CN103304274A - Bronze green crystalline glaze and firing method thereof - Google Patents
Bronze green crystalline glaze and firing method thereof Download PDFInfo
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- CN103304274A CN103304274A CN2013102324994A CN201310232499A CN103304274A CN 103304274 A CN103304274 A CN 103304274A CN 2013102324994 A CN2013102324994 A CN 2013102324994A CN 201310232499 A CN201310232499 A CN 201310232499A CN 103304274 A CN103304274 A CN 103304274A
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Abstract
The invention provides a bronze green crystalline glaze which is prepared from the following raw materials in parts by weight: 20-25 parts of potash feldspar, 8-10 parts of calcite, 2-5 parts of kaolin, 4-8 parts of aluminium oxide, 1-5 parts of basic cupric carbonate and 0.5-2 parts of titanium dioxide. The bronze green crystalline glaze has the beneficial effects that a bronze green porcelain product with a strong and rich artistic effect can be obtained according to the formula of the glaze and the firing method provided by the invention, the bronze green porcelain product is exquisite and beautiful, the formula is simple, the operation is convenient and the cost is low.
Description
(1) technical field
The present invention relates to a kind of bronze green crystal glaze, and use this glaze to fire the method for bronze green crystal glaze.
(2) background technology
Painted on the surface of ceramic, glazing is a kind of effective means that increases ceramic texture and aesthetic feeling, and the artistic effect that each glaze colours or pattern rose is different, various glaze colours, pattern or its combination are arranged in the market, and this mainly is to develop according to the demand in market.Have a kind of Gu that returns to return very on the Vehicles Collected from Market, pursue the general mood of nature, many things are particular about is a kind of simpleness, generous artistic effect.Naturally no exception for ceramic industry.Verdigris color can be given a kind of time immemorial of people, long, generous, simple sensation, if its pattern is made on the surface of ceramic utensil by the form of muffle painting, be to make the human consumer feel to have the dense Gu Zhiwei that returns, but in retrieval, find no this type of bibliographical information.
(3) summary of the invention
The object of the invention provides a kind of bronze green crystal glaze and method for cooking thereof with strong simple and honest artistic effect.
The technical solution used in the present invention is:
A kind of bronze green crystal glaze, its raw material mass mixture ratio is as follows; 20～25 parts of potassium felspar sands, 8～10 parts in calcite, 2～5 parts of kaolin, 4～8 parts of aluminium sesquioxides, 1～5 part of ventilation breather, 0.5～2 part of titanium dioxide.
Preferably, its raw material mass mixture ratio is as follows: 21.99 parts of potassium felspar sands, 9.23 parts in calcite, 3.40 parts of kaolin, 5.38 parts of aluminium sesquioxides, 2.00 parts of ventilation breathers, 1.4 parts of titanium dioxide.
The invention still further relates to a kind of method of using described glaze to fire bronze green crystal glaze, described method comprises: described glaze is mixed according to mass ratio 100:70～80 with water, and sink-float, sieve (100～300 order) gets glaze slip; Transferring glaze slip proportion is 1.51, glazes on the ceramic body, and electrical kiln is fired, and cooling obtains the ceramic that there is bronze green crystal glaze on the surface.
Preferably, to fire program as follows for described electrical kiln:
Fs: be warmed up to 150 ℃, time 150min from 20 ℃;
Subordinate phase: be warmed up to 300 ℃, time 100min from 150 ℃;
Phase III: be warmed up to 800 ℃, time 200min from 300 ℃;
Quadravalence section: be warmed up to 1240 ℃, time 240min from 800 ℃;
Five-stage: be warmed up to 1250 ℃, time 20min from 1240 ℃;
The 6th stage: 1250 ℃ are incubated 10 minutes.
Beneficial effect of the present invention is mainly reflected in: according to glaze formula of the present invention and method for cooking, can access the bronze green ceramic products with strong simple and honest artistic effect, and exquisite attractive in appearance; Prescription is simple, and easy to operate, cost is low.
(4) embodiment
The present invention is described further below in conjunction with specific embodiment, but protection scope of the present invention is not limited in this:
Embodiment 1:
Glaze quality prescription: 21.99 parts of potassium felspar sands, 9.23 parts in calcite, 3.40 parts of kaolin, 5.38 parts of aluminium sesquioxides, 2.00 parts of ventilation breathers, 1.4 parts of titanium dioxide mix.
Method for cooking: after above-mentioned batching is mixed, mass ratio according to glaze, porcelain ball milling ball, water is 1: 2.5: 0.8, about ball milling 50 hours, then glaze slip to cross the aperture be Φ 0.061mm(250 order) sieve, tailing over 0.02%～0.06%, can to change drainer over to for subsequent use.Glazing; Be Φ 0.154mm(100 order with the aperture again before the glazing) sieve filter, in sieve, put into the suction iron staff, glaze first through inhaling the iron staff deironing through the filtration of sifting out, elimination body refuse and impurity, it is 1.51 that glaze slip transfers to proportion, clean the dust on ceramic body surface before the glazing with clear water, the glaze layer thickness is 0.8mm.
Electrical kiln burns till: base substrate is put into kiln, and the fs burns 150 ℃ from 20 ℃ by 150 minutes, removes the moisture in the base substrate; Subordinate phase burns 300 ℃ from 150 ℃ by 100 minutes, and moisture eliminates; Phase III burns 800 ℃ from 300 ℃ by 200 minutes, makes base substrate stable; The quadravalence section burns 1240 ℃ from 800 ℃ by 240 minutes, makes the abundant melting of glaze; Five-stage burns 1250 ℃ from 1240 ℃ by 20 minutes, is incubated 10 minutes, and the glaze crystallization is fully finished.Then naturally cooling, by the time 100 ℃ can kiln discharge.
Finally obtain the glaze effect: glazing effect has the smooth glaze of inferior light, and color has the green crystal effect of unearthed bronze work, simple and unsophisticated atmosphere, and some place of glaze can be mingled with a small amount of brown crystallization spot and have more elegant effect.Be fit to make large property sight vessel.
Embodiment 2:
Glaze quality prescription: 21.99 parts of potassium felspar sands, 9.23 parts in calcite, 3.40 parts of kaolin, 5.38 parts of aluminium sesquioxides, 1.00 parts of ventilation breathers, 1.4 parts of titanium dioxide mix.
Method for cooking and firing mode are with embodiment 1.
Copper is main chromogenic reagent in this patent glaze, thus in embodiment 2 0.5 part of ventilation breather, in the situation that copper raw material reduces, light dark green of glaze, the glaze that seems is dull, and is sour and astringent.
Embodiment 3:
Glaze quality prescription: 21.99 parts of potassium felspar sands, 9.23 parts in calcite, 3.40 parts of kaolin, 5.38 parts of aluminium sesquioxides, 5.00 parts of ventilation breathers, 1.4 parts of titanium dioxide mix.
Method for cooking and firing mode are with embodiment 1.
The color development of copper raw material is extensive, the color development that how much has a strong impact on glaze of amount, and when copper reached 5 component in the glaze component, milkiness appearred in glaze, and indecency black shows the unglazed of not melting property.
Claims (4)
1. bronze green crystal glaze, its raw material mass mixture ratio is as follows; 20～25 parts of potassium felspar sands, 8～10 parts in calcite, 2～5 parts of kaolin, 4～8 parts of aluminium sesquioxides, 1～5 part of ventilation breather, 0.5～2 part of titanium dioxide.
2. glaze as claimed in claim 1 is characterized in that its raw material mass mixture ratio is as follows: 21.99 parts of potassium felspar sands, 9.23 parts in calcite, 3.40 parts of kaolin, 5.38 parts of aluminium sesquioxides, 2.00 parts of ventilation breathers, 1.4 parts of titanium dioxide.
3. right to use requires 1 or 2 described glaze to fire the method for bronze green crystal glaze, and described method comprises: described glaze is mixed according to mass ratio 100:70～80 with water, and sink-float is sieved, and gets glaze slip; Transferring glaze slip proportion is 1.51, glazes on the ceramic body, and electrical kiln is fired, and cooling obtains the ceramic that there is bronze green crystal glaze on the surface.
4. method as claimed in claim 3 is characterized in that described electrical kiln is fired program as follows:
Fs: be warmed up to 150 ℃, time 150min from 20 ℃;
Subordinate phase: be warmed up to 300 ℃, time 100min from 150 ℃;
Phase III: be warmed up to 800 ℃, time 200min from 300 ℃;
Quadravalence section: be warmed up to 1240 ℃, time 240min from 800 ℃;
Five-stage: be warmed up to 1250 ℃, time 20min from 1240 ℃;
The 6th stage: 1250 ℃ are incubated 10 minutes.
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| CN201310232499.4A CN103304274B (en) | 2013-06-08 | 2013-06-08 | Bronze green crystalline glaze and firing method thereof |
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| CN201310232499.4A CN103304274B (en) | 2013-06-08 | 2013-06-08 | Bronze green crystalline glaze and firing method thereof |
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| CN103304274A true CN103304274A (en) | 2013-09-18 |
| CN103304274B CN103304274B (en) | 2015-04-29 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104418609A (en) * | 2013-08-19 | 2015-03-18 | 李宏伟 | Splash-ink ringing glaze |
| CN105565666A (en) * | 2015-12-30 | 2016-05-11 | 江苏宜翔陶瓷科技有限公司 | Preparation method of three-dimensional red chestnut matte artistic glaze for ceramic container |
| CN107540217A (en) * | 2017-09-30 | 2018-01-05 | 浙江工业大学之江学院 | A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze |
| CN107540216A (en) * | 2017-09-30 | 2018-01-05 | 浙江工业大学之江学院 | A kind of yellowish-brown colour glaze and the method for firing yellowish-brown color glaze |
| CN107572789A (en) * | 2017-09-30 | 2018-01-12 | 浙江工业大学之江学院 | A kind of matt light green color crystalline glaze material and the method for firing matt light green color crystalline glaze |
| CN107673614A (en) * | 2017-09-30 | 2018-02-09 | 浙江工业大学之江学院 | A kind of matt Blue crystalline glaze material and the method for firing matt Blue crystalline glaze |
| CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
| CN110526580A (en) * | 2019-09-29 | 2019-12-03 | 上海视觉艺术学院 | A kind of bronze glaze and preparation method thereof |
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| CN1488596A (en) * | 2003-08-21 | 2004-04-14 | 湖南泰鑫瓷业有限公司 | Copper green crystalline glaze and preparing method thereof |
| CN101306958A (en) * | 2008-07-03 | 2008-11-19 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making crystal fancy glaze |
| CN101913911A (en) * | 2010-07-30 | 2010-12-15 | 湖南华联溢百利瓷业有限公司 | Acid corrosion-resistant copper-green glaze and preparation method thereof |
| CN102515858A (en) * | 2011-12-14 | 2012-06-27 | 广东长城集团有限公司 | Sintering method of crystal glaze |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1488596A (en) * | 2003-08-21 | 2004-04-14 | 湖南泰鑫瓷业有限公司 | Copper green crystalline glaze and preparing method thereof |
| CN101306958A (en) * | 2008-07-03 | 2008-11-19 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method of making crystal fancy glaze |
| CN101913911A (en) * | 2010-07-30 | 2010-12-15 | 湖南华联溢百利瓷业有限公司 | Acid corrosion-resistant copper-green glaze and preparation method thereof |
| CN102515858A (en) * | 2011-12-14 | 2012-06-27 | 广东长城集团有限公司 | Sintering method of crystal glaze |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104418609A (en) * | 2013-08-19 | 2015-03-18 | 李宏伟 | Splash-ink ringing glaze |
| CN104418609B (en) * | 2013-08-19 | 2016-01-06 | 李宏伟 | The dizzy trace glaze of scribbling sketch |
| CN105565666A (en) * | 2015-12-30 | 2016-05-11 | 江苏宜翔陶瓷科技有限公司 | Preparation method of three-dimensional red chestnut matte artistic glaze for ceramic container |
| CN105565666B (en) * | 2015-12-30 | 2018-05-08 | 江苏宜翔陶瓷科技有限公司 | The three-dimensional red chestnut frosted artistic glaze preparation method of ceramic vessel |
| CN107540217A (en) * | 2017-09-30 | 2018-01-05 | 浙江工业大学之江学院 | A kind of sepia crystalline glaze material and the method for firing sepia crystalline glaze |
| CN107540216A (en) * | 2017-09-30 | 2018-01-05 | 浙江工业大学之江学院 | A kind of yellowish-brown colour glaze and the method for firing yellowish-brown color glaze |
| CN107572789A (en) * | 2017-09-30 | 2018-01-12 | 浙江工业大学之江学院 | A kind of matt light green color crystalline glaze material and the method for firing matt light green color crystalline glaze |
| CN107673614A (en) * | 2017-09-30 | 2018-02-09 | 浙江工业大学之江学院 | A kind of matt Blue crystalline glaze material and the method for firing matt Blue crystalline glaze |
| CN107673614B (en) * | 2017-09-30 | 2020-10-09 | 浙江工业大学之江学院 | Matte blue crystalline glaze and method for firing same |
| CN107540216B (en) * | 2017-09-30 | 2021-01-05 | 浙江工业大学之江学院 | Brown glaze and method for firing brown glaze |
| CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
| CN110526580A (en) * | 2019-09-29 | 2019-12-03 | 上海视觉艺术学院 | A kind of bronze glaze and preparation method thereof |
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| CN103304274B (en) | 2015-04-29 |
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Address after: 312030 Shaoxing, Keqiao province Ke Hua Road, No. 958, No. Patentee after: Zhijiang College of Zhejiang University of Tehcnology Address before: 310024 No. 182, Zhijiang Road, Hangzhou, Zhejiang, Xihu District Patentee before: Zhijiang College of Zhejiang University of Tehcnology |
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Granted publication date: 20150429 Termination date: 20160608 |