CN107384199A - A kind of vehicle glass coating liquid and preparation method thereof - Google Patents

A kind of vehicle glass coating liquid and preparation method thereof Download PDF

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Publication number
CN107384199A
CN107384199A CN201710661584.0A CN201710661584A CN107384199A CN 107384199 A CN107384199 A CN 107384199A CN 201710661584 A CN201710661584 A CN 201710661584A CN 107384199 A CN107384199 A CN 107384199A
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parts
coating liquid
tsl
added
preparation
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伊婕
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/06—Waxes
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
    • C03C17/008—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character comprising a mixture of materials covered by two or more of the groups C03C17/02, C03C17/06, C03C17/22 and C03C17/28
    • C03C17/009—Mixtures of organic and inorganic materials, e.g. ormosils and ormocers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2237—Oxides; Hydroxides of metals of titanium
    • C08K2003/2241—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/10—Transparent films; Clear coatings; Transparent materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of vehicle glass coating liquid and preparation method thereof, coating liquid component includes 10 20 parts of polyether silicone in parts by weight, 5 15 parts of hexadecyl trimethoxy silane, 10 25 parts of ethoxylated dodecyl alcohol, 5 10 parts of jasmine oil, 28 parts of nano particle, 34 12 parts of TSL 8330s, 5 15 parts of fluorine carbon surfactant, 20 40 parts of montanin wax emulsion, up to 8 18 parts of code tree fat, 25 parts of nanometer titanium dioxide, 30 40 parts of 16 parts of silicon powder and deionized water, preparation method of the present invention is simple, obtained coating liquid can improve the wearability on vehicle glass surface, the light transmittance of glass can be increased simultaneously, increase finish.

Description

A kind of vehicle glass coating liquid and preparation method thereof
Technical field
The present invention relates to coating liquid preparing technical field, specially a kind of vehicle glass coating liquid and preparation method thereof.
Background technology
Vehicle glass coating liquid refers to plate a layer thickness on vehicle glass surface and only has several to more than ten nanometer to see The hydrophobic protective film loseed, water droplet can not be formed the irregular moisture film of interference people's sight.It is widely used in the front and rear windscreen of automobile Glass, side windshield, the surface of rearview mirror, ensure that rainy day glass remains in that sight is good.Shield glass, after Mirror is after using this product, and the sight of driver is no longer influenceed by rain film, and degree of getting a clear view increases considerably, and substantially increases The comfortableness and security driven under the conditions of rainy day.
Vehicle glass coating liquid of the prior art can not be effectively protected glass surface, and light transmittance is low.
The content of the invention
It is an object of the invention to provide a kind of vehicle glass coating liquid and preparation method thereof, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：A kind of vehicle glass coating liquid, coating liquid component Include polyether silicone 10-20 parts, hexadecyl trimethoxy silane 5-15 parts, ethoxylated dodecyl alcohol in parts by weight 10-25 parts, jasmine oil 5-10 parts, nano particle 2-8 parts, 3- TSL 8330 4-12 parts, fluorine carbon surface are lived Property agent 5-15 parts, montanin wax emulsion 20-40 parts, up to code tree fat 8-18 parts, nanometer titanium dioxide 2-5 parts, silicon powder 1-6 parts and go Ionized water 30-40 parts.
Preferably, the preferable composition proportion of coating liquid component includes 15 parts of polyether silicone, hexadecyl trimethoxy silicon 10 parts of alkane, 18 parts of ethoxylated dodecyl alcohol, 8 parts of jasmine oil, 5 parts of nano particle, 8 parts of 3- TSL 8330s, 10 parts of fluorine carbon surfactant, 30 parts of montanin wax emulsion, up to 13 parts of code tree fat, 4 parts of nanometer titanium dioxide, 3 parts of silicon powder and 35 parts of deionized water.
Preferably, its preparation method comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation method of the present invention is simple, and obtained coating liquid can The wearability on vehicle glass surface is improved, while the light transmittance of glass can be increased, increases finish；Wherein, add in the present invention The ethoxylated dodecyl alcohol and fluorine carbon surfactant added, it can effectively remove the greasy dirt of glass surface；In the present invention The nanometer titanium dioxide and silicon powder of addition, can make that coating liquid permeability is more preferable, and the retention time is longer, and levelling is more preferable；In addition, this The preparation method used in invention is simple to operate, can further improve the activity of coating liquid.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects Enclose.
The present invention provides following technical scheme：A kind of vehicle glass coating liquid, coating liquid component include in parts by weight Polyether silicone 10-20 parts, hexadecyl trimethoxy silane 5-15 parts, ethoxylated dodecyl alcohol 10-25 parts, jasmine oil 5- 10 parts, nano particle 2-8 parts, 3- TSL 8330 4-12 parts, fluorine carbon surfactant 5-15 parts, cover denier Wax emulsion 20-40 parts, up to code tree fat 8-18 parts, nanometer titanium dioxide 2-5 parts, silicon powder 1-6 parts and deionized water 30-40 parts.
Embodiment one：
Coating liquid component includes 10 parts of polyether silicone, 5 parts of hexadecyl trimethoxy silane, laruyl alcohol polyoxy in parts by weight 10 parts of vinethene, 5 parts of jasmine oil, 2 parts of nano particle, 4 parts of 3- TSL 8330s, fluorine carbon surfactant 5 Part, 20 parts of montanin wax emulsion, up to 30 parts of 8 parts of code tree fat, 2 parts of nanometer titanium dioxide, 1 part of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Embodiment two：
Coating liquid component includes 20 parts of polyether silicone, 15 parts of hexadecyl trimethoxy silane, laruyl alcohol and gathered in parts by weight 25 parts of oxygen vinethene, 10 parts of jasmine oil, 8 parts of nano particle, 12 parts of 3- TSL 8330s, fluorine carbon surface are lived 15 parts of agent of property, 40 parts of montanin wax emulsion, up to 40 parts of 18 parts of code tree fat, 5 parts of nanometer titanium dioxide, 6 parts of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Embodiment three：
Coating liquid component includes 12 parts of polyether silicone, 6 parts of hexadecyl trimethoxy silane, laruyl alcohol polyoxy in parts by weight 12 parts of vinethene, 6 parts of jasmine oil, 3 parts of nano particle, 5 parts of 3- TSL 8330s, fluorine carbon surfactant 6 Part, 24 parts of montanin wax emulsion, up to 32 parts of 10 parts of code tree fat, 3 parts of nanometer titanium dioxide, 2 parts of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Example IV：
Coating liquid component includes 18 parts of polyether silicone, 13 parts of hexadecyl trimethoxy silane, laruyl alcohol and gathered in parts by weight 22 parts of oxygen vinethene, 9 parts of jasmine oil, 7 parts of nano particle, 10 parts of 3- TSL 8330s, fluorine carbon surface-active 13 parts of agent, 35 parts of montanin wax emulsion, up to 38 parts of 16 parts of code tree fat, 5 parts of nanometer titanium dioxide, 5 parts of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Embodiment five：
Coating liquid component includes 14 parts of polyether silicone, 12 parts of hexadecyl trimethoxy silane, laruyl alcohol and gathered in parts by weight 20 parts of oxygen vinethene, 7 parts of jasmine oil, 4 parts of nano particle, 10 parts of 3- TSL 8330s, fluorine carbon surface-active 11 parts of agent, 34 parts of montanin wax emulsion, up to 34 parts of 16 parts of code tree fat, 2 parts of nanometer titanium dioxide, 3 parts of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Embodiment six：
Coating liquid component includes 15 parts of polyether silicone, 10 parts of hexadecyl trimethoxy silane, laruyl alcohol and gathered in parts by weight 18 parts of oxygen vinethene, 8 parts of jasmine oil, 5 parts of nano particle, 8 parts of 3- TSL 8330s, fluorine carbon surface-active 10 parts of agent, 30 parts of montanin wax emulsion, up to 35 parts of 13 parts of code tree fat, 4 parts of nanometer titanium dioxide, 3 parts of silicon powder and deionized water.
The preparation method of the present embodiment comprises the following steps：
A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
Preparation method of the present invention is simple, and obtained coating liquid can improve the wearability on vehicle glass surface, while can Increase the light transmittance of glass, increase finish；Wherein, the ethoxylated dodecyl alcohol added in the present invention and fluorine carbon surface are lived Property agent, it can effectively remove the greasy dirt of glass surface；The nanometer titanium dioxide and silicon powder added in the present invention, can make plated film Liquid permeability is more preferable, and the retention time is longer, and levelling is more preferable；Obtained through overtesting, traditional coating liquid light transmittance is poor, easily makes glass There is the phenomenon of flower in glass, and uses the coating liquid of the present invention, it is possible to increase the light transmittance of glass；In addition, used in the present invention Preparation method is simple to operate, using the order of low-temperature heat, mixed at high speed and refrigeration, can further improve the work of coating liquid Property.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (3)

  1. A kind of 1. vehicle glass coating liquid, it is characterised in that：Coating liquid component includes polyether silicone 10-20 in parts by weight Part, hexadecyl trimethoxy silane 5-15 parts, ethoxylated dodecyl alcohol 10-25 parts, jasmine oil 5-10 parts, nano particle 2- 8 parts, 3- TSL 8330 4-12 parts, fluorine carbon surfactant 5-15 parts, montanin wax emulsion 20-40 parts, reach Code tree fat 8-18 parts, nanometer titanium dioxide 2-5 parts, silicon powder 1-6 parts and deionized water 30-40 parts.
  2. A kind of 2. vehicle glass coating liquid according to claim 1, it is characterised in that：The preferable composition of coating liquid component Proportioning includes 15 parts of polyether silicone, 10 parts of hexadecyl trimethoxy silane, 18 parts of ethoxylated dodecyl alcohol, jasmine oil 8 Part, 5 parts of nano particle, 8 parts of 3- TSL 8330s, 10 parts of fluorine carbon surfactant, montanin wax emulsion 30 Part, up to 35 parts of 13 parts of code tree fat, 4 parts of nanometer titanium dioxide, 3 parts of silicon powder and deionized water.
  3. 3. realize a kind of preparation method of vehicle glass coating liquid described in claim 1, it is characterised in that：Its preparation method Comprise the following steps：
    A, by polyether silicone, hexadecyl trimethoxy silane, ethoxylated dodecyl alcohol, jasmine oil, nano particle, 3- Added after TSL 8330 mixing and low-temperature heat reaction is carried out in retort, temperature is 40 DEG C, and the time is 20min, it is slowly cooled to room temperature afterwards, obtains mixed liquor A；
    B, sequentially added in mixed liquor A 3- TSL 8330s, fluorine carbon surfactant, montanin wax emulsion, Added up to code tree fat and deionized water, after mixing in agitator tank and carry out high-speed stirred, speed is 3000 revs/min, and the time is 30min, nanometer titanium dioxide, silicon powder are added in whipping process；
    C, refrigerating chamber refrigeration 6h is put into after 20min is stood after stirring terminates, that is, obtains coating liquid.
CN201710661584.0A 2017-08-04 2017-08-04 A kind of vehicle glass coating liquid and preparation method thereof Withdrawn CN107384199A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111393926A (en) * 2020-03-16 2020-07-10 北京京蝠环保科技有限公司 Water-based coating liquid
CN111849352A (en) * 2020-07-22 2020-10-30 广东佰旺实业有限公司 Automobile glass antiwear agent and preparation method thereof
CN116496698A (en) * 2023-05-30 2023-07-28 西安紫怡汽车用品有限公司 Automobile glass coating liquid

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102516886A (en) * 2011-09-29 2012-06-27 青岛唐尼环境产品有限公司 Aqueous automobile film-plating solution and its preparation method
CN105754381A (en) * 2015-03-04 2016-07-13 张扬 Nano anti-reflection coating liquid and preparation method and application thereof
CN106905739A (en) * 2017-04-20 2017-06-30 马鞍山市润启新材料科技有限公司 A kind of environment-friendly type additive paint and its preparation technology

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102516886A (en) * 2011-09-29 2012-06-27 青岛唐尼环境产品有限公司 Aqueous automobile film-plating solution and its preparation method
CN105754381A (en) * 2015-03-04 2016-07-13 张扬 Nano anti-reflection coating liquid and preparation method and application thereof
CN106905739A (en) * 2017-04-20 2017-06-30 马鞍山市润启新材料科技有限公司 A kind of environment-friendly type additive paint and its preparation technology

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111393926A (en) * 2020-03-16 2020-07-10 北京京蝠环保科技有限公司 Water-based coating liquid
CN111849352A (en) * 2020-07-22 2020-10-30 广东佰旺实业有限公司 Automobile glass antiwear agent and preparation method thereof
CN116496698A (en) * 2023-05-30 2023-07-28 西安紫怡汽车用品有限公司 Automobile glass coating liquid
CN116496698B (en) * 2023-05-30 2024-03-19 西安紫怡汽车用品有限公司 Automobile glass coating liquid

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