CN108148691A - A kind of preparation method of pollution-free food grade meal wash agent - Google Patents
A kind of preparation method of pollution-free food grade meal wash agent Download PDFInfo
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- CN108148691A CN108148691A CN201710720719.6A CN201710720719A CN108148691A CN 108148691 A CN108148691 A CN 108148691A CN 201710720719 A CN201710720719 A CN 201710720719A CN 108148691 A CN108148691 A CN 108148691A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/268—Carbohydrates or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/266—Esters or carbonates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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Abstract
The present invention relates to a kind of preparation method of pollution-free food grade meal wash agent, feeding grade stainless steel cauldrons；Ionized water is removed, pours into stainless steel cauldron；Hydroxymethyl cellulose is taken, pours into deionized water, obtains mixture a；Xanthans is taken to pour into mixture a, obtains mixture b；Pollution-free food grade acidity body is taken, step mixture b is instilled, obtains mixture c；Feeding salt pours into mixture c, obtains mixture d；Xylitan monostearate is taken to pour into mixture d, obtains Mischung；Cane suger is taken to pour into mixing e, obtains mixture f；Glucose is taken to pour into mixture f；Tsingtao beer is taken to pour into mixture g, obtains mixture h；Potassium sorbate is taken to pour into mixture h, obtains mixture i；Food flavor is taken to pour into mixture i to get finished product.
Description
Technical field
The present invention relates to food-grade meal wash agent technical field more particularly to a kind of preparation sides of pollution-free food grade meal wash agent
Method.
Background technology
At present, major meal wash is net, manufacturer of liquid detergent is in the net process of meal wash is prepared, it will usually use cation form
Face activating agent, nonionic surfactant, anion surfactant, as neopelex (English abbreviation SDBS),
The raw materials such as sodium sulfate of polyethenoxy ether of fatty alcohol (English abbreviation AES), addition builder (chemical synthesis).Do not have always for many years
The significant problem of infiltration rate can be effectively solved, with foods such as net, the liquid detergent washings fruits and vegetables of infiltration rate meal wash
When, pesticide residue and toxin after washing are under the action of the net infiltration rate of meal wash again washing water intoxication element with 1% aqueous solution
(net 1 gram of meal wash：99 grams of water) 8-16s speed quickly immersed inside water fruits and vegetables, secondary contamination with wash is caused to them.
Using such meal wash is net, liquid detergent brings harm to health of people in our daily lifes.Also weaken the product simultaneously
Competitiveness.And above-mentioned neopelex, it is a kind of white or faint yellow powdery or chip solid, hardly possible volatilization is soluble in
Water is dissolved in water into translucent solution, and micro- poison, its concentrated solution has skin certain stimulation, is that industrial detergent is common
Anionic surfactant has stronger penetration, once usage amount is slightly excessive, will bring injury to human body, and ten
Dialkyl benzene sulfonic acids sodium is not food grade materials, and it is incomplete to degrade, and certain pollution is caused to environment.Poly alkyl alcohol
Ethylene oxide ether sodium sulfate permeability is stronger, because its is cheap, application is the most universal, inevitably produces in process of production
The raw by-product being known：Dioxanes.Dioxanes is irritant to skin, eye and respiratory system, and may be right
Liver, kidney and nervous system damage, and when acute poisoning may lead to death, carcinogen has been listed in the U.S., less
It can be edible.Destroy balance of nature.Piece alkali (sodium hydroxide) has extremely strong corrosivity, and solution or dust are splashed on skin,
The accident in worker's glasses is especially splashed at work happen occasionally and cause lifelong disability, can generate soft scab, and can penetrate into deep
Layer tissue.For piece alkali in itself without smell, when hydrolysis, can release a large amount of heat, generate water mist, have not enough time to the piece ground caustic end of hydrolysis
It will float in air with water mist.If sucked by human body, respiratory system will be caused to damage, harm is larger.Chemistry closes
The penetration that contains into builder, benzene, lead, mercury, etc. heavy metals, the violated molecule being also harmful to containing chemical synthesis etc. it is a variety of right
The substance that human body is harmful to by fruit, residual vegetable after washing, enters water fruits and vegetables and people under the action of itself penetration
In vivo cause secondary pollution with injury.
Manufacturer is not food grade materials in the raw material that preparation more than meal wash uses only, in liquid detergent process, second is that having
Harmful industrial chemicals, damages to health, and toxic chemical synthesis residual has the chemistry for destroying human normal hormone
Substance, infiltration rate to washings, to human body, it is big to environment potential hazard, the meal wash with infiltration rate belongs to dangerous production only
Product can not be promoted the use of in the future.
Invention content
It is a primary object of the present invention to provide a kind of preparation method of pollution-free food grade meal wash agent, with ecosystem food and
Food-grade material is raw material, and the meal wash agent being prepared is environmentally safe, and people, will not be to human physiological functions once eaten by mistake
It has an impact or damages, reached a kind of edible effect of meal wash agent；Can Non-water washing, greatly saved water resource；Have
Stronger resistance to hard water as a kind of efficient, environmentally friendly, energy saving, safe and nontoxic civilian pollution-free food grade meal wash agent, can replace
For products such as the net, liquid detergents of existing meal wash；The green meal wash agent can reach food-grade, so as to be used for the life of civilian meal wash agent
Prepared by production, and the effect of the pollution-free food grade meal wash agent is net with existing meal wash, the effect of liquid detergent is suitable, even better, more
Easily promote the use of.
To achieve the above object, the technical solution taken of the present invention is：
A kind of preparation method of pollution-free food grade meal wash agent, includes the following steps：
(1) clean food-grade stainless steel reaction kettle is taken, it is spare；
(2) deionized water that parts by weight is taken to be 91.6 parts, pours into food-grade stainless steel reaction kettle, is stirred until homogeneous,
And heat, the temperature of deionized water is made to rise to 76-86 DEG C；
(3) hydroxymethyl cellulose that parts by weight is taken to be 0.18-0.2 parts, is poured into the deionized water of step (2), is stirred
To uniform, mixture a is obtained；
(4) xanthans that parts by weight is taken to be 0.3-0.4 parts, pours into the mixture a of step (3), is stirred until homogeneous, obtains
Mixture b；
(5) the pollution-free food grade acidity body that parts by weight are 0.05-0.07 parts is taken, is instilled in the mixture b of step (4),
It is stirred until homogeneous, obtains mixture c；
(6) salt that parts by weight is taken to be 0.8-1.2 parts, is poured into the mixture c of step (5), and stirring 10-20min is extremely
Uniformly, mixture d is obtained；
(7) xylitan monostearate that parts by weight is taken to be 0.3-0.4 parts, is poured into the mixture d of step (6),
25-35min is stirred to uniform, obtains Mischung；
(8) it is 2-2.6 part of cane suger to take parts by weight, is poured into the mixing e of step (7), stirs 5-15min to equal
It is even, obtain mixture f；
(9) glucose that parts by weight is taken to be 2.1-2.8 parts, is poured into the mixture f of step (8), stirs 10-20min
To uniform, mixture g is obtained；
(10) Tsingtao beer that parts by weight is taken to be 2.6-3.2 parts, pours into the mixture g of step (9), stirs to equal
It is even, obtain mixture h；
(11) potassium sorbate that parts by weight is taken to be 0.3-0.5 parts, pours into the mixture h of step (10), stirs to equal
It is even, obtain mixture i；
(12) food flavor that parts by weight is taken to be 0.05-0.1 parts, is poured into the mixture i of step (11), and stirring is extremely
Uniformly, mixture j is obtained, capping kettle, heat preservation 30min postcoolings are to room temperature to get finished product.
Food-grade stainless steel reaction kettle in step (1) uses reaction kettle of the material for Stainless steel 316 L；
Pollution-free food grade acidity body in step (5) refers to the patented product of Patent No. 201610562860.3.
The instillation time of pollution-free food grade acidity body in step (5) is 20min.
Preferably, the preparation method of a kind of pollution-free food grade meal wash agent described above, with 91.6 parts of deionized waters,
0.19 part of hydroxymethyl cellulose, 0.35 part of xanthans, 0.06 part of pollution-free food grade acidity body, 1 portion of salt, 0.35 part of xylitol
Acid anhydride monostearate, 2.3 portions of cane sugers, 2.45 parts of glucose, 2.9 portions of Tsingtao beers, 0.4 part of potassium sorbate, 0.75 part of food
It is raw material with essence.
The present invention also provides the food-grade meal wash agent prepared using the above method.
Compared with prior art, the present invention has the advantages that：Using ecosystem food and food-grade material as raw material,
The meal wash agent being prepared is environmentally safe, and people will not have an impact or damage to human physiological functions, reach once eaten by mistake
A kind of edible effect of meal wash agent is arrived；Can Non-water washing, greatly saved water resource；With stronger resistance to hard water,
As a kind of efficient, environmentally friendly, energy saving, safe and nontoxic civilian pollution-free food grade meal wash agent, alternative existing meal wash is net, it is clean to wash
The products such as essence；The green meal wash agent can reach food-grade, be prepared, and the green so as to be used for the production of civilian meal wash agent
The effect of food-grade meal wash agent is net with existing meal wash, the effect of liquid detergent is suitable, even better, it is easier to promote the use of.
Specific embodiment
To be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, with reference to
Specific embodiment, the present invention is further explained.
Embodiment 1
Using 26kg deionized waters, 4.6kg potassium hydrogen peroxymonosulfates, 16kg light-coloured vinegars and 60kg citric acids as raw material；By deionization
Water is added in reaction kettle, is opened and is stirred and be warming up to 46 DEG C, adds in potassium hydrogen peroxymonosulfate, is continuously heating to after keeping the temperature 26min
100-120 DEG C, keep the temperature 28min after be cooled to 46 DEG C, then add in light-coloured vinegar stirring 6min, add citric acid, capping kettle,
Keep the temperature 48min；Pollution-free food grade acidity body, the i.e. patented product of Patent No. 201610562860.3 can be obtained.
Embodiment 2
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg grapes
The food flavor of sugar, 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 3
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg grapes
The food flavor of sugar, 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 4
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg grapes
The food flavor of sugar, 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 5
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 6
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 7
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 8
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 9
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 10
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 11
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 12
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 13
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 14
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 15
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 16
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 17
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 18
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 19
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 20
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 21
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 22
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 23
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 24
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 25
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 26
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 27
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 28
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 29
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 30
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 31
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Embodiment 32
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Embodiment 33
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 86 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 20min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 35min is to uniform for stirring；Add in sugarcane
Sugar, 15min is to uniform for stirring, adds in glucose, and stirring 20min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Comparative example 34
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 9min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 35
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 21min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 36
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 4min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 37
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 16min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in mountain to uniform
Potassium sorbate is stirred until homogeneous, and is added in food flavor, is stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature, i.e.,
Obtain food-grade meal wash agent.
Comparative example 38
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 24min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 39
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 36min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 40
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 9min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 41
It is prepared with 91.6kg deionized waters, 0.19kg hydroxymethyl celluloses, 0.35kg xanthans, 0.06kg embodiments 1
Pollution-free food grade acidity body, 1kg salt, the xylitan monostearate of 0.35kg, 2.3kg cane sugers, 2.45kg glucose,
The food flavor of 2.9kg Tsingtao beers, 0.4kg potassium sorbates and 0.75kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 21min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 42
It is prepared with 91.5kg deionized waters, 0.17kg hydroxymethyl celluloses, 0.29kg xanthans, 0.04kg embodiments 1
Pollution-free food grade acidity body, 0.79kg salt, the xylitan monostearate of 0.29kg, 1.99kg cane sugers, 2.09kg Portugals
The food flavor of grape sugar, 2.59kg Tsingtao beers, 0.29kg potassium sorbates and 0.04kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
Comparative example 43
It is prepared with 91.7kg deionized waters, 0.21kg hydroxymethyl celluloses, 0.41kg xanthans, 0.08kg embodiments 1
Pollution-free food grade acidity body, 1.19kg salt, the xylitan monostearate of 0.41kg, 2.61kg cane sugers, 2.81kg Portugals
The food flavor of grape sugar, 3.21kg Tsingtao beers, 0.51kg potassium sorbates and 0.11kg is raw material；
Following operate is carried out under conditions of deionized water temperature is kept to be 76 DEG C：Hydroxymethyl cellulose is poured into deionization
In water, it is stirred until homogeneous；Xanthans is added in, is stirred until homogeneous；Pollution-free food grade acidity body is instilled, is stirred until homogeneous；Add in food
Salt, 10min is to uniform for stirring；Polyoxyethylene ether xylitan monostearate is added in, 25min is to uniform for stirring；Add in sugarcane
Sugar, 5min is to uniform for stirring, adds in glucose, and stirring 10min adds in Tsingtao beer, is stirred until homogeneous, add in sorb to uniform
Sour potassium, is stirred until homogeneous, add in food flavor, be stirred until homogeneous, capping kettle, heat preservation 30min postcoolings to room temperature to get
Food-grade meal wash agent.
For the properties of product of food-grade meal wash agent for probing into above-described embodiment and comparative example obtains, following test is carried out.
Experiment A takes above-described embodiment and the food-grade meal wash agent sample of comparative example preparation, is placed under room temperature, observes sample
Mode of appearance obtains experimental data and records.
Experiment B takes food-grade meal wash agent sample prepared by above-described embodiment and comparative example, be respectively placed in -5 DEG C ± 2 DEG C, 40
It 24 hours in DEG C ± 1 DEG C of refrigerator, takes out and restores to be placed at room temperature for, by hearing smell whether have peculiar smell, and seen whether layering, heavy
Shallow lake, discoloration and turbid phenomenon, obtain experimental data and record.
Experiment C takes above-described embodiment and the food-grade meal wash agent sample of comparative example preparation, passes through PH test paper determination samples PH
Value, obtains experimental data and records.
Experiment D takes above-described embodiment and the food-grade meal wash agent sample of comparative example preparation, passes through state of the People's Republic of China (PRC)
Family's standard GB/T 13173-2008 surfactant detergents test methods test the gross activity object content of sample, it obtains
Go out experimental data and record.
Experiment E takes above-described embodiment and the food-grade meal wash agent sample of comparative example preparation, and sample is measured by measuring degreasing power
The performance of product.6 pieces of glass slides with alcohol are cleaned, weighs after to be dried, is accurate to 0.0001g；Each piece of glass slide is immersed
In the greasy dirt of (20 ± 1) DEG C, until 55mm eminences, about 3s are taken out, and the greasy dirt that the attachment of glass slide lower edge is accumulated is exhausted with filter paper,
The dry 1h under the conditions of (30 ± 2) DEG C is immediately placed in glass frame, weighs, is accurate to 0.0001g；According to China's water quality situation,
With reference to detergent detergency assay method, using 250x10-6Hard water, calcium ions and magnesium ions ratio be 6:4 are prepared；Weigh anhydrous chlorine
Change calcium 0.165g, magnesium sulfate (MgSO4.7H20) 0.247g is diluted to 1L, as 250x10 with distilled water-6Hard water；It weighs
10g detergent, uses 250x10-6Hard water to be diluted to 1L for use；The greasy dirt glass slide made is carefully placed into degreasing power and measures dress
On the stent put.It takes 700ml above-described embodiments and meal wash agent solution that comparative example prepares is poured into the beaker of analyzer,
(30 ± 2) DEG C (or at room temperature) under conditions of, (agitation revolution is controlled in 250rmin washing 3min-1), visually observe beaker
Middle liquid color changes and records；Cleaning solution is poured out, distilled water 700ml is separately taken, rinses 1min under the same conditions；It takes out and carries glass
Piece is hung on stent, is dried diel at room temperature, is weighed, be accurate to 0.0001g；Take the average value of six pieces of glass slide degreasing powers
The as average degreasing power of the meal wash agent, and record.
By testing above, the experimental data integrated obtains the result as shown in table 1,2,3.
Table 1
Table 2
Table 3
It is obtained by result above, embodiment 2-33 effects are good, illustrate that food-grade meal wash agent physical and chemical properties are good；It is right
Ratio 34-43 is ineffective, illustrates that food-grade meal wash agent physical and chemical properties are poor.
Further to test the shelf-life of this product and whether being pernicious to people, Example food-grade meal wash agent sample, into
Row tests below.
Experiment one
Shelf-life tests (1 year)
According to ALST test methods, standards of grading are as follows：
All features and standard sample of 5.0 products are completely the same：
4.5 products can receive, but then have slight difference compared with standard sample：
4.0 products can receive, but then some difference compared with standard sample：
3.5 products can receive, but then have significant difference compared with standard sample：
3.0 products can neither receive, and can not say cannot receive：
2.5 products cannot somewhat receive：
2.0 products cannot a little receive：
1.5 descriptions of product cannot receive with showing：
1.0 products cannot receive completely：
Test two acute oral toxicity tests
Experimental animal：The KM small white mouses that medical experiment animal center provides, weight 200g or so；
Detection method：Small white mouse 10, half male and half female, before experiment after fasting 24 hours, property gavage 4ml samples several times,
Seeing need to observe 14 days.
Testing result：
Acute oral toxicity test
Experimental animal：The KM small white mouses that medical experiment animal center provides, weight：2008 or so.
Detection method：Small white mouse 10.Half male and half female.Before experiment after fasting for 24 hours.Property gavage 4ml samples several times, continuously
Observation 14 days.
Testing result：
Test Results
Conclusion：Institute sample LD50＞ 5000mg/kg weight, true border are nontoxic.
Claims (3)
1. a kind of preparation method of pollution-free food grade meal wash agent, which is characterized in that include the following steps：
（1）Clean food-grade stainless steel reaction kettle is taken, it is spare；
（2）The deionized water that parts by weight is taken to be 91.6 parts, pours into food-grade stainless steel reaction kettle, is stirred until homogeneous, and adds
Heat makes the temperature of deionized water rise to 76-86 DEG C；
（3）The hydroxymethyl cellulose that parts by weight is taken to be 0.18-0.2 parts, pours into step（2）Deionized water in, stir to equal
It is even, obtain mixture a；
（4）The xanthans that parts by weight is taken to be 0.3-0.4 parts, pours into step（3）Mixture a in, be stirred until homogeneous, must mix
Object b；
（5）The pollution-free food grade acidity body that parts by weight are 0.05-0.07 parts is taken, instills step（4）Mixture b in, stirring
To uniform, mixture c is obtained；
（6）The salt that parts by weight is taken to be 0.8-1.2 parts, pours into step（5）Mixture c in, 10-20min is to uniform for stirring,
Obtain mixture d；
（7）The xylitan monostearate that parts by weight is taken to be 0.3-0.4 parts, pours into step（6）Mixture d in, stirring
25-35min obtains Mischung to uniform；
（8）The cane suger that parts by weight is taken to be 2-2.6 parts, pours into step（7）Mixing e in, 5-15min is to uniform for stirring, obtains
Mixture f；
（9）The glucose that parts by weight is taken to be 2.1-2.8 parts, pours into step（8）Mixture f in, 10-20min is to equal for stirring
It is even, obtain mixture g；
（10）The Tsingtao beer that parts by weight is taken to be 2.6-3.2 parts, pours into step（9）Mixture g in, be stirred until homogeneous, obtain
Mixture h；
（11）The potassium sorbate that parts by weight is taken to be 0.3-0.5 parts, pours into step（10）Mixture h in, be stirred until homogeneous, obtain
Mixture i；
（12）The food flavor that parts by weight is taken to be 0.05-0.1 parts, pours into step（11）Mixture i in, be stirred until homogeneous,
Mixture j is obtained, capping kettle, heat preservation 30min postcoolings are to room temperature to get finished product；
The step（1）In food-grade stainless steel reaction kettle use reaction kettle of the material for Stainless steel 316 L；
The step（5）In pollution-free food grade acidity body refer to the patented product of Patent No. 201610562860.3；
The step（5）In pollution-free food grade acidity body the instillation time be 20min.
2. a kind of preparation method of pollution-free food grade meal wash agent according to claim 1, it is characterised in that：It is gone with 91.6 parts
Ionized water, 0.19 part of hydroxymethyl cellulose, 0.35 part of xanthans, 0.06 part of pollution-free food grade acidity body, 1 portion of salt, 0.35 part
Xylitan monostearate, 2.3 portions of cane sugers, 2.45 parts of glucose, 2.9 portions of Tsingtao beers, 0.4 part of potassium sorbate,
0.75 part of food flavor is raw material.
3. a kind of food-grade meal wash agent prepared by preparation method using claims 1 or 2.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115651771A (en) * | 2022-09-26 | 2023-01-31 | 南昌大学 | Preparation method of tea saponin detergent |
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| CN107164982A (en) * | 2017-07-04 | 2017-09-15 | 济宁锦祥科技发展有限公司 | A kind of textile printing and dyeing pollution-free food level detergent |
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| CN1450864A (en) * | 1999-07-27 | 2003-10-22 | 罗狄亚公司 | Hops acid antibacterial compositions |
| CN104508106A (en) * | 2012-07-27 | 2015-04-08 | 花王株式会社 | Dish detergent composition |
| CN104498207A (en) * | 2014-11-28 | 2015-04-08 | 桂林市和胤祥新型材料有限公司 | Environment-friendly sterilizing dish washing detergent |
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