weights Amount percentage, similarly hereinafter), rubbing agent 0.01-40%, sweetener 0.01-40%, thickener 0.01-4%, from foaming agent 0.01- The edible aromatic 0.02-4% of 15%, buffer 0.02-5% surfactants 0.02-10%, other functions additive is appropriate； Ground floor wax coating is microwax 100%；It is gum arabic 0.01-10%, trehalose that second coating applies sugar layer material ratio 0.05-90%, water 0.05-30%, third layer coating are Brazil wax 90-99.5%, titanium dioxide 0.5-10%.

The technique for making this product is classified into four steps：

1st, the preparation of sugared core：The uniform stirring mixed foaming agent, self foaming agent, sweet in a clean container for suitable capacity Taste agent, rubbing agent, thickener, wetting agent, characteristic adding ingredient etc. are the viscosity of cream embryo, wet until form the cream embryo of uniform and delicate Degree needs are controlled in suitable scope.During need to control the humidity of whipping temp and environment, cream embryo displays a timing slightly Between after, be transferred on molding machine, cut mould according to definite shape, obtaining has certain humidity, the spherical or blocky-shaped particle of hardness；

2nd, ground floor sugar-coat is sprayed, microwax has been melted in advance, open coating pan, control kettle temperature, will at 40-80 DEG C Particles of these shapings are transferred in coating pan, are sprayed on microwax in the rotation of coating pan above sugared slug particle and are formed the A glace；

3rd, spray second layer sugar-coat, in advance by trehalose or, xylitol, mannitol, maltitol and water and I Infusion, into syrup, checks viscosity, color, the transparency states of syrup to uncle's natural gum in sugar boiler according to a certain percentage.Shift the 2nd In particle to coating pan obtained by step, the sugar-coat is sprayed at particle surface at 50-120 DEG C of temperature under the rotation status；System This layer of sugar-coat made is very crucial to product quality, and the selection of its moisture ratio and sugar type is extremely important, inappropriate choosing Select and will be difficult to make product that there is the smooth outward appearance of drying within storage period, have impact on the shelf-life of product.When making this step sugar-coat It should also be appreciated that particle must be controlled in the very short time period in coating pan, temperature and humidity is regulated.Such as temperature adjustment too Height is not suitable for particle spray coating, can select and is sprayed in the spraying pot of decompression in pot

4th, polish, will Brazil wax be polished in spraying on particle obtained by the 3rd step at 60-120 DEG C of temperature.Equally This step is also required to control time, temperature and humidity of the particle in coating pan.Be not suitable for particle spray coating as temperature is too high, it is optional Sprayed with the spraying pot of decompression in pot.

Each step spraying thickness be required for control, especially layers 2 and 3 polishing layer ensure that by It is as far as possible thin in the case of grain seal isolation air.Because polishing layer too thick chewing when have hard crisp piece of generation, as having impurity, The thin layer as chewing gum is made, is chewed just without foreign body sensation.

The sugar-coat for making this its outer layer of product is extremely important, although we can use xylitol, erythrose, grape The carbohydrates such as sugar, sucrose do sugar-coat, but, these components store a period of time after easily the moisture absorption and cause sugar-coat soften cracking, Storage period and quality are reduced, fusing point sugar too high is not appropriate for making sugar-coat, it is possible to being selected as the sugar that sugar-coat is used It is little.

The ratio for making syrup water is equally critically important, and suitable ratio can just obtain the good shelf-life, while again It is easy into slurry spraying.During syrup is boiled, moisture scatters and disappears at any time, and the final contained humidity of its sugarcoating layer is to be worth fastidious Problem.Suitable water content stored in a humidity environment by product be also not easy sugar-coat quickly soften it is rotten.

The present invention is described in further detail below by way of specific preferred embodiment, but the present invention be not limited in it is following Embodiment.Percentage in following components is weight percent content.

Embodiment 1

A kind of MC new product is brushed teeth sugar, and comprising sugared core segment and sugar shell coatings, concrete component is as follows,

Sugared core segment：(weight is percentage composition, total amount 100% in its formula)：

Dicalcium phosphate dihydrate 24%；Cellulose gel 12%；Glycerine (NMF) 30%；Carragheen 2.0%；Dodecyl Sodium sulphate (foaming agent) 3.6%；Sodium lauroyl sarcosine (foaming agent) 1.0%；Sucralose (sweetener) 0.4%；Edible perfume Essence (flavouring agent) 2..4%；Sodium acid carbonate 1.2%；Sodium carbonate 3.0%；Xylitol 20%；Citric acid：0.2%；Methyl hydroxybenzoate 0.2%；

Sugar shell coatings formula is：First coating, pure microwax；Second coating formula is：The deionized water of Arabic gum 12% 24%, trehalose 74%；3rd coating Brazil wax 100%；

Preparation method can be expressed as follows：

1st, at ambient temperature by carragheen dispersing and dissolving in above-mentioned material sequentially added in glycerine, then xylitol, Sucralose, methyl hydroxybenzoate, cellulose gel, calcium monohydrogen phosphate, citric acid, sodium carbonate, sodium acid carbonate are slowly stirred uniform shape Into without the fine and smooth creamy material of particle, it is subsequently adding lauryl sodium sulfate, sodium lauroyl sarcosine, essence and is stirred for Even, creamy material is soft but tack-free, uses mould extrusion molding.

2nd, ground floor is sprayed：Crystallite wax thickness about 0.5-30um, formula rate：100% microwax；Sprayed in coating pan Ground floor.

3rd, the 2nd coating is sprayed：

Gum arabic is scattered in warm water in advance, load weighted trehalose is subsequently adding, mixing and stirring, slowly It is warming up to mixture to melt completely, rotates coating pan, control sugar-coat pot temperature for 70-90 DEG C, is sprayed at step gained particle table Face, rotary speed is 50-60r/m between 5s-50s the time in coating pan to keep particle.

4th, the 3rd coating：Coating pan is opened, control sugar-coat kettle temperature will melt in 90 ± 1 DEG C of rotary speed 50rps The Brazil wax of change is sprayed at particle surface obtained by step in coating pan, forms uniform and smooth outer layer.

Compliance test result

Embodiment of the present invention compliance test result can be expressed as follows：

The product that the application formula and technique are made, is packaged into the bottle of 200, every box, is distributed to 10 volunteers, Boarded a plane with travelling band, smoothly passed through during safety check.Oral cavity discharge clear water first is soaked with clear water using preceding, one is then poured out from bottle Brush teeth sugar, the sugared particle that will brush teeth is put into oral cavity chewing, and a large amount of foams generations, adjoint fragrance overflow lip, pick up tooth after about 10-15 second Brush examination brush tens seconds to two minutes, oral cavity is clean, material in discharge opening, is contained with clear water and gargles and spue.

During chewing and brushing teeth, impression is recorded, and scored.

10 volunteer's scorings are collected, arithmetic mean of instantaneous value is calculated as shown in table 1 below：

In table 1：Every a reference value for feeling index of toothpaste and chewing gum is set to 10 points, sugar is brushed teeth such as and corresponding product It is close then to points 10 points, such as impression be better than a reference value if provide 11 points, it is more to provide 12 points better than a reference value, better than a reference value very At most provide 13 points；Conversely, providing 9 points if a reference value that impression is worse than setting, such as relatively it is worse than a reference value and provides 8 points, difference is very 7 points are at most given, as this cannot compare, are not scored (use/represent).

The embodiment of table 1 uses sense organ effect comparison table with different type oral care product

From the total result of above-mentioned table 1, the volunteer for using thinks：The product has more preferable than toothpaste and chewing gum Use feeling.It can replace toothpaste as the product in the cleaning oral cavity that cleans one's teeth.

Embodiment 2

Dicalcium phosphate dihydrate 31%；Glycerine (wetting agent) 30%；Carragheen 1.2%；Carbomer 0.8%；Lauroyl flesh ammonia Sour sodium (surfactant-foaming agent) 3.5%；Sucralose (sweetener) 0.2%；Acesulfame potassium 0.2%；Flavoring essence (fragrance Agent) 2.0%；Sodium acid carbonate 3%；Sodium carbonate 0.5%；Mannitol 26%；Disodium-hydrogen：0.2%；Potassium nitrate 0.8%；It is male Cortex Moutan extract 0.2%；Menthyl lactate 0.1%；WS-23 0.1%；The propylben 0.1% of methyl hydroxybenzoate 0.1%.

Sugar shell coatings formula is：Ground floor, pure microwax；Second layer coating formula is：Arabic gum：9%, deionized water 20%, maltitol 71%.Third layer is matched：Brazil wax 99%, titanium dioxide 1%.

Making step is as follows：

1st, carragheen, carbomer dispersion in above-mentioned material are dissolved in glycerine at ambient temperature, are then sequentially added Xylitol, Sucralose, acesulfame potassium, methyl hydroxybenzoate, propyl ester, calcium monohydrogen phosphate, citric acid, sodium carbonate, sodium acid carbonate, phosphoric acid hydrogen Sodium, potassium nitrate etc., are slowly stirred and are formed uniformly without particle, fine and smooth paste, are subsequently adding sodium lauroyl sarcosine, essence (dissolving Cortex Moutan extract in advance) is stirred for uniformly, and creamy material is soft but tack-free, is extruded with mould and cuts into easily throwing The particle or bulk for spreading.

2nd, ground floor is sprayed：Coating pan is opened, control kettle temperature will be melted into the microwax spray of liquid at 50-80 DEG C It is applied to particle surface, spray time 10-50 seconds, thickness about 0.1-30um, formula rate：100% microwax；Sprayed in coating pan Apply ground floor

3rd, the 2nd coating is sprayed：

Endure slurry：Gum arabic is scattered in warm water in advance, load weighted maltitol is subsequently adding, mixed equal It is even, it is to slowly warm up to mixture and melts completely.Spraying：Rotation coating pan, controls sugar-coat pot temperature for 70-90 DEG C, and sugar-coat is starched Step gained particle surface is sprayed at, rotary speed is 30-60rps between 5s-50s the time in coating pan to keep particle.

4th, the 3rd coating：The Brazil wax that will have melted be sprayed in coating pan step obtained by particle surface formed Uniform and smooth outer layer.

Compliance test result

45 volunteers for there are teeth sensitive symptoms are chosen, experiment is compared.It is divided into A, B, C group, every group of 15 people, before packet 5 ± 2 DEG C of freezing running water is contained with spray gun, is sprayed around the facing of sensitive teeth with uniform pressure, allow volunteer to experience What cold water brought feels bad degree and by the marking of this degree, first each volunteer is tested before experiment and provides fraction, controls Per cell mean, sex, there was no significant difference for age distribution difference, when chilled water is persistently ejected into disease teeth face, nociception It is insufferable to provide 5 points；Though there is pain but can stand and provide 3 points；Though experience Quench tooth do not have pain or The very slight person of pain provides 1 point, certainly for better closer to 1 point for cacodontia.A groups the present embodiment product on probation 25 days, B The toothpaste 25 days that group is made using addition equal amount potassium nitrate and Paeonol extract, C groups are using without adding potassium nitrate and pellet The toothpaste that skin phenol extraction thing makes 25 days, it is all 2 times to exhort every group of daily access times of no one, every time close to 3 minutes.

The particle every of the present embodiment on probation weighs about 1.5 grams, and contrast toothpaste also requires that every time on probation substantially 1.5 grams (squeezing Demonstrated on toothbrush), paid a return visit in test process and repeat to exhort.Result such as table 2 below：

The volunteer of table 2 the present embodiment on probation is contrasted (data are arithmetic mean of instantaneous value in table) with the sensitivity of tooth degree of reference substance

	A groups	B groups	C groups
				Before on probation	3.80±1.47	4.06±1.28	4.06±1.28
After 25 days	2.20±1.26	2.33±1.44	3.93±1.48

The result of table 2 is shown：Product of the present invention uses the A groups after 25 days and the sensitivity of tooth of the B groups using toothpaste Degree is all substantially reduced (p<0.05), better than C groups are not added with the blank toothpaste of functional component.Experiment of brushing teeth demonstrates this Invention product ability with certain prevention mouth disease as toothpaste.

Embodiment 3

Natural whiting 17%, silica 1 8%；Glycerine (NMF) 24%；Carragheen 1.2%；Dodecyl sulphate Sodium (foaming agent) 3.0%；Cocounut oil acyl CAB 0.6%；Sucralose (sweetener) 0.3%；Saccharin sodium 0.2；Edible perfume Smart (flavouring agent) 1.8%；Sodium acid carbonate 1.2%；Sodium dihydrogen phosphate 2%；Tertiary sodium phosphate 0.6%；Glucitol 28%；Nipalgin Methyl esters 0.3%；Menthyl lactate 0.6%；Titanium dioxide 0.3%；Magnolia cortex P.E 0.6%；Kuh-seng alkali extract 0.3%.

Sugar shell coatings formula is：Ground floor pectin：10% deionized water 20%, trehalose 65%, xylitol 5%.Second Layer Brazil wax 100%.

Making step is as follows：

1st, carragheen dispersing and dissolving in above-mentioned material in glycerine, is then sequentially added into glucose at ambient temperature Alcohol, Sucralose, saccharin sodium, methyl hydroxybenzoate, propyl ester, natural whiting, silica, sodium acid carbonate, sodium dihydrogen phosphate, phosphorus Sour sodium etc. is slowly stirred and is formed uniformly without particle, fine and smooth paste, is subsequently adding surfactant, essence and is stirred for uniformly, The outward appearance and humidity of observation detection cream embryo, extruded with mould cut into coating pan or other rotary pots easily shed Grain is block.

2nd, ground floor is sprayed：

Endure slurry：Pectin is scattered in warm water in advance, load weighted marine alga sugar alcohol, xylitol is subsequently adding, mixed Uniformly, it is to slowly warm up to mixture to melt completely, and decocts a few minutes slightly.

Spraying：Rotation coating pan, controls sugar-coat pot temperature for 70-90 DEG C, and sugar-coat slurry is sprayed at into upper step gained particle table Face, rotary speed is 30-60rps between 5s-50s the time in coating pan to keep particle.

3rd, second coating is sprayed：The Brazil wax that will have melted is sprayed at particle surface obtained by step in coating pan Form uniform and smooth outer layer.

Compliance test result

The product made of the inventive embodiments 3 is tested.15 volunteers are chosen, Evaluation product is carried out to them before experiment Mode, the time, perceive training.Implication is tested with implication tester before brushing teeth, they is then divided into three groups --- first Group, second group and third group, there was no significant difference for the average value and standard deviation of implication test value before controlling every group to brush teeth, after brushing teeth again Must not be eaten before secondary test or drink anything.First group chews certain reputable brand chewing gum 4 minutes, and it is real that second group chews the present invention the 3rd Apply brushing teeth sugared and brushing teeth for example, it is desirable to which second group is chewed and the time of merging of brushing teeth also is 4 minutes, and third group is used certain reputable brand Toothpaste is brushed teeth 4 minutes.

After every group of 50 points of completion clean mouth, implication value is tested, it is as shown in table 3 below.

The embodiment of table 3 and reference substance brush teeth after implication test table

Test event	First group	Second group	Third group
				Use preceding (arithmetic mean of instantaneous value, ppm)	320	315	323
Use (arithmetic mean of instantaneous value, ppm) after 50 minutes	189	85	122

The result of table 3 can be seen that：Using preceding, three groups have a certain degree of halitosis per capita, try out different dentifrices Implication all obtains different improvement afterwards.But prove that there is the halitosis that cleans one's teeth more more preferable than toothpaste to imitate using product of the invention Really, reached the purpose of breath freshening, although and can mitigate implication bad smell with chewing-gum chewing merely, effect is remote Far away from the effect using product of the present invention and this mode that cleans one's teeth of the invention.

The above, is only presently preferred embodiments of the present invention, and any formal limitation is not made to the present invention, therefore It is every without departing from technical solution of the present invention content, any simply repaiied according to what technical spirit of the invention was made to above example Change, equivalent variations and modification, still fall within the range of technical solution of the present invention.

Claims

1. a kind of MC new product is brushed teeth sugar, it is characterised in that：By weight percentage, the sugar of brushing teeth is by 60%- 95% sugared core segment and the sugar shell coatings composition of 5%-40%；The sugared core segment includes following components：

Wetting agent 0.01-50%, rubbing agent 0.01-40%, sweetener 0.01-40%, thickener 0.01-4%, from foaming agent 0.01-15%, buffer 0.02-5%, surfactant 0.02-10%, eat aromatic 0.02-4%, other functions addition Appropriate agent.

2. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：The sugar shell coatings are by first Layer, the second layer and third layer composition；

The ground floor is including but not limited to microwax or paraffin, insect wax, beeswax, Brazil wax, other edible waxes；Or Including but not limited to the sugar-coat that xylitol, mannitol, marine alga sugar alcohol, maltitol make；

The sugar-coat that the second layer sugar coating makes including but not limited to xylitol, mannitol, marine alga sugar alcohol, maltitol；

The third layer is including but not limited to microwax or paraffin, beeswax, insect wax, Brazil wax, other edible waxes；Or Comprising the sugar-coat that xylitol, mannitol, marine alga sugar alcohol, maltitol make.

3. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：The sugar shell coatings include marine alga Mixing more than sugar or maltitol, mannitol, the one or both of xylitol, its percentage in sugar-coat is 50- 96%, preferred proportion is 65-95%.

4. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：It is described from foaming ingredient be carbonic acid In sodium, potassium carbonate, sodium acid carbonate, saleratus, citric acid any one or both more than mixing, its weight percentage is 0.01-15%, preferably 0.1-12%, more preferably 0.5-10%.

5. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：The thickener be carragheen or The mixing more than one or both of Carbomer or xanthans or pectin or cellulose gel or gellan gum, its percentage is 0.01-4%, is preferably in a proportion of 0.1-4%；

The surfactant is foaming agent, including but not limited to sodium lauroyl sarcosine, lauroyl Sodium Glycinate, with 8-14 Fatty alcohol acylamino acid sodium (or potassium) salt of individual carbon, fatty alcohol sulfate sodium (or potassium) salt with 8-14 carbon of carbochain, band There is fatty alcohol carboxylic acid esters' sodium (or potassium) salt of 8-14 carbochain of carbon；Alkyl-glucoside, alkyl sucrose glycosides, cocounut oil acyl propyl group beet Alkali etc., its percentage is 0.02-10%, is preferably in a proportion of 0.1-5%.

6. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：The wetting agent is included but not limited In the nontoxic polyalcohols such as glycerine, D-sorbite, propane diols, polyethylene glycol, butanediol, inositol；

The abrasive is natural stone-powder, winnofil, dicalcium phosphate dihydrate, hydroxyl of the granularity in the range of 20-2000 mesh Apatite, calcium pyrophosphate, calcium phosphate dibasic anhydrous, calcium phosphate, silica, aluminium hydroxide, anhydrous sodium metaphosphate, resin, plant Fiber, microcrystalline cellulose etc.；Preferable particle size 300-1000 mesh particle as rubbing agent, but for as string Mild abrasive, it is also possible to from granularity in 50-800 mesh scopes as friction component；

The aromatic includes but is not limited to one or several energy such as liquid essence, powdered flavor, menthyl lactate, menthol It is enough to increase the composition that fragrance and refrigerant sense are received.

7. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：Contain sweetener in formula：Bag Glucose, sucrose, fructose, mannose, maltose, stevioside, erythrose, xylitol etc. are included but are not limited to sense organ sweet taste Material, and those synthesis high sweet multiples material such as saccharin, Sucralose, acesulfame potassium, honey element, Aspartame etc..

8. MC new product according to claim 1 is brushed teeth sugar, it is characterised in that：The root bark of tree peony can be also added in combination The effects such as phenol, tranxamic acid, sodium monofluorophosphate, sodium chloride, strontium chloride, potassium nitrate, vitamin, material was appropriate, it is also possible to reuse The extract component of other plant extract such as Notogineng Extract, ginseng extract, the bark of official magnolia, soapberry, kuh-seng, can also use The extract of animal extracts such as donkey-hide gelatin, honey.

9. the MC new product any one of claim 1-8 brush teeth sugar preparation method, it is characterised in that：Be by Following steps are prepared：

1) preparation of sugared core：

In clean container uniform stirring mixed surfactant (foaming agent), from foaming agent, sweetener, rubbing agent, thickener, Wetting agent, aromatic, characteristic addition functional component etc. are until form the cream embryo of uniform and delicate；

2) spray ground floor sugar-coat, melted microwax in advance, open coating pan, control kettle temperature 40-80 DEG C by these The particle of shaping is transferred in coating pan, is sprayed on microwax in the rotation of coating pan above sugared slug particle and is formed ground floor Sugar-coat；

3) spray second layer sugar-coat, in advance by trehalose or, xylitol, mannitol and water and gum arabic be according to certain Ratio in sugar boiler infusion into syrup；Shift in particle to the coating pan obtained by the 2nd step, the syrup exists under rotation status Particle surface is sprayed at 50-120 DEG C of temperature；

4) polish, at 60-120 DEG C of temperature, Brazil wax on the 3rd step gained particle spray coating is polished.

10. MC new product according to claim 9 is brushed teeth sugar, it is characterised in that：Step 1) in, during need The humidity of control whipping temp and environment, after cream embryo displays certain hour slightly, is transferred to and cuts on the machine of touching, and is cut according to definite shape Mould, obtains the particle with spherical, rod or bulk.

MC new product any one of 11. claim 1-8 brush teeth sugar application method, it is characterised in that：Its Application method can be expressed as：

First take during the flake products being made put oral cavity into and chew, product can bubble automatically quickly during chewing, and fragrance also discharges quickly, At this moment pick up toothbrush and dip in fraction of water, to put in start in the mouth and brush teeth, foam in discharge oral cavity, is cleaned up with clear water after a few minutes Oral cavity.