CN108077997A - A kind of preparation method and applications of cigarette filter combination - Google Patents
A kind of preparation method and applications of cigarette filter combination Download PDFInfo
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- CN108077997A CN108077997A CN201711317478.7A CN201711317478A CN108077997A CN 108077997 A CN108077997 A CN 108077997A CN 201711317478 A CN201711317478 A CN 201711317478A CN 108077997 A CN108077997 A CN 108077997A
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- filter combination
- cigarette
- cigarette filter
- preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention provides a kind of preparation methods of cigarette filter combination, take tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole, it blends, it is sufficiently mixed, cellulase and pectinase enzymatic hydrolysis are added in into mixture, hydrolysis temperature is 50 ~ 60 DEG C, enzymolysis liquid is sealed by fermentation 2 ~ 5 days, fermentate decompression is filtered into obtain cigarette filter combination, gained cigarette filter combination is added in into cigarette paper, pipe tobacco, in the production technology of filter stick or tipping paper, utilize tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are as raw material, significantly reduce the CO in flue gas, nitrosamine and crotons aldehyde.
Description
Technical field
The present invention relates to technical field of cigarettes more particularly to a kind of preparation method and applications of cigarette filter combination.
Background technology
With the continuous progress of society, health is also increasingly paid attention to be subject to cigarette consumption person, and cigarette " reducing tar and reducing harm " is
As the mostly important problem of tobacco business.At present there are many technical solution of " reducing tar and reducing harm ", but suction is also reduced simultaneously
The mouthfeel of cigarette is unfavorable for promoting.
102697182 B of grant number CN disclose it is a kind of reduce cigarette smoke in ammonia additives of filter tip preparation method and
Using by the way that ferroheme to be added in the production technology of additive, having reached the content for reducing ammonia in flue gas, but gained cigarette smoking
Mouthfeel it is poor.102839565 B of grant number CN disclose reduce cigarette mainstream flue gas harmful components cigarette paper additive and
It is applied, by the processing technology that tobacco extract, tea extraction, air permeability conditioning agent and high active combustion agent are added in cigarette paper
In, realize the removal to the multiple harmful substances in cigarette, but removal effect is unsatisfactory, and cigarette smoking mouthfeel also compared with
Difference.
The content of the invention
In order to solve deficiency of the prior art, the present invention provides a kind of preparation method of cigarette filter combination and its answers
With.
The technical solution adopted by the present invention is：A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, is obtained
Mixture；
(2) cellulase and pectinase enzymatic hydrolysis are added in into mixture, hydrolysis temperature is 50~60 DEG C, obtains enzymolysis liquid；
(3) enzymolysis liquid is sealed by fermentation 2~5 days, obtains zymotic fluid；
(4) fermentate decompression is filtered into obtain cigarette filter combination.
Further, the tobacco extract is flue-cured tobacco tobacco extract.
Further, the mass ratio of the tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole
For 10:5~8:1~3:5~10:2.
Preferably, the mass ratio of the tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole is
10:7:1:9:2。
Further, the additive amount of the cellulase and pectase accounts for the 0.5% and 0.8% of mixture quality respectively.
Gained cigarette filter combination is added in cigarette paper, pipe tobacco, filter stick or connect by a kind of application of cigarette filter combination
In the production technology for filling paper.
Preferably, gained cigarette is added in by the 1~5% of filter rod quality in the forming process of filter stick with filter combination.
Compared with prior art, the beneficial effects of the invention are as follows：
(1) by the use of tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole as raw material, effectively
Reduce CO, nitrosamine and the crotons aldehyde in flue gas；
(2) select flue-cured tobacco tobacco extract that can more effectively remove the harmful components in flue gas；
(3) cellulase and pectase are used cooperatively the suction to harmful components that can further promote cigarette filter combination
It produces effects fruit；
(4) when cigarette is added in filter combination in filter stick, the best results that are reached.
Specific embodiment
The preparation method of the present invention is described in further detail with reference to embodiments.
Blank example
The harmful substance contents being measured to regular-size cigarette in its flue gas, according to YCT 497-2014 cigarette Chinese-style cigarettes
Style sensory evaluation method evaluates its flue gas taste, as a result sees Tables 1 and 2 respectively.
Embodiment 1
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:5:1:5:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.5% He of mixture quality respectively
0.8%, hydrolysis temperature is 50 DEG C, obtains enzymolysis liquid；
(3) enzymolysis liquid is sealed by fermentation 2 days, obtains zymotic fluid；
(4) fermentate decompression is filtered into obtain cigarette filter combination.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Embodiment 2
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:8:3:10:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
Step (2) (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Embodiment 3
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
Step (2) (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Reference examples 1
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is burley tobaccos tobacco extract；
Step (2) (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Reference examples 2
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta and damascenone are taken, is blended, is sufficiently mixed, mass ratio 10:7:1, mixture is obtained,
The tobacco extract is flue-cured tobacco tobacco extract；
Step (2) (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Embodiment 4
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.5% He of mixture quality respectively
0.8%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
Step (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Reference examples 3
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.2% He of mixture quality respectively
0.2%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
Step (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Reference examples 4
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 1% He of mixture quality respectively
1%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
Step (3) (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Embodiment 5
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.5% He of mixture quality respectively
0.8%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
(3) enzymolysis liquid is sealed by fermentation 5 days, obtains zymotic fluid；
Step (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
Embodiment 6
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.5% He of mixture quality respectively
0.8%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
(3) enzymolysis liquid is sealed by fermentation 4 days, obtains zymotic fluid；
Step (4) is same as Example 1.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1, its flue gas mouth is evaluated according to YCT 497-2014 cigarette Chinese-style cigarette style sensory evaluation methods
Taste the results are shown in Table 2.
Reference examples 5
A kind of preparation method of cigarette filter combination, comprises the following steps：
(1) tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, matter
Amount is than being 10:7:1:9:2, mixture is obtained, the tobacco extract is flue-cured tobacco tobacco extract；
(2) add in cellulase into mixture and pectinase enzymatic hydrolysis, additive amount account for 0.5% He of mixture quality respectively
0.8%, hydrolysis temperature is 60 DEG C, obtains enzymolysis liquid；
(3) enzymolysis liquid decompression is filtered into obtain cigarette filter combination.
Gained filter combination is added in by the 3% of filter rod quality in the forming process of filter stick, is detected in each group flue gas and is harmful to
The content of substance is as shown in table 1.
From table 1 it follows that made using tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole
For raw material, mass ratio 10:7:1:9:When 2, CO, tar, nitrosamine and crotons aldehyde in flue gas are significantly reduced；Choosing
The harmful components in flue gas can be more effectively removed with flue-cured tobacco tobacco extract, cellulase and pectase are used cooperatively can be into one
Step promotes the assimilation effect to harmful components of cigarette filter combination, and additive amount accounts for 0.5% He of mixture quality respectively
0.8%, when hydrolysis temperature is 60 DEG C, the best results that are reached；When cigarette is added in filter combination in filter stick, reached
Best results.As shown in table 2, the filter combination obtained using above-mentioned parameter adds in the sense organ matter with blank example in cigarette filter rod
Amount is close.
Embodiment 7
The cigarette filter combination of gained in embodiment 6 is added in the 1% of filter rod quality in the forming process of filter stick, inspection
The content for surveying the harmful substances from flue gases of gained cigarette is as shown in table 1.
Embodiment 8
The cigarette filter combination of gained in embodiment 6 is added in the 5% of filter rod quality in the forming process of filter stick, inspection
The content for surveying the harmful substances from flue gases of gained cigarette is as shown in table 1.
Reference examples 6
The cigarette filter combination of gained in embodiment 6 is added in the 3% of filter rod quality in the forming process of cigarette paper,
The content of the harmful substances from flue gases of detection gained cigarette is as shown in table 1.
Reference examples 7
The cigarette filter combination of gained in embodiment 6 is added in the 3% of filter rod quality in the forming process of pipe tobacco, inspection
The content for surveying the harmful substances from flue gases of gained cigarette is as shown in table 1.
Reference examples 8
The cigarette filter combination of gained in embodiment 6 is added in the 3% of filter rod quality in the forming process of tipping paper,
The content of the harmful substances from flue gases of detection gained cigarette is as shown in table 1.
Table 1
| Grouping | Nitrosamine (nmol/ branch) | CO (mg/ branch) | Crotonaldehyde (μ g/ branch) |
| Blank example | 36.6 | 12.8 | 20.7 |
| Embodiment 1 | 12.5 | 8.3 | 17.4 |
| Embodiment 2 | 11.2 | 8.0 | 15.9 |
| Embodiment 3 | 10.1 | 7.5 | 12.6 |
| Reference examples 1 | 17.6 | 10.3 | 18.9 |
| Reference examples 2 | 18.1 | 10.5 | 16.8 |
| Embodiment 4 | 9.5 | 6.2 | 10.9 |
| Reference examples 3 | 12.8 | 9.4 | 16.4 |
| Reference examples 4 | 15.7 | 11.6 | 14.5 |
| Embodiment 5 | 9.0 | 5.5 | 8.7 |
| Embodiment 6 | 8.6 | 5.1 | 8.1 |
| Reference examples 5 | 16.1 | 9.4 | 13.2 |
| Embodiment 7 | 11.8 | 8.4 | 10.2 |
| Embodiment 8 | 7.9 | 4.8 | 7.5 |
| Reference examples 6 | 13.1 | 9.6 | 9.7 |
| Reference examples 7 | 11.2 | 10.6 | 11.5 |
| Reference examples 8 | 12.0 | 9.4 | 11.3 |
As shown in Table 1 and Table 2, gained cigarette filter combination adds in the best results reached in filter stick, when filtering group
When closing object in the forming process of 5% addition filter stick of filter rod quality, the absorption of the harmful substance in cigarette smoke is slightly carried
Height, but the mouthfeel of gained cigarette is decreased obviously.
Table 2
| Grouping | Sweet taste (0~5) | Tart flavour (0~5) | Bitter taste (0~5) | Cool taste (0~5) |
| Blank example | 3.5 | 3.2 | 0 | 3.7 |
| Embodiment 6 | 3.1 | 3.8 | 0 | 4.1 |
| Embodiment 8 | 2.0 | 2.4 | 0 | 3.1 |
Above desirable embodiment according to the invention is enlightenment, and by above-mentioned description, related personnel completely can be with
Without departing from the scope of the technological thought of the present invention', various changes and amendments are carried out.The technical scope of this invention
The content being not limited on specification, it is necessary to determine the technical scope according to the scope of the claims.
Claims (7)
1. a kind of preparation method of cigarette filter combination, which is characterized in that comprise the following steps：
（1）Tobacco extract, eclipta, damascenone, wild chrysanthemum and butylated hydroxy anisole are taken, is blended, is sufficiently mixed, must be mixed
Object；
（2）Cellulase and pectinase enzymatic hydrolysis are added in into mixture, hydrolysis temperature is 50 ~ 60 DEG C, obtains enzymolysis liquid；
（3）Enzymolysis liquid is sealed by fermentation 2 ~ 5 days, obtains zymotic fluid；
（4）Fermentate decompression is filtered into obtain cigarette filter combination.
A kind of 2. preparation method of cigarette filter combination according to claim 1, which is characterized in that the tobacco extraction
Object is flue-cured tobacco tobacco extract.
A kind of 3. preparation method of cigarette filter combination according to claim 1, which is characterized in that the tobacco extraction
Object, eclipta, damascenone, the mass ratio of wild chrysanthemum and butylated hydroxy anisole are 10:5~8:1~3:5~10:2.
A kind of 4. preparation method of cigarette filter combination according to claim 1 or 3, which is characterized in that the tobacco
Extract, eclipta, damascenone, the mass ratio of wild chrysanthemum and butylated hydroxy anisole are 10:7:1:9:2.
A kind of 5. preparation method of cigarette filter combination according to claim 1, which is characterized in that the cellulase
Account for the 0.5% and 0.8% of mixture quality respectively with the additive amount of pectase.
6. gained cigarette filter combination is added in cigarette paper, pipe tobacco, filter stick or tipping by a kind of application of cigarette filter combination
In the production technology of paper.
7. the application of a kind of cigarette filter combination according to claim 6, which is characterized in that by gained cigarette filtering group
Object is closed to add in the forming process of filter stick by the 1 ~ 5% of filter rod quality.
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