CN107540217A - A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze - Google Patents
A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze Download PDFInfo
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- CN107540217A CN107540217A CN201710919919.4A CN201710919919A CN107540217A CN 107540217 A CN107540217 A CN 107540217A CN 201710919919 A CN201710919919 A CN 201710919919A CN 107540217 A CN107540217 A CN 107540217A
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Abstract
The invention discloses a kind of sepia crystalline glaze material, it is characterised in that：Described sepia crystalline glaze material each component is formed according to following quality proportioning：20~30 parts of potassium feldspar, 5~10 parts of calcite, 2~8 parts of zinc oxide, 2~6 parts of kaolin, 1~4 part of aluminum oxide, 1~5 part of nickel oxide.The invention also discloses a kind of method that sepia crystalline glaze is fired using the sepia crystalline glaze material：By the sepia crystalline glaze material and water according to mass ratio 100：70~80 mixing, sink-float, sieve (100~200 mesh), obtain mixed liquor；The ceramic body of biscuiting is immersed into gained mixed liquor, taken out after 2~3s, electrical kiln is fired 12 hours, cooling, obtains the ceramic for having sepia crystalline glaze to surface.The present invention can obtain the sepia ceramic with sepia crystallization effect, and exquisite attractive in appearance, artistic effect is strong；Formula is simple, and easy to operate, cost is low；Glaze superposition can obtain more special artistic effect porcelain.
Description
(1) technical field
The present invention relates to a kind of sepia crystalline glaze material, and the method using this glaze firing sepia crystalline glaze.
(2) background technology
Coloring, glazing are a kind of effective means for increasing ceramic texture and aesthetic feeling on the surface of ceramic, and
And the artistic effect that each glaze colours or pattern rise is different, have in the market various glaze colours, pattern or
Its combination of person.In the market glaze various types, but strong seldom of artistic effect.
(3) content of the invention
It is an object of the present invention to provide a kind of art effect is strong, glaze effect stability, the obvious glaze of decorative effect can profit
The special artistic effect of sepia crystallization caused by the oxidation firing of matt glaze is created with it.
The technical solution adopted by the present invention is：
A kind of sepia crystalline glaze material, described sepia crystalline glaze material each component are formed according to following quality proportioning：Potassium
20~30 parts of feldspar, 5~10 parts of calcite, 2~8 parts of zinc oxide, 2~6 parts of kaolin, 1~4 part of aluminum oxide, nickel oxide 1~5
Part.
Further, it is preferred that described sepia crystalline glaze material each component is formed according to following quality proportioning：Potassium feldspar
24.98 parts, 5.99 parts of calcite, 3.64 parts of zinc oxide, 3.86 parts of kaolin, 1.53 parts of aluminum oxide, 2.00 parts of nickel oxide.
Further, the invention further relates to a kind of side that sepia crystalline glaze is fired using the sepia crystalline glaze material
Method, methods described include：
(1) weighed according to amounts of components described in claim 1 and sepia crystalline glaze material is prepared；
(2) by the sepia crystalline glaze material and water according to mass ratio 100：70~80 mixing, sink-float, sieving (100~
200 mesh), obtain mixed liquor；
(3) ceramic body of biscuiting being immersed into gained mixed liquor, taken out after 2~3s, electrical kiln is fired 12 hours, cooling,
Surface, which must be arrived, the ceramic of sepia crystalline glaze.
Preferably, it is as follows to fire program for the electrical kiln：
First stage：150 DEG C are warming up to from 20 DEG C, time 150min；
Second stage：300 DEG C are warming up to from 150 DEG C, time 100min；
Phase III：800 DEG C are warming up to from 300 DEG C, time 200min；
Fourth stage：1240 DEG C are warming up to from 800 DEG C, time 240min；
5th stage：1250 DEG C are warming up to from 1240 DEG C, time 20min；
6th stage：1250 DEG C are incubated 10 minutes.
To reach specific artistic effect, can by the first first-class layer of transparent glaze of ceramic body, then locally coat it is brown
Color crystalline glaze material, after 1250 DEG C of electrical kiln is fired 12 hours, the special-effect that sepia slightly has pale white crystals can be obtained
Sepia crystalline glaze.
Compared with prior art, the beneficial effects are mainly as follows：
The sepia ceramic with sepia crystallization effect can be obtained, exquisite attractive in appearance, artistic effect is strong；Formula
Simply, easy to operate, cost is low；Glaze superposition can obtain more special artistic effect porcelain.
(4) embodiment
With reference to specific embodiment, the present invention is described further, but protection scope of the present invention is not limited in
This：
Embodiment 1：
A kind of sepia crystalline glaze material, each component are formed according to following quality proportioning：The mass parts of potassium feldspar 24.98, Fang Xie
The mass parts of stone 5.99, the mass parts of zinc oxide 3.64, the mass parts of kaolin 3.86, the mass parts of aluminum oxide 1.53, the matter of nickel oxide 2.00
Amount part mixes.
Method for cooking：By above-mentioned sepia crystalline glaze and water according to mass ratio 100：75 mixing, sink-float, cross 120 mesh sieves, obtain
Mixed liquor, the base substrate of biscuiting is immersed into gained mixed liquor, taken out after 2~3s, is fired 12 hours for 1250 DEG C in electrical kiln, cooling,
Obtain the ceramic of the strong sepia crystallization effect of artistic feeling.
Firing temperature curve：
Electrical kiln is burnt till：Base substrate is put into kiln, the first stage burnt 150 DEG C from 20 DEG C by 150 minutes, removed in base substrate
Moisture；Second stage burnt 300 DEG C from 150 DEG C by 100 minutes, and moisture eliminates；Phase III passes through 200 points from 300 DEG C
Clock burns 800 DEG C, makes base substrate stable；Fourth stage burnt 1240 DEG C from 800 DEG C by 240 minutes, glaze is fully melted；The
Five stages burnt 1250 DEG C from 1240 DEG C by 20 minutes, were incubated 10 minutes, glaze crystallization is fully completed.Then drop naturally
Temperature, when 100 degree can be with kiln discharge.
Embodiment 2：
A kind of sepia crystalline glaze material, each component are formed according to following quality proportioning：The mass parts of potassium feldspar 24.98, Fang Xie
The mass parts of stone 5.99, the mass parts of zinc oxide 3.64, the mass parts of kaolin 3.86, the mass parts of aluminum oxide 1.53, the mass of nickel oxide 0.5
Part mixes.
Method for cooking is same as Example 1 with sintering curve.
Due to nickel oxide in glaze for, addition less than 1% almost all be melted in glass phase, will not be analysed in glaze paint
Go out crystallization, and only granular nickel oxide just easily forms spot crystallization effect.So in the glaze of embodiment 2 not
The glazing effect that sepia crystallizes into embodiment 1, simply obtain the glazing effect of independent sepia.
Embodiment 3：
A kind of sepia crystalline glaze material, each component are formed according to following quality proportioning：The mass parts of potassium feldspar 24.98, Fang Xie
The mass parts of stone 5.99, the mass parts of zinc oxide 7, the mass parts of kaolin 3.86, the mass parts of aluminum oxide 1.53, the mass parts of nickel oxide 2.00
Mix.
Method for cooking is same as Example 1 with sintering curve.
The amount of the zinc oxide of embodiment 3 is one times of embodiment 1, and obtained glazing effect is the partially blue glaze colours of brown, due to
Nickel oxide can send blue seawater green in the glaze of high zinc, thus it is few in amount, palm fibre is inclined in the lime glaze under the atmosphere of oxidation
Brown.
Embodiment 4：
A kind of sepia crystalline glaze material, each component are formed according to following quality proportioning：The mass parts of potassium feldspar 24.98, Fang Xie
The mass parts of stone 5.99, the mass parts of zinc oxide 3.64, the mass parts of kaolin 3.86, the mass parts of aluminum oxide 4.00, the matter of nickel oxide 2.00
Amount part mixes.
Method for cooking is same as Example 1 with sintering curve.
Due to helping color development in the glaze containing aluminum oxide and zinc oxide, fusion range is increased, in alumina content increase
To after 4.00 mass parts, mobility is substantially died down, and the sepia glaze paint of semi-molten is produced in embodiment 4.
Claims (4)
- A kind of 1. sepia crystalline glaze material, it is characterised in that：Described sepia crystalline glaze material each component is matched somebody with somebody according to following quality Than forming：20~30 parts of potassium feldspar, 5~10 parts of calcite, 2~8 parts of zinc oxide, 2~6 parts of kaolin, 1~4 part of aluminum oxide, oxygen Change 1~5 part of nickel.
- 2. sepia crystalline glaze material as claimed in claim 1, it is characterised in that：Described sepia crystalline glaze material each component is pressed Formed according to following quality proportioning：24.98 parts of potassium feldspar, 5.99 parts of calcite, 3.64 parts of zinc oxide, 3.86 parts of kaolin, oxidation 1.53 parts of aluminium, 2.00 parts of nickel oxide.
- 3. a kind of method that sepia crystalline glaze material as claimed in claim 1 or 2 fires sepia crystalline glaze, its feature exist In：Methods described is carried out in accordance with the following steps：(1) weighed according to amounts of components described in claim 1 and sepia crystalline glaze material is prepared；(2) by the sepia crystalline glaze material and water according to mass ratio 100：70~80 mixing, rise and fall, and sieving, obtain mixed liquor；(3) ceramic body of biscuiting is immersed into gained mixed liquor, taken out after 2~3s, electrical kiln is fired 12 hours, cooling, is obtained There is the ceramic of sepia crystalline glaze on surface.
- 4. method as claimed in claim 3, it is characterised in that it is as follows that the electrical kiln fires program：First stage：150 DEG C are warming up to from 20 DEG C, time 150min；Second stage：300 DEG C are warming up to from 150 DEG C, time 100min；Phase III：800 DEG C are warming up to from 300 DEG C, time 200min；Fourth stage：1240 DEG C are warming up to from 800 DEG C, time 240min；5th stage：1250 DEG C are warming up to from 1240 DEG C, time 20min；6th stage：1250 DEG C are incubated 10 minutes.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710919919.4A CN107540217A (en) | 2017-09-30 | 2017-09-30 | A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze |
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| CN201710919919.4A CN107540217A (en) | 2017-09-30 | 2017-09-30 | A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173869A (en) * | 2011-01-19 | 2011-09-07 | 江苏高淳陶瓷股份有限公司 | Preparation method of non-ferrous tea dust crystalline glaze |
| CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
-
2017
- 2017-09-30 CN CN201710919919.4A patent/CN107540217A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102173869A (en) * | 2011-01-19 | 2011-09-07 | 江苏高淳陶瓷股份有限公司 | Preparation method of non-ferrous tea dust crystalline glaze |
| CN103304274A (en) * | 2013-06-08 | 2013-09-18 | 浙江工业大学之江学院工业研究院 | Bronze green crystalline glaze and firing method thereof |
Non-Patent Citations (3)
| Title |
|---|
| （美）泰勒: "《釉 釉料及陶瓷颜色配制手册》", 30 November 2015, 上海科学技术出版社 * |
| 杨保祥: "《钛基材料制造》", 31 January 2015, 冶金工业出版社 * |
| 王超: "《陶瓷装饰技术》", 31 October 2013, 中国轻工业出版社 * |
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Application publication date: 20180105 |