CN107929543A - A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof - Google Patents
A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof Download PDFInfo
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- CN107929543A CN107929543A CN201711271881.0A CN201711271881A CN107929543A CN 107929543 A CN107929543 A CN 107929543A CN 201711271881 A CN201711271881 A CN 201711271881A CN 107929543 A CN107929543 A CN 107929543A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses a kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, 10~20 parts of the roxburgh anoectochilus terminal bud fresh goods of coming will be picked, after being cleaned using clear water, drying technique is dehydrated, it is made by extraction, evaporative filtration, centrifugal concentrating, the dry multiple steps of powder by spraying, it not only at utmost remains the nutritive value of roxburgh anoectochilus terminal bud（14 kinds of trace elements and 16 kinds of amino acid）, the application range of roxburgh anoectochilus terminal bud is also improved, it is used more convenient, increase eating mouth feel etc..
Description
Technical field
The present invention relates to plant extraction method and technology field, in particular to a kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof.
Background technology
Roxburgh anoectochilus terminal bud alias Shorthairy Antenoron, rough melic herb, be orchid family Anoectochilus Blume wild rare medicinal plant, be known as " king of medicine ", "
The laudatory titles such as golden herbal medicine ", " god's medicine ".According to《Fujian medicine will》Record, roxburgh anoectochilus terminal bud characteristic is sweet, flat；Return lung, liver, kidney, bladder warp
；Clearing heat and cooling blood, expelling wind and removing dampness, for ephritis, cystitis, diabetes, bronchus, rheumatic arthritis, acute infantile convulsion
Deng.Roxburgh anoectochilus terminal bud is extracted, is concentrated, is filtered, spray after be made pulvis, product save to greatest extent roxburgh anoectochilus terminal bud it is effective into
Part, water can be instantly dissolved in and be adapted to various people to take.
Modern roxburgh anoectochilus terminal bud is widely used in the diseases such as hepatitis, ephritis, cystitis, diabetes, bronchitis, rheumatic arthritis
Disease treatment.Roxburgh anoectochilus terminal bud is Fujian platform characteristic Chinese herbal medicine, the title among the people for being known as " king of medicine ".Roxburgh anoectochilus terminal bud：The generating source of Chinese medicinal granular formulation
In traditional Chinese herbal decoction, a kind of product that the prepared slices of Chinese crude drugs are reformed in recent years is come from.Granule had both maintained decoction and has absorbed very fast, work
With it is rapid the advantages of, and overcome decoction and face that the used time decocts inconvenience, dose is big, the shortcomings of easily going mouldy.It is adapted to industrialized production,
And product quality is stablized.
In the market is in the majority with dry jewel orchid and roxburgh anoectochilus terminal bud tea on the product of roxburgh anoectochilus terminal bud, by way of stewing or steeping drink
Drink, inconvenient to carry, and there are particle residue thing after brewing, mouthfeel is drunk in influence, contained peculiar element retention rate compared with
It is low, it is not easy to absorb.
The content of the invention
The purpose of the present invention is exactly to solve the above-mentioned problems, there is provided a kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, its
Have the characteristics that to be convenient for carrying, quick brewing, low particle residue thing, nutritive value it is high.
The present invention is in order to achieve the above object, using following scheme：
A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, using roxburgh anoectochilus terminal bud fresh goods as raw material, comprises the following steps that：
（1）Drying：10 ~ 20 parts next of roxburgh anoectochilus terminal bud fresh goods of picking is put into clear water and is cleaned, vacant 5 on strainer ~ after ten minutes,
It is put into drying baker, 70 ~ 90 DEG C of temperature, when drying 2 ~ 3 is small；
（2）Extraction：10 ~ 20 parts of dry jewel orchid after drying is directly placed into back taper extractor, 150~300 parts of addition is pure
Water, using vapour cooking, vapor (steam) temperature is 110~120 DEG C, and vapor pressure is 0.15~0.25MPa, and digestion time is small for 1~2
When, stand after ten minutes, start second of boiling, vapor (steam) temperature, air pressure are constant, the time shorten to 0.5 ~ 1 it is small when；
（3）Evaporative filtration：By step（2）About 3 cubic metres of the extracting solution of acquisition flows into extraction liquid storage tank, then will extract in liquid storage tank
Extracting solution insert external circulation evaporator, heating and temperature control at 60 ~ 70 DEG C, continue 1.5-2.5 it is small when, obtain concentrated extract；
Concentrated extract is finally imported into 2 cubic metres of concentration liquid storage tanks；
（4）Centrifugal concentrating：By concentrated extract by 1100L/h flow speeds import horizontal centrifugal thin film evaporator in, temperature 40 ~
60 DEG C, under the conditions of 0.2 ~ 0.25MPa of pressure, when centrifugal operation 2.5 ~ 3 is small；
（5）Dry powder by spraying：By step（4）The concentrated extract of acquisition, using special spray dryer, in tower pressure-
140MPa or so, 230 DEG C of inlet air temperature, 96 ~ 98 DEG C of leaving air temp, 90 DEG C of humidity, atomizer operating rate 15-20Hz/h or so
Under the conditions of be made roxburgh anoectochilus terminal bud concentration powder.
Preferably, in the leach step, will clean, it is vacant after 10 ~ 20 parts of roxburgh anoectochilus terminal bud fresh goods be directly placed into back taper and carry
Take tank, add 150~300 parts of pure water, using vapour cooking, vapor (steam) temperature is 110~120 DEG C, vapor pressure for 0.15~
0.25MPa, when digestion time is 1~2 small, stands after ten minutes, starts second of boiling, vapor (steam) temperature, air pressure are constant, the time
Shorten to 0.5 ~ 1 it is small when.
Preferably, in the leach step, 10 parts of dry jewel orchid after drying is directly placed into back taper extractor, is added
150 parts of pure water, using vapour cooking, vapor (steam) temperature is 120 DEG C, vapor pressure 0.2MPa, quiet when digestion time is 1 small
Put after ten minutes, start second of boiling, vapor (steam) temperature, air pressure are constant, the time shorten to 0.5 it is small when.
Preferably, in the leach step, 20 parts of dry jewel orchid after drying is directly placed into back taper extractor, is added
300 parts of pure water, using vapour cooking, vapor (steam) temperature is 130 DEG C, vapor pressure 0.25MPa, quiet when digestion time is 2 small
Put after ten minutes, start second of boiling, vapor (steam) temperature, air pressure are constant, the time shorten to 1 it is small when.
Preferably, in the milling step, in 96 DEG C of temperature, pressure 10MPa, the roxburgh anoectochilus terminal bud concentration powder of making is optimal.
The beneficial effects of the invention are as follows：
1st, a kind of roxburgh anoectochilus terminal bud concentration powder that can directly take after mixing it with water is provided, use, carrying are more convenient.
2nd, higher purity, nutritive value higher are maintained（It is peculiar rich in 14 kinds of trace elements and 16 kinds through authority's detection
Amino acid）.
3rd, it is green safe nuisanceless without any additive, trust edible.
Embodiment
With reference to the embodiment of the present invention, to further illustrate technical scheme.
Embodiment 1：
A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, using roxburgh anoectochilus terminal bud fresh goods as raw material, comprises the following steps that：
（1）Drying：By pick come 10 parts of roxburgh anoectochilus terminal bud fresh goods be put into clear water clean, on strainer it is vacant after five minutes, be put into baking
Dry case, temperature 70 C, when drying 3.5 is small；
（2）Extraction：10 parts of dry jewel orchid after drying is directly placed into back taper extractor, 150 parts of pure water is added, uses steaming
Steam cooker, vapor (steam) temperature are 120 DEG C, vapor pressure 0.25MPa, digestion time for 2 it is small when, stand after ten minutes, start the
Secondary boiled, vapor (steam) temperature, air pressure are constant, the time shorten to 0.5 it is small when；
（3）Evaporative filtration：By step（2）The extracting solution of acquisition is put into extraction liquid storage tank, will be evacuated in tank body, at normal temperatures
Stand 0.5 it is small when, then by extract liquid storage tank in extracting solution insert external circulation evaporator, heating and temperature control at 60 DEG C, continue
0.5 it is small when, obtain concentrated extract；
（4）Centrifugal concentrating：By in concentrated extract centrifugal-film evaporator, under the conditions of 40 DEG C of temperature, pressure 0.25MPa, centrifuge
When operation 2 is small；
（5）Powder processed：By step（4）The concentrated extract of acquisition, using special spray dryer, in 98 DEG C of temperature, pressure 9.6MPa
Under the conditions of, roxburgh anoectochilus terminal bud concentration powder is made.
Embodiment 2：
A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, using roxburgh anoectochilus terminal bud fresh goods as raw material, comprises the following steps that：
（1）Drying：By pick come 20 parts of roxburgh anoectochilus terminal bud fresh goods be put into clear water clean, on strainer it is vacant after ten minutes, be put into
Drying baker, temperature 70 C, when drying 4 is small；
（2）Extraction：20 parts of dry jewel orchid after drying is directly placed into back taper extractor, 300 parts of pure water is added, uses steaming
Steam cooker, vapor (steam) temperature are 120 DEG C, vapor pressure 0.25MPa, digestion time for 2 it is small when, stand after ten minutes, start the
Secondary boiled, vapor (steam) temperature, air pressure are constant, the time shorten to 1 it is small when；
（3）Evaporative filtration：By step（2）The extracting solution of acquisition is put into extraction liquid storage tank, will be evacuated in tank body, at normal temperatures
Stand 1 it is small when, then the extracting solution extracted in liquid storage tank is inserted into external circulation evaporator, 70 DEG C of heating-up temperature, continue 1 it is small when, obtain
To concentrated extract；
（4）Centrifugal concentrating：By in concentrated extract centrifugal-film evaporator, under the conditions of 100 DEG C of temperature, pressure 0.15MPa, centrifuge
When operation 1 is small；
（5）Powder processed：By step（4）The concentrated extract of acquisition, using special spray dryer, in 98 DEG C of temperature, pressure 9.6MPa
Under the conditions of, roxburgh anoectochilus terminal bud concentration powder is made.
Embodiment 3：
A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, using roxburgh anoectochilus terminal bud fresh goods as raw material, comprises the following steps that：
（1）Extraction：By pick come 20 parts of roxburgh anoectochilus terminal bud fresh goods be put into clear water clean, on strainer it is vacant after ten minutes, directly
Back taper extractor is put into, adds 300 parts of pure water, using vapour cooking, vapor (steam) temperature is 130 DEG C, and vapor pressure is
0.25MPa, when digestion time is 2 small, stands after ten minutes, starts second of boiling, and vapor (steam) temperature, air pressure are constant, time contracting
It is short when being 1 small；
（2）Evaporative filtration：By step（1）The extracting solution of acquisition is put into extraction liquid storage tank, will be evacuated in tank body, at normal temperatures
Stand 1 it is small when, then the extracting solution extracted in liquid storage tank is inserted into external circulation evaporator, 70 DEG C of heating-up temperature, continue 1.5 it is small when,
Obtain concentrated extract；
（3）Centrifugal concentrating：By in concentrated extract centrifugal-film evaporator, under the conditions of temperature 60 C, pressure 0.25MPa, centrifuge
When operation 4 is small；
（4）Powder processed：By step（3）The concentrated extract of acquisition, using special spray dryer, in 98 DEG C of temperature, pressure 9.8MPa
Under the conditions of, roxburgh anoectochilus terminal bud concentration powder is made.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understand on the basis of the principle of the present invention and spirit is not departed from, these embodiments can be carried out with a variety of changes, modification, replaced
And modification, without departure from protection scope of the present invention, limited by the claim and its equivalent.
Claims (5)
- A kind of 1. roxburgh anoectochilus terminal bud concentration powder and preparation method thereof, using roxburgh anoectochilus terminal bud fresh goods as raw material, it is characterised in that including following system Make step：Drying：10 ~ 20 parts next of roxburgh anoectochilus terminal bud fresh goods of picking is put into clear water and is cleaned, vacant 5 on strainer ~ after ten minutes, put Enter drying baker, 70 ~ 90 DEG C of temperature, when drying 2 ~ 3 is small；Extraction：10 ~ 20 parts of dry jewel orchid after drying is directly placed into back taper extractor, adds 150~300 parts of pure water, Using vapour cooking, vapor (steam) temperature is 110~120 DEG C, and vapor pressure is 0.15~0.25MPa, when digestion time is 1~2 small, Stand after ten minutes, start second of boiling, vapor (steam) temperature, air pressure are constant, the time shorten to 0.5 ~ 1 it is small when；Evaporative filtration：By step（2）About 3 cubic metres of the extracting solution of acquisition flows into extraction liquid storage tank, then by extraction liquid storage tank Extracting solution inserts external circulation evaporator, and heating and temperature control when persistently 1.5-2.5 is small, obtains concentrated extract at 60 ~ 70 DEG C；Most Concentrated extract is imported into 2 cubic metres of concentration liquid storage tanks afterwards；Centrifugal concentrating：Concentrated extract is imported in horizontal centrifugal thin film evaporator by 1100L/h flow speeds, in temperature 40 ~ 60 DEG C, under the conditions of 0.2 ~ 0.25MPa of pressure, when centrifugal operation 2.5 ~ 3 is small；Dry powder by spraying：By step（4）Concentrated extract after processing, using special spray dryer, in tower pressure- 140Pa or so, 230 DEG C of inlet air temperature, 96 ~ 98 DEG C of leaving air temp, relative humidity 90%, atomizer operating rate 15-20Hz/h are left Roxburgh anoectochilus terminal bud concentration powder is made under the conditions of the right side.
- 2. roxburgh anoectochilus terminal bud concentration powder according to claim 1 and preparation method thereof, it is characterised in that in the leach step, 10 ~ 20 parts of roxburgh anoectochilus terminal bud fresh goods after will be clean, vacant is directly placed into back taper extractor, adds 150~300 parts of pure water, uses Vapour cooking, vapor (steam) temperature are 110~120 DEG C, and vapor pressure is 0.15~0.25MPa, when digestion time is 1~2 small, is stood After ten minutes, start second of boiling, vapor (steam) temperature, air pressure are constant, the time shorten to 0.5 ~ 1 it is small when.
- 3. roxburgh anoectochilus terminal bud concentration powder according to claim 1 and preparation method thereof, it is characterised in that in the leach step, 10 parts of dry jewel orchid after drying is directly placed into back taper extractor, 150 parts of pure water is added, uses vapour cooking, steam Temperature is 120 DEG C, vapor pressure 0.25MPa, when digestion time is 1 small, stands after ten minutes, starts second of boiling, steam Stripping temperature, air pressure are constant, the time shorten to 0.5 it is small when.
- 4. roxburgh anoectochilus terminal bud concentration powder according to claim 1 and preparation method thereof, it is characterised in that in the leach step, 20 parts of dry jewel orchid after drying is directly placed into back taper extractor, 300 parts of pure water is added, uses vapour cooking, steam Temperature is 130 DEG C, vapor pressure 0.25MPa, when digestion time is 2 small, stands after ten minutes, starts second of boiling, steam Stripping temperature, air pressure are constant, the time shorten to 1 it is small when.
- 5. roxburgh anoectochilus terminal bud concentration powder according to claim 1 and preparation method thereof, it is characterised in that in the milling step, In 96 DEG C of temperature, pressure 10MPa, the roxburgh anoectochilus terminal bud concentration powder of making is optimal.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711271881.0A CN107929543A (en) | 2017-12-06 | 2017-12-06 | A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711271881.0A CN107929543A (en) | 2017-12-06 | 2017-12-06 | A kind of roxburgh anoectochilus terminal bud concentration powder and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112618658A (en) * | 2020-12-29 | 2021-04-09 | 联和东浩(厦门)药业有限公司 | Processing method of traditional Chinese medicine decoction pieces containing anoectochilus formosanus |
| CN112841651A (en) * | 2021-01-26 | 2021-05-28 | 刘育娟 | Concentrated powder of anoectochilus roxburghii |
Citations (4)
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|---|---|---|---|---|
| JPH06293655A (en) * | 1993-04-02 | 1994-10-21 | Nippon Mektron Ltd | Hypolipidemic agent and hypoglycemic agent |
| CN104146127A (en) * | 2014-08-26 | 2014-11-19 | 哈尔滨灵丹鸿运茶品有限公司 | Roxburgh anoectochilus herb heat clearing and blood cooling tea and production method thereof |
| CN105106653A (en) * | 2015-09-22 | 2015-12-02 | 福建金草生物集团股份有限公司 | Preparation method of anoectochilus roxburghii granules |
| CN106474324A (en) * | 2016-10-21 | 2017-03-08 | 代立新 | A kind of Chinese medicine instant tea preparation technology |
-
2017
- 2017-12-06 CN CN201711271881.0A patent/CN107929543A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06293655A (en) * | 1993-04-02 | 1994-10-21 | Nippon Mektron Ltd | Hypolipidemic agent and hypoglycemic agent |
| CN104146127A (en) * | 2014-08-26 | 2014-11-19 | 哈尔滨灵丹鸿运茶品有限公司 | Roxburgh anoectochilus herb heat clearing and blood cooling tea and production method thereof |
| CN105106653A (en) * | 2015-09-22 | 2015-12-02 | 福建金草生物集团股份有限公司 | Preparation method of anoectochilus roxburghii granules |
| CN106474324A (en) * | 2016-10-21 | 2017-03-08 | 代立新 | A kind of Chinese medicine instant tea preparation technology |
Non-Patent Citations (2)
| Title |
|---|
| 刘修明: "《茶与茶文化基础知识》", 31 January 2004, 中国劳动社会保障出版社 * |
| 张以忠等: "金线莲研究的现状与展望", 《贵州科学》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112618658A (en) * | 2020-12-29 | 2021-04-09 | 联和东浩(厦门)药业有限公司 | Processing method of traditional Chinese medicine decoction pieces containing anoectochilus formosanus |
| CN112841651A (en) * | 2021-01-26 | 2021-05-28 | 刘育娟 | Concentrated powder of anoectochilus roxburghii |
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