CN107361411A - A kind of preparation method of wool flocking thermal underwear face fabric - Google Patents
A kind of preparation method of wool flocking thermal underwear face fabric Download PDFInfo
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- CN107361411A CN107361411A CN201710504518.2A CN201710504518A CN107361411A CN 107361411 A CN107361411 A CN 107361411A CN 201710504518 A CN201710504518 A CN 201710504518A CN 107361411 A CN107361411 A CN 107361411A
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- wool
- flocking
- face fabric
- thermal underwear
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Classifications
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B3/00—Mechanical removal of impurities from animal fibres
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B21/00—Successive treatments of textile materials by liquids, gases or vapours
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/02—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fibres, slivers or rovings
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B9/00—Solvent-treatment of textile materials
- D06B9/02—Solvent-treatment of textile materials solvent-dyeing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N7/00—Flexible sheet materials not otherwise provided for, e.g. textile threads, filaments, yarns or tow, glued on macromolecular material
- D06N7/0097—Web coated with fibres, e.g. flocked
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Animal Husbandry (AREA)
- Mechanical Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Undergarments, Swaddling Clothes, Handkerchiefs Or Underwear Materials (AREA)
Abstract
The invention provides a kind of preparation method of wool flocking thermal underwear face fabric, comprise the following steps：(1) wool skin is screened and impurity elimination；(2) it is pretreated fur hydro-peening is clean, then dry；(3) after the compound alkali lye of the fur cleaned up addition is handled 24 hours at 60 80 DEG C, regulation PH is 7, filters while hot, obtains wool, then will be washed, dried；(4) will be by wool textile；(5) dyed, shear treatment obtains wool lint again.(6) thermal underwear face fabric is made by static flocking technology.Thermal underwear face fabric obtained by the present invention obtains thermal underwear face fabric using wool lint through electrostatic spinning, natural environmental-protective, soft fine and smooth, good warmth retention effect, meets the high quality requirement of consumer.
Description
Technical field
The invention belongs to cold-proof underwear processing technique field, and in particular to a kind of preparation of wool flocking thermal underwear face fabric
Method.
Background technology
Cold-proof underwear belongs to personal warming clothes, is adapted to late fall and the winter of cold to wear, and put on the swelling that will not seem
It is swollen, it is light agile.With the increasingly raising of people's living standard, the continuous renewal of consumption idea, consumer is to weaving face fabric
The consumption of quality, kind and environmental protection etc. requires more and more higher.Vast disappear is received at present using cold-proof underwear made from flocking technology
The favor of the person of expense, but flocking in the market is made using chemical fibre more, and product is single, and feel is poor, without natural
Smooth, fine and smooth, the high-grade feel of animal fur, it is difficult to meet the market demand of diversification.
As the wool fiber of important textile raw material, there are many advantages：Excellent elasticity, spreadability and thermal insulation, favorably
The thermal with human body is kept in fabric shape；Soft gloss and good moisture adsorption and releasing energy, can obtain comfortable fabric
Style；Unique felting property is advantageous to fabric forming and densification；It is good that distinctive spiral macromolecular and cross-linked structure assign fiber
Good elasticity recovery and setting mechanism.Wool is processed into flocked fiber, is applied to the guarantor that can meet people on cold-proof underwear
The warm, demand of natural environmental-protective.
Chinese patent ZL201110146760X provides a kind of preparation method of leather flocking short fiber, by corium corner
Flocking corium chopped fiber is made through screening the techniques such as color separation, high frequency cleaning, low-temperature grinding, spraying colouring and airflow drying in material.Should
Method turns waste into wealth corium leftover pieces, but its chopped fiber percentage of impurity is higher, and the protein residue of animal's leather, which is difficult to remove, to be done
Only, and the dyeing of made flocking chopped fiber is uneven, and dye stability is poor.
The content of the invention
The invention provides a kind of preparation method of wool flocking thermal underwear face fabric, using wool lint through electrostatic spinning
Thermal underwear face fabric is obtained, natural environmental-protective, soft fine and smooth, good warmth retention effect, meets the high quality requirement of consumer.
The technical proposal for solving the technical problem of the invention is：
A kind of preparation method of wool flocking thermal underwear face fabric, comprises the following steps：
(1) pre-process：Wool skin is subjected to screening and obtains the close fur of quality with impurity elimination；
(2) aerosol hydro-peening：The fur that will be pre-processed through step (1) is clean through aerosol hydro-peening, then through 40-60 DEG C of vacuum drying；
(3) alkali cleaning：The fur cleaned up obtained by step (2) is added into compound alkali lye 2-4 hours are handled at 60-80 DEG C
Afterwards, it is 7 to adjust PH, filters while hot, obtains wool, then will be washed, dried；Will be dynamic by the special compound alkali lye of the present invention
Leather component in thing fur is decomposed so that fur is rapidly separated, and good separating effect, then filtered obtains wool.
(4) wool is added into shredding in mixing willow to mix, then cleaned through scutcher shredding, carding machine cards, spinned simultaneously
Twist fineness is 20-35 μm of wool raw yarn；
(5) dye：Wool raw yarn is added in dyeing cylinder, then dye solution is added toward dyeing in cylinder, is heated to 50-70
DEG C, after insulation dyeing 3-5 hours, tryptophan and color fixing agent are added, continues isothermal holding after 30 minutes, regulation PH is 7, is taken out
Wool raw yarn, after 90-100 DEG C is dried in vacuo 30 minutes, room temperature is cooled to, then through washing 3-5 times, then at 40-60 DEG C of vacuum
Drying obtains fineness and is 20-35 μm of wool yarn, and cuts into the wool lint that length is 1-5mm；
(6) the wool lint obtained by step (5) is made into flocking, acrylic acid makees adhesive, carries out 3-5 electrostatic spinning to base fabric
On layer flocking fabric, then at 110-130 DEG C baking 5-8 minutes, after heat treatment on forming machine, then with blower fan by remain plant
Suede is blown away, then through combing to obtain institute's wool flocking thermal underwear face fabric.
For usual people to the acquisition pattern of wool from periodically shearing, this mode typically results on sheepskin residual wool not
It can be fully used, and the cultured output of China flock of sheep is limited, wool limited source, therefore be efficiently sheep using existing resource
A great problem in hair Yarn Processing Technology.
And the method for compound alkali cleaning depilation of the present invention can effectively utilize all wools on sheepskin, production of wool
It is higher.
Preferably, the compound alkali lye described in step (3) is made up of following parts by weight component：20-30 part bicarbonates
Sodium, 5-10 parts ethylenediamine, 3-5 parts sodium metasilicate, 1-3 parts aminophylline, 1-3 parts alum and 30-40 part water.Compound alkali lye is using a variety of
Weak base compounding forms, and alkaline matter can be dissolved in the material of water with the fat in animal's leather and albumen qualitative response generation, so that
Obtain animal's leather to decompose so that fur quick separating.According to highly basic processing, then wool can be caused to degrade, influence its smoothness.
Sodium metasilicate in compound alkali lye can form layer protecting film in wool surfaces, further reduce alkali lye and it is damaged, and alum can be with
Increase the compliance and glossiness of wool.
Preferably, the mass ratio of the fur and compound alkali lye described in step (3) is 1：10-15.
Preferably, the dye solution described in step (4) is made up of following parts by weight component：20-30 parts are acid cloudy
Ion pigment, 30-40 parts water and 1-3 part cosolvents.
It is further preferred that described acidic anionic pigment be selected from acid red, acid black, acid blue, acid ash, acid golden yellow and
At least one of acid brown.
It is further preferred that described cosolvent is sodium cetanesulfonate, polyoxyethylene sorbitan monooleate or dehydration
Sorbitan fatty acid ester.
Preferably, the color fixing agent described in step (4) is cetylpyridinium chloride or brocide.Acid
Property anionic pigment be one of the dyestuff commonly used in animal skin, but its shortcoming is that dyeing is uneven, and dyeing firmness needs to be carried
It is high.Tryptophan in alkalescent, can be reacted with acidic anionic pigment as a kind of alkaloid, at the same can and wool surfaces
Protein crosslink reaction so that dyeing firmness be improved.From cetylpyridinium chloride or cetyl
Yl pyridines make color fixing agent, can be reacted with acidic anionic pigment, further function as the effect of fixation.
It is further preferred that the mass ratio of the wool raw yarn, dye solution, tryptophan and color fixing agent described in step (4) is 1：10-
20：0.03-0.05：0.05-0.08.
Preferably, the material of the bottom cloth layer described in step (4) is cotton, acrylic fibers or terylene.
Beneficial effects of the present invention are：
1st, compound base extraction wool skin is formed using a variety of weak base compounding, so that animal's leather decomposes so that fur
Quick separating, while wool is not caused to damage again, influence the quality of wool lint.
2nd, the wool lint bright prepared by the present invention, even dyeing, dyeing firmness are high.
3rd, wool lint processing method provided by the present invention, can be effectively using the wool near sheepskin, and wool yield is more
It is high.
4th, the thermal underwear face fabric obtained by the present invention obtains thermal underwear face fabric using wool lint through electrostatic spinning, naturally
Environmentally friendly, soft fine and smooth, good warmth retention effect, meet the high quality requirement of consumer.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments to the present invention
It is further elaborated.
Embodiment 1
(1) pre-process：Wool skin is subjected to screening and obtains the close fur of quality with impurity elimination；
(2) aerosol hydro-peening：The fur that will be pre-processed through step (1) is clean through aerosol hydro-peening, then through 40 DEG C of vacuum dryings；
(3) alkali cleaning：After the compound alkali lye of the fur cleaned up addition obtained by step (2) is handled 4 hours at 60 DEG C, adjust
It is 7 to save PH, filters while hot, obtains wool, then will be washed, dried.The compound alkali lye is by following parts by weight component group
Into：20 parts of sodium acid carbonates, 8 parts of ethylenediamines, 4 parts of sodium metasilicate, 1 part of aminophylline, 2 parts of alum and 35 parts of water, described animal fur
Mass ratio with compound alkali lye is 1：10.
(4) wool is added into shredding in mixing willow to mix, then cleaned through scutcher shredding, carding machine cards, spinned simultaneously
Twist fineness is 20 μm of wool raw yarn；
(5) dye：100g wools raw yarn is added in dyeing cylinder, then dye solution is added toward dyeing in cylinder, is heated to 50
DEG C, after insulation dyeing 5 hours, add 3g tryptophans and with 6g cetylpyridinium chlorides, continue isothermal holding after 30 minutes,
It is 7 to adjust PH, takes out wool raw yarn, after 100 DEG C are dried in vacuo 30 minutes, is cooled to room temperature, then through washing 3-5 times, then at
60 DEG C of vacuum dryings obtain fineness and are 20 μm of wool yarn, and cut into the wool lint that length is 3mm；Described dye solution
It is made up of following parts by weight component：20 parts of acid reds, 35 parts of water and 3 parts of sodium cetanesulfonates.
(6) the wool lint obtained by step (5) is made into flocking, acrylic acid makees adhesive, carries out 4 electrostatic spinnings on earth
Flocking fabric is obtained on layer of cloth, is bakeed 6 minutes then at 120 DEG C, is blown after heat treatment on forming machine, then with blower fan by flocking is remained
Walk, then through combing to obtain institute's wool flocking thermal underwear face fabric.
Made thermal underwear face fabric bright, color is homogeneous, soft, smooth, scalds through high temperature and does not fade, in
SEM electricity Microscopic observations, wool lint surface fracture are less.
Embodiment 2
(1) pre-process：Wool skin is subjected to screening and obtains the close fur of quality with impurity elimination；
(2) aerosol hydro-peening：The fur that will be pre-processed through step (1) is clean through aerosol hydro-peening, then through 50 DEG C of vacuum dryings；
(3) alkali cleaning：After the compound alkali lye of the fur cleaned up addition obtained by step (2) is handled 2 hours at 80 DEG C, adjust
It is 7 to save PH, filters while hot, obtains wool, then will be washed, dried；The compound alkali lye is by following parts by weight component group
Into：25 parts of sodium acid carbonates, 10 parts of ethylenediamines, 3 parts of sodium metasilicate, 3 parts of aminophyllines, 3 parts of alum and 30 parts of water, described fur and multiple
The mass ratio for closing alkali lye is 1：12.
(4) wool is added into shredding in mixing willow to mix, then cleaned through scutcher shredding, carding machine cards, spinned simultaneously
Twist fineness is 25 μm of wool raw yarn；
(5) dye：100g wools raw yarn is added in dyeing cylinder, then toward addition 1000g dye solutions in dyeing cylinder, added
Heat to 60 DEG C, insulation dyeing 4 hours after, add 5g tryptophans and with 8g cetylpyridinium chlorides, continue isothermal holding 30
After minute, regulation PH is 7, takes out wool raw yarn, after 90 DEG C are dried in vacuo 30 minutes, is cooled to room temperature, then through washing 3-5
It is secondary, obtain fineness then at 60 DEG C of vacuum dryings and be 25 μm of wool yarn, and cut into the wool lint that length is 5mm；Described
Dye solution is made up of following parts by weight component：30 parts of acid golden yellows, 30 parts of water and 1 part of polyethenoxy sorbitan list oil
Acid esters.
(6) the wool lint obtained by step (5) is made into flocking, acrylic acid makees adhesive, carries out 3 electrostatic spinnings on earth
Flocking fabric is obtained on layer of cloth, is bakeed 8 minutes then at 110 DEG C, is blown after heat treatment on forming machine, then with blower fan by flocking is remained
Walk, then through combing to obtain institute's wool flocking thermal underwear face fabric.
Made thermal underwear face fabric bright, color is homogeneous, soft, smooth, scalds through high temperature and does not fade, in
SEM electricity Microscopic observations, thermal underwear face fabric surface fracture are less.
Embodiment 3
(1) pre-process：Wool skin is subjected to screening and obtains the close fur of quality with impurity elimination；
(2) aerosol hydro-peening：The fur that will be pre-processed through step (1) is clean through aerosol hydro-peening, then through 60 DEG C of vacuum dryings；
(3) alkali cleaning：After the compound alkali lye of the fur cleaned up addition obtained by step (2) is handled 3 hours at 70 DEG C, adjust
It is 7 to save PH, filters while hot, obtains wool, then will be washed, dried；The compound alkali lye is by following parts by weight component group
Into：30 parts of sodium acid carbonates, 5 parts of ethylenediamines, 5 parts of sodium metasilicate, 2 parts of aminophyllines, 1 part of alum and 40 parts of water, described animal fur
Mass ratio with compound alkali lye is 1：15.
(4) wool is added into shredding in mixing willow to mix, then cleaned through scutcher shredding, carding machine cards, spinned simultaneously
Twist fineness is 35 μm of wool raw yarn；
(5) dye：100g wools raw yarn is added in dyeing cylinder, then toward addition 2000g dye solutions in dyeing cylinder, added
Heat to 70 DEG C, insulation dyeing 3 hours after, add 4g tryptophans and with 5g cetylpyridinium chlorides, continue isothermal holding 30
After minute, regulation PH is 7, takes out wool raw yarn, after 95 DEG C are dried in vacuo 30 minutes, is cooled to room temperature, then through washing 3-5
It is secondary, produce fineness then at 60 DEG C of vacuum dryings and be 35 μm of wool yarn, and cut into the wool lint that length is 1mm；It is described
Dye solution be made up of following parts by weight component：25 parts of acid blues, 35 parts of water and 3 parts of sorbitan fatty esters.
(6) the wool lint obtained by step (5) is made into flocking, acrylic acid makees adhesive, carries out 5 electrostatic spinnings on earth
Flocking fabric is obtained on layer of cloth, is bakeed 5 minutes then at 130 DEG C, is blown after heat treatment on forming machine, then with blower fan by flocking is remained
Walk, then through combing to obtain institute's wool flocking thermal underwear face fabric.
Made thermal underwear face fabric bright, color is homogeneous, soft, smooth, scalds through high temperature and does not fade, in
SEM electricity Microscopic observations, thermal underwear face fabric surface fracture are less.
Comparative example 1
Operated with embodiment 1 it is identical, unlike use in step (3) mass concentration for 30% sodium hydrate aqueous solution replacement
Compound alkali lye, made cold-proof underwear color and luster is dark, and color is homogeneous, and feel is partially puckery, scalds through high temperature and does not fade.
Comparative example 2
Operated with embodiment 1 it is identical, unlike do not add tryptophan in step (4), made cold-proof underwear color and luster is dark, color
It is homogeneous, it is soft, smooth, scald and fade through high temperature.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should be included in the scope of the protection.
Claims (9)
1. a kind of preparation method of wool flocking thermal underwear face fabric, it is characterised in that the processing method comprises the following steps：
(1) pre-process：Wool skin is subjected to screening and obtains the close fur of quality with impurity elimination；
(2) aerosol hydro-peening：The fur that will be pre-processed through step (1) is clean through aerosol hydro-peening, then through 40-60 DEG C of vacuum drying；
(3) alkali cleaning：The fur cleaned up obtained by step (2) is added into compound alkali lye 2-4 hours are handled at 60-80 DEG C
Afterwards, it is 7 to adjust PH, filters while hot, obtains wool, then will be washed, dried；
(4) wool is added into shredding in mixing willow to mix, then cleaned through scutcher shredding, carding machine cards, spinned and twist
Obtain the wool raw yarn that fineness is 20-35 μm；
(5) dye：Wool raw yarn is added in dyeing cylinder, then dye solution is added toward dyeing in cylinder, is heated to 50-70
DEG C, after insulation dyeing 3-5 hours, tryptophan and color fixing agent are added, continues isothermal holding after 30 minutes, regulation PH is 7, is taken out
Wool raw yarn, after 90-100 DEG C is dried in vacuo 30 minutes, room temperature is cooled to, then through washing 3-5 times, then at 40-60 DEG C of vacuum
Drying obtains fineness and is 20-35 μm of wool yarn, and cuts into the wool lint that length is 1-5mm；
(6) the wool lint obtained by step (5) is made into flocking, acrylic acid makees adhesive, carries out 3-5 electrostatic spinning to base fabric
On layer flocking fabric, then at 110-130 DEG C baking 5-8 minutes, after heat treatment on forming machine, then with blower fan by remain plant
Suede is blown away, then through combing to obtain institute's wool flocking thermal underwear face fabric.
2. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 1, it is characterised in that institute in step (3)
The compound alkali lye stated is made up of following parts by weight component：20-30 parts sodium acid carbonate, 5-10 parts ethylenediamine, 3-5 parts sodium metasilicate,
1-3 parts aminophylline, 1-3 parts alum and 30-40 part water.
3. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 1, it is characterised in that institute in step (3)
The fur and the mass ratio of compound alkali lye stated are 1：10-15.
4. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 1, it is characterised in that institute in step (4)
The dye solution stated is made up of following parts by weight component：20-30 part acidic anionics pigment, 30-40 parts water and 1-3 part hydrotropies
Agent.
5. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 4, it is characterised in that described acidity is cloudy
Ion pigment is selected from least one of acid red, acid black, acid blue, acid ash, acid golden yellow and acid brown.
6. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 4, it is characterised in that described cosolvent
For sodium cetanesulfonate, polyoxyethylene sorbitan monooleate or sorbitan fatty ester.
7. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 1, it is characterised in that institute in step (4)
The color fixing agent stated is cetylpyridinium chloride or brocide.
8. the preparation method of the wool flocking thermal underwear face fabric as described in claim 1 or 7, it is characterised in that in step (4)
Described wool raw yarn, dye solution, the mass ratio of tryptophan and color fixing agent are 1：10-20：0.03-0.05：0.05-0.08.
9. the preparation method of wool flocking thermal underwear face fabric as claimed in claim 1, it is characterised in that institute in step (4)
The material for the bottom cloth layer stated is cotton, acrylic fibers or terylene.
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| CN201710504518.2A CN107361411A (en) | 2017-06-28 | 2017-06-28 | A kind of preparation method of wool flocking thermal underwear face fabric |
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| CN201710504518.2A CN107361411A (en) | 2017-06-28 | 2017-06-28 | A kind of preparation method of wool flocking thermal underwear face fabric |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108078273A (en) * | 2018-01-22 | 2018-05-29 | 孙旭锋 | A kind of horse tail hair sping mattress |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108078273A (en) * | 2018-01-22 | 2018-05-29 | 孙旭锋 | A kind of horse tail hair sping mattress |
| CN108078273B (en) * | 2018-01-22 | 2024-04-02 | 孙旭锋 | Horsetail Mao Danhuang mattress |
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