CN102516886A - Aqueous automobile film-plating solution and its preparation method - Google Patents
Aqueous automobile film-plating solution and its preparation method Download PDFInfo
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- CN102516886A CN102516886A CN2011103103434A CN201110310343A CN102516886A CN 102516886 A CN102516886 A CN 102516886A CN 2011103103434 A CN2011103103434 A CN 2011103103434A CN 201110310343 A CN201110310343 A CN 201110310343A CN 102516886 A CN102516886 A CN 102516886A
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Abstract
The invention discloses an aqueous automobile film-plating solution, which is prepared by the following raw materials by weight: 0.5-2 parts of alkylphenol polyoxyethylene, 3-6 parts of fatty alcohol polyoxyethylene ether, 2-9 parts of a polymer suspending agent, 0.1-1.6 parts of a fluorocarbon surfactant, 12-25 parts of a montan wax emulsion, 3-6 parts of white mineral oil, 1-5 parts of an aqueous silicone oil emulsion, 35.9-72.1 parts of water, 2-4 parts of isopropyl alcohol, and 0.1-0.5 parts of a bactericide. The solid content of the montan wax emulsion is 15-35%, and the solid content of the aqueous silicone oil emulsion is 35-55%. Based on the utility model patent ''automobile glaze-sealing film-plating wipes'' applied by the applicant, the invention conducts secondary research and development. First, improvement and innovation are conducted on the emulsion process of the main component montan wax, so that the material particle size can be closer to nanoscale. Overcoming of the difficulty makes polishing easier and brightness higher so as to generate a mirror effect. Meanwhile, other components are adjusted so as to bring about better permeability, longer retention time and better levelling property. Long-term use of the film-plating solution product of the invention can reach the effects of making old cars new and maintaining new cars new.
Description
Technical field
The present invention relates to a kind of automobile coating liquid, especially relate to automobile coating liquid of a kind of water-based and preparation method thereof, belong to chemical field.
Background technology
The progressively raising of Along with people's standard of living, the family that has automobile in China is more and more with the individual, has in the further differentiation of car life people, and owner also can more and more be paid attention to the maintenance of automobile.The maintenance of automobile had both comprised that the maintenance of automotive interior also comprised the maintenance of automobile external car lacquer.Along with the automobile growth of duration of service, like that a lot of trickle scratches will appear in the metal car lacquer surface of car, the brightness of car lacquer is reduced; Becoming, darkness deepens; Particularly along with automobile wash number and the increase of sweeping the train number number, under the effect of micronic dust, this phenomenon is more and more serious.Therefore a lot of lacquer painting cosmetics occurred, the lacquer painting beauty treatment in the market and the product of maintenance roughly are divided three classes: wax, envelope glaze and plated film.It is the petroleum-type product that these products all belong to solvent-borne type, and itself is oxidation easily just, limited to the protection and the cosmetic result of car lacquer, goes back contaminate environment simultaneously; Wherein existing envelope glaze, coating operation program complicacy, they carry out sanding and polishing earlier need for automobile finish, and this itself will damage the car lacquer.
Summary of the invention
To the deficiency of prior art, technical problem to be solved by this invention is, a kind of aqueous automobile coating liquid and preparation method thereof is provided, and makes material particle size more near nano level, and schedule of operation is simple, can itself not damage the car lacquer
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of aqueous automobile coating liquid, and its raw material by following parts by weight is processed:
TX10 0.5-2 part, AEO 3-6 part, polymer suspension agent 2-9 part; Fluorine carbon tensio-active agent 0.1-1.6 part, montanin wax emulsion 12-25 part, white mineral oil 3-6 part; Water-based silicone oil emulsion 1-5 part; Water 35.9-72.1 part, Virahol 2-4 part, sterilant 0.1-0.5 part; The solid content of said montanin wax emulsion is 15-35%, and the solid content of water-based silicone oil emulsion is 35-55%.
A kind of preparation method of above-mentioned aqueous automobile coating liquid may further comprise the steps:
(1) deionized water is heated to 85 ℃, with montanin wax (trade(brand)name: Licowax KLE) join in the hot water, naturally cool to normal temperature after the stirring, make the montanin wax emulsion in the above-mentioned prescription;
(2) in whisking appliance, add by above-mentioned prescription and stirred 40 minutes after than water and TX10, add AEO again, stirs adding fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then;
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
Optimize, the whipping temp of montanin wax is 90 ℃ among the preparation method of above-mentioned aqueous automobile coating liquid, its step (1), and churning time is 30 minutes.
The present invention is on the basis of the utility model patent " automobile glaze-sealing film-coating wet towel " the applicant, has carried out the secondary research and development, at first on the emulsifying process of staple montanin wax, improves and innovates; Make material particle size more near nano level, the capturing of this difficulty make to polish and become easily, and brightness is higher and produced mirror effect; We have adjusted other compositions simultaneously; Make perviousness better, the hold-time is longer, and levelling is better; This product of life-time service can reach fully: make used car become new, new car is protected new effect.
Embodiment
Below in conjunction with accompanying drawing and embodiment to the invention further explain.
Embodiment 1
The present invention is a kind of aqueous automobile coating liquid, and its raw material by following parts by weight is processed:
0.5 part of TX10; 3 parts of AEOs; 2 parts of polymer suspension agents like vinyl pyrrolidone, also can replace with vinyl acetate copolymer; 0.1 part in fluorine carbon tensio-active agent, like fluorocarbon surfactant FCN, refined Science and Technology Ltd. produces by Hangzhou benevolence, and Chemical Composition is fluorine-containing nonionogenic tenside; 12 parts of montanin wax emulsions; 3 parts of white mineral oils; 1 part of water-based silicone oil emulsion; 35.9 parts in water; 2 parts of Virahols; 0.1 part in sterilant, like triumphant pine, triumphant pine is the transliteration of English KATONH, and effective constituent is the mixture of RH-893 CIT and MIT, and molecular formula is C4H4C1NOS+C4H5NOS, and molecular weight is 149.56+115.06; The solid content of montanin wax emulsion is 15%; The solid content of water-based silicone oil emulsion is 35%.
A kind of preparation method of above-mentioned aqueous automobile coating liquid may further comprise the steps:
(1) deionized water is heated to 85 ℃, (trade(brand)name: Licowax KLE) join in the hot water, constant temperature stirs after 30 minutes for 90 ℃ and naturally cools to normal temperature, makes the montanin wax emulsion in the above-mentioned prescription with montanin wax;
(2) in whisking appliance, add behind entry and the TX10 and stirred 40 minutes, add AEO again, stirs and add the fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then by above-mentioned prescription ratio;
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
Embodiment 2
The present invention is a kind of aqueous automobile coating liquid, and its raw material by following parts by weight is processed:
2 parts of TX10s; 6 parts of AEOs; 9 parts of polymer suspension agents are like xanthan gum; 1.6 parts in fluorine carbon tensio-active agent; Like fluorine carbon tensio-active agent
-14-1B, give birth to tea by Yingzheng Scirnce and Technology Co., Ltd., Shanghai; 25 parts of montanin wax emulsions, 6 parts of white mineral oils, 5 parts of water-based silicone oil emulsions, 72.1 parts in water; 4 parts of Virahols, 0.5 part in sterilant like BIT20, is made by Taizhou City Ou Lai chemical industry ltd proprietary technology; Main effective constituent is BIT, and chemical name is 1, the 2-benzisothiazole-3-ketone; The solid content of said montanin wax emulsion is 15-35%, and the solid content of water-based silicone oil emulsion is 35-55%.
Fluorocarbon surfactant can be called tensio-active agent with capillary one type of material that extremely low concentration reduces solvent significantly.Fluorocarbon surfactant is a most important kind in the special surface active agent; Wasserstoffatoms in the hydrocarbon chain of finger hc-surfactant is all or part of to be replaced by fluorine atom; Be that fluorocarbon chain has replaced hydrocarbon chain, so the nonpolar group in the tensio-active agent not only have the performance of hydrophobic property but also unique oleophobic.
A kind of preparation method of above-mentioned aqueous automobile coating liquid may further comprise the steps:
(1) deionized water is heated to 85 ℃, (trade(brand)name: Licowax KLE) join in the hot water, constant temperature stirs after 30 minutes for 90 ℃ and naturally cools to normal temperature, makes the montanin wax emulsion in the above-mentioned prescription with montanin wax;
(2) in whisking appliance, add by above-mentioned prescription and stirred 40 minutes after than water and TX10, add AEO again, stirs adding fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then;
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
The present invention is a kind of aqueous automobile coating liquid, and liquid is the creamy white water-based emulsion, uses non-woven fabrics to be carrier, is applied in car and paints, and dry back is with the manual burnish of ultra-fine fibre wiper.
Embodiment 3
The present invention is a kind of aqueous automobile coating liquid, and its raw material by following parts by weight is processed:
1.5 parts of TX10s; 4.5 parts of AEOs; 5.5 parts of polymer suspension agents are like carbomer; 0.8 part in fluorine carbon tensio-active agent; Like
-14-2A, provide by Yingzheng Scirnce and Technology Co., Ltd., Shanghai; 18 parts of montanin wax emulsions, 5 parts of white mineral oils, 3 parts of water-based silicone oil emulsions, 50 parts, 3 parts of Virahols, 0.3 part in sterilant, as new 99, vast biochemical ltd provides by Nantong, Guangzhou, and pH value is 2~4; The solid content of said montanin wax emulsion is 25%, and the solid content of water-based silicone oil emulsion is 45%.
A kind of preparation method of above-mentioned aqueous automobile coating liquid may further comprise the steps:
(1) deionized water is heated to 85 ℃, (trade(brand)name: Licowax KLE) join in the hot water, constant temperature stirs after 30 minutes for 90 ℃ and naturally cools to normal temperature, makes the montanin wax emulsion in the above-mentioned prescription with montanin wax;
(2) in whisking appliance, add by above-mentioned prescription and stirred 40 minutes after than water and TX10, add AEO again, stirs adding fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then:
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
Embodiment 4
The present invention is a kind of aqueous automobile coating liquid, and its raw material by following parts by weight is processed:
2 parts of TX10s; 6 parts of AEOs; 9 parts of polymer suspension agents are like Walocel MT 20.000PV; 1.6 parts in fluorine carbon tensio-active agent; Like fluorine carbon tensio-active agent
-14-1B, provide by Yingzheng Scirnce and Technology Co., Ltd., Shanghai; 25 parts of montanin wax emulsions, 6 parts of white mineral oils, 5 parts of water-based silicone oil emulsions, 72.1 parts in water; 4 parts of Virahols, 0.5 part in sterilant like BIT20, is made by Taizhou City Ou Lai chemical industry ltd proprietary technology; Main effective constituent is BIT, and chemical name is 1, the 2-benzisothiazole-3-ketone; The solid content of said montanin wax emulsion is 15-35%, and the solid content of water-based silicone oil emulsion is 35-55%.
A kind of preparation method of above-mentioned aqueous automobile coating liquid may further comprise the steps:
(1) deionized water is heated to 85 ℃, (trade(brand)name: Licowax KLE) join in the hot water, constant temperature stirs after 30 minutes for 90 ℃ and naturally cools to normal temperature, makes the montanin wax emulsion in the above-mentioned prescription with montanin wax;
(2) in whisking appliance, add by above-mentioned prescription and stirred 40 minutes after than water and TX10, add AEO again, stirs adding fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then;
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
Certainly, above-mentioned explanation is not to be limitation of the present invention, and the present invention also is not limited to above-mentioned giving an example; Those skilled in the art; In essential scope of the present invention, the variation of making, remodeling, interpolation or replacement all should belong to protection scope of the present invention.
Claims (3)
1. aqueous automobile coating liquid, it is characterized in that: the raw material by following parts by weight is processed:
TX10 0.5-2 part, AEO 3-6 part, polymer suspension agent 2-9 part; Fluorine carbon tensio-active agent 0.1-1.6 part, montanin wax emulsion 12-25 part, white mineral oil 3-6 part; Water-based silicone oil emulsion 1-5 part; Water 35.9-72.1 part, Virahol 2-4 part, sterilant 0.1-0.5 part; The solid content of said montanin wax emulsion is 15-35%, and the solid content of water-based silicone oil emulsion is 35-55%.
2. the preparation method of the described aqueous automobile coating liquid of claim 1 may further comprise the steps:
(1) deionized water is heated to 85 ℃, montanin wax is joined in the hot water, naturally cool to normal temperature after the stirring, make the montanin wax emulsion in the above-mentioned prescription;
(2) in whisking appliance, add behind entry and the TX10 and stirred 40 minutes, add AEO again, stirs and add the fluorine carbon tensio-active agent after 30-40 minute, stirred 20 minutes, add white mineral oil stirring 2 hours then by above-mentioned prescription ratio;
(3) in above-mentioned whisking appliance, stirred 30 minutes behind the adding polymer suspension agent again, and then add Virahol, stirred 15 minutes, add sterilant again, stirred 10 minutes, add the water-based silicone oil emulsion at last, stirred 30 minutes;
(4) the montanin wax emulsion with preparation in the step (1) adds in the above-mentioned whisking appliance, stirs to leave standstill after 60 minutes to get final product discharging in 12 hours.
3. the preparation method of aqueous automobile coating liquid according to claim 2 is characterized in that: the whipping temp of montanin wax is 90 ℃ in the described step (1), and churning time is 30 minutes.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105153937A (en) * | 2015-08-24 | 2015-12-16 | 广州赫厉狮森汽车用品有限公司 | Total-synthesis solid wax capable of forming platinum coating film and preparation method of total-synthetic solid wax |
CN107384199A (en) * | 2017-08-04 | 2017-11-24 | 伊婕 | A kind of vehicle glass coating liquid and preparation method thereof |
CN107418447A (en) * | 2017-04-21 | 2017-12-01 | 南宁市钱隆汽车租赁有限公司 | Automobile coating liquid |
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CN101050401A (en) * | 2007-04-02 | 2007-10-10 | 刘正明 | Caring agent of covered membrane for environmental protective car wash without water |
CN201276261Y (en) * | 2008-08-04 | 2009-07-22 | 隋向人 | Wet tissue for sealing glaze and plating film on surface of vehicle paint |
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CN1265992A (en) * | 1999-03-06 | 2000-09-13 | 速特99化工有限公司 | Wet cloth for washing,water-proof fine renovating and polishing car paint film |
CN1273993A (en) * | 2000-05-11 | 2000-11-22 | 华南理工大学 | Process for preparing multifunctional cleaning-polishing agent for car and its application method |
CN1332102A (en) * | 2000-06-26 | 2002-01-23 | 林浩 | Automobile and motorcycle deterging and brightening towel |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN105153937A (en) * | 2015-08-24 | 2015-12-16 | 广州赫厉狮森汽车用品有限公司 | Total-synthesis solid wax capable of forming platinum coating film and preparation method of total-synthetic solid wax |
CN107418447A (en) * | 2017-04-21 | 2017-12-01 | 南宁市钱隆汽车租赁有限公司 | Automobile coating liquid |
CN107384199A (en) * | 2017-08-04 | 2017-11-24 | 伊婕 | A kind of vehicle glass coating liquid and preparation method thereof |
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