CN107201644A - The preparation method of chemically-resistant splash inflaming retarding fabric - Google Patents

The preparation method of chemically-resistant splash inflaming retarding fabric Download PDF

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Publication number
CN107201644A
CN107201644A CN201710551194.8A CN201710551194A CN107201644A CN 107201644 A CN107201644 A CN 107201644A CN 201710551194 A CN201710551194 A CN 201710551194A CN 107201644 A CN107201644 A CN 107201644A
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China
Prior art keywords
control
cloth
chemically
padding
fiber
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CN201710551194.8A
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Inventor
钱俊
汤晓兰
曹丽霞
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Changshu Baofeng Special Fiber Co Ltd
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Changshu Baofeng Special Fiber Co Ltd
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Priority to CN201710551194.8A priority Critical patent/CN107201644A/en
Publication of CN107201644A publication Critical patent/CN107201644A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/40—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads
    • D03D15/47—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads multicomponent, e.g. blended yarns or threads
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
    • D03D15/513—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads heat-resistant or fireproof
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
    • D03D15/533—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads antistatic; electrically conductive
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
    • D03D15/54—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads coloured
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
    • D06B3/18—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
    • D06B3/185—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines below the bath level
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C7/00—Heating or cooling textile fabrics
    • D06C7/02—Setting
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C9/00—Singeing
    • D06C9/02—Singeing by flame
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/26—Polymers or copolymers of unsaturated carboxylic acids or derivatives thereof
    • D06M2101/28—Acrylonitrile; Methacrylonitrile
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    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
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    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/34—Polyamides
    • D06M2101/36—Aromatic polyamides
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    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10—Repellency against liquids
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/20—Cellulose-derived artificial fibres
    • D10B2201/22—Cellulose-derived artificial fibres made from cellulose solutions
    • D10B2201/24—Viscose
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    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2321/00—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D10B2321/10—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2321/00—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D10B2321/10—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
    • D10B2321/101—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide modacrylic
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
    • D10B2331/021—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides aromatic polyamides, e.g. aramides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

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  • Mechanical Engineering (AREA)
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Abstract

A kind of preparation method of chemically-resistant splash inflaming retarding fabric, step：One-ply yarn or double strand yarn are spun into by 20 79% comfort type inherent fire-retardant fiber, the composite fibre of 20 79% high fire-retardance inherent fire-retardant fiber and 1 5% antistatic fibre or by the composite fibre of 95 99% high fire-retardance inherent fire-retardant fiber and 1 5% antistatic fibre using the match close spinning process of network, yarn for weaving purpose line is obtained；Yarn for weaving purpose line is weaved, fabric is obtained；Fabric is introduced into rinsing bowl washing, and is dried and is singed under yardage roll debatching state, semi-finished product cloth is obtained；Semi-finished product cloth is introduced into the padding machine equipped with padding liquid to be padded, goes out padding liquor tank and is dried, obtain Final finishing cloth；Final finishing cloth is introduced into forming machine sizing, finished product is obtained.Technical process is brief；With excellent anti-flammability, antistatic behaviour and gas permeability；Ensure the stability of pH value and performance stabilization and color fastness are excellent；Chemically-resistant splash abrasive effect is good and environmentally friendly.

Description

The preparation method of chemically-resistant splash inflaming retarding fabric
Technical field
The invention belongs to textile function fabric preparing technical field, and in particular to a kind of system of chemically-resistant splash inflaming retarding fabric Preparation Method.
Background technology
Foregoing chemically-resistant splash is chemical species splash (as follows).With country pair and labourer's occupational protection Related laws and regulations, the constantly improve of regulations and reinforcing publicity, the labor safety consciousness of self-protection of the whole society is significantly increased, had The market demand for having the weaving face fabric of safeguard function constantly increases, while the requirement to such weaving face fabric is increasingly harsh, specifically Show as implementing protective fabric refinement system, so-called refinement system refers to：Corresponding work(is used for the professional population in different posies The fabric of energy, the protective fabric such as taken as troop operation relatively pays attention to bullet-proof, and for example the protective fabric of fire-entry suit Bias toward anti-flammability, be engaged in for another example oil product (oil depot, gas station) operation crowd dress clothes protective fabric lay particular emphasis on it is anti- Electrostatic, and then the protective fabric of the clothes of such as related to hazardous chemical occupational population is particular about chemically-resistant splash corrosivity, etc. Deng.
As is known in the industry, production, carrying, modulation, repairing or cleaning and dangerous chemical and corrosive goods are engaged in The occupational staff of qualitative correlation is possible to the splash injury by alkali, acid, salt, ester etc in the course of the work, and wearing protective garment can The injury that effectively barrier chemical substance is caused to body, but be due to the weaving face fabric that China corrodes currently for chemically-resistant splash The more other functional fabrics of development technique are for example fire-retardant, anti-static function fabric relatively lags behind, thus foregoing occupational staff dress Protective garment generally uses common fire retardant protective clothing, specific aim shortcoming, it is difficult to meet labour protection safety requirements.
The technical information of anti-chemical splash fabric, such as document A can be seen in disclosed Chinese patent literature) .CN202965373U " the biochemical defence suit fabric " recommended, its structure ecto-entad is followed successively by outer polyurethane coating, polyvinyl alcohol and applied Layer, interior polyurethane coating and continuous synthetic fibre layer, i.e., in the polyamide fibre layer (through fire-retardant tackified finish) for specifically having certain flame retardant effect outside with painting Mode for cloth is coated with interior polyurethane, polyethylene coating and outer layer of polyurethane successively, and the fabric that the patent is recommended is essentially coating Fabric, the dress temporarily during for spraying insecticide is helpful, but be due to airtight, poor durability and lose environmental protection without The garment material for the personnel for being related to the operations such as alkali, acid, the salt and ester dress being preferably mentioned above as applicant；And for example document B a kind of) " processing method of chemically fabric " that .CN104963188A is provided, this method is to purified cotton yarns or polyester The fabric that line is made into examines through base successively, turn over seam, singe, cold dome, short steaming washing, dyeing, wherein dyeing is arranged in again after dyeing Open-width desizing range is washed, and cloth cover pH value is reached 5.5-6.8 and capillary effect >=8cm/min, then carry out successively chemically arrangement, Pre- shrinkage porosite is dried and baked, chemically arrange dressing liquid used by fluorine system water and oil repellent agent PKOBOLNB-NH80-140g/L, Synergist JVA40-60g/L and HAC-pH value conditioning agent 0.3-1.5g/L, the pH value of dressing liquid is 5.5-6.8.Should Although technique effect of the technical scheme that CN104963188A is provided with the 0025th section of record of specification, there is following lack Regret：First, due to the fabric being made into using purified cotton yarns or polyester-cotton blend yarn, and due to purified cotton yarns and polyester-cotton blend yarn in itself And intolerant to strong acid and highly basic, thus be not enough to reach resistance sulfuric acid, hydrochloric acid, nitric acid, caustic soda and anti-adjacent diformazan in nature The purpose of the chemical solvents such as benzene, methanol, acetone, so that fabric is difficult in adapt to environmental requirement complicated and changeable；Second, the fabric Dyed after the completion of weaving, this dyeing needs to consume substantial amounts of water resource, and the dyestuff absorptivity of fabric is low, easily Large effect is produced to environment, the theory of green ecological sustainable development is not met, while dyeing can be to fabric in Final finishing The performances such as strength have a negative impact；Third, it was found from the description of the patent specification full text, because it is used commonly Padding process, thus be difficult to ensure the even results in fabric face film forming, influence chemical defence performance；Fourth, fire-retardant due to lacking With the function such as antistatic, thus there is fastidious property to use occasion, i.e., be equally not suitable with operating environment requirements complicated and changeable.Enter And such as document C) " a kind of anti-chemical reagent fabric and its manufacture method " that .CN105437677A is introduced, it is followed successively by from inside to outside The woven fabric of bamboo charcoal viscose fiber and terylene, PTFE coatings, the composite non-weaving cloth of aramid fiber or glass fibre and Polyphenylene sulfied, PTFE overlay films (the 0006th section and 0018 section of specification), fabric involved by the patent application scheme is essentially composite laminate fabric, Not only make trouble and be difficult to meet industrial amplification production requirement, and woven fabric, composite non-weaving cloth and overlay film pass through Adhesive realizes combination each other, and loses environmental protection using adhesive, and fabric is water-fastness especially involved by the patent application Effect is fragile, for example, there is the anxiety of layering when being put into washing machine cleaning.
For above-mentioned prior art, it is necessary to improved, be this applicant made it is lasting and beneficial repay examination with it is anti- Multiple experiment, forms technical scheme described below finally.
The content of the invention
The task of the present invention is to provide a kind of preparation method of chemically-resistant splash inflaming retarding fabric, the letter of this method processing step It is short, the chemically-resistant splash for meeting industrial amplification production requirement and being obtained by this method is not used by harsh equipment limit Inflaming retarding fabric has lasting and excellent chemically-resistant splash corrosive effect, environmental protection and security ideal, excellent in flame retardance and gone back Take comfortable with good anti-static function and good permeability.
What the task of the present invention was performed by, a kind of preparation method of chemically-resistant splash inflaming retarding fabric, including it is following Step：
A yarn for weaving purpose line) is prepared, uses the match close spinning process of network will be more essential than the comfort type for 20-79% by quality % Fire resistance fibre, 20-79% high fire-retardance inherent fire-retardant fiber and 1-5% antistatic fibre three mixing composite fibre or Person will be more mixed than what both high fire-retardance inherent fire-retardant fibers and 1-5% antistatic fibre for 95-99% were mixed by quality % Condensating fiber is spun into one-ply yarn or double strand yarn, obtains yarn for weaving purpose line；Wherein：Described high fire-retardance inherent fire-retardant fiber and comfortable Type inherent fire-retardant fiber is coloured fiber or dyed colored fibre through original liquid coloring；
B) weave, by by step A) obtained yarn for weaving purpose line weaved by loom, obtains fabric；
C) pre-processing, by by step B) obtained fabric introduces rinsing bowl in the form of yardage roll and washes and control washing warm Degree, control yardage roll rotating speed and control washing time, washing go out rinsing bowl after terminating and carried out successively under yardage roll debatching state Dry and singe, control drying temperature and control cloth speed obtain semi-finished product cloth；
D) Final finishing, by by step C) obtained semi-finished product cloth introduces the padding machine equipped with padding liquid in padding liquor tank and soaked Roll and control padding liquid temperature, control double of finished fabric of padding machine roll compacting power, control semi-finished product cloth gait of march and control Pick-up processed, goes out padding liquor tank and is dried and control drying temperature and control cloth speed, obtain Final finishing cloth, wherein：The leaching The formula of mangle is：Chemical defence auxiliary agent 80-160g/L, synergist 10-40g/L, bleeding agent 0.2-1g/L and fixative 0.5-2g/L；
E) shape, by by step D) obtained Final finishing cloth introduces forming machine and shapes and control after setting temperature and control The gait of march of cloth is arranged, chemically-resistant splash inflaming retarding fabric is obtained.
In the specific embodiment of the present invention, step A) described in comfort type inherent fire-retardant fiber change to be fire-retardant One or more in property viscose rayon, polyacrylic and polyester fiber and flame retardant polyester fiber, described high fire-retardance inherent fire-retardant fiber is Aramid fiber 1313 or Fanglun l414 fiber, described antistatic fibre is Atnistatic neylon fiber, antistatic PET filament or Antistatic acrylic fiber fiber；Described one-ply yarn and the number of double strand yarn are 20-60s.
The present invention another specific embodiment in, step B) described in fabric grammes per square metre be 170-300g/m2, width A width of 1.4-1.6m.
The present invention another specific embodiment in, step C) described in control washing temperature be by washing temperature Control as 60-90 DEG C, described controls yardage roll rotating speed to be to control yardage roll rotating speed to be 20-40rpm, described control washing time It is to control washing time to be 2-3h.
In another specific embodiment of the present invention, step C) described in the temperature dried be 70-90 DEG C, it is described It by cloth speed control is 50-70m/min to control cloth speed to be, described singing is to make cloth with 120-150m/min speed by way of singing The burner of machine and use by burner burn off cloth cover filoplume and floating hair, the temperature of the burner is 180-200 DEG C.
Also have a specific embodiment in the present invention, step D) described in the temperature of control padding liquid be to soak The temperature control of mangle is 25-35 DEG C, and the described roll compacting power for controlling double of finished fabric is will to roll Stress control for 0.02- 0.025MPa, the described gait of march for controlling semi-finished product cloth is to control gait of march to be 30-60m/min, described control Pick-up is to control pick-up to be 60-80%, and described controls drying temperature to be to control drying temperature to be 105-130 DEG C, Described controls cloth speed to be to control cloth speed to be 30-60m/min.
In a still more specific embodiment of the invention, step D) described in pad and two rolled for two leachings.
The present invention so that in a specific embodiment, step D) described in padding liquid be such to prepare, In the padding liquor tank of water is filled, the chemical defence auxiliary agent 80-160g/L is first put into the padding liquor tank and stirred, then will be described Synergist 10-40g/L input padding liquor tanks stir, and then bleeding agent 0.2-1g/L input padding liquor tanks stir, then Fixative 0.5-2g/L input padding liquor tanks are stirred, padding liquid is obtained.
Described chemical defence auxiliary agent is the anti-soda acid finishing agents of FHA, institute in yet a further embodiment of the present invention The synergist stated is Link synergist, and described bleeding agent permeates wetting agent for DN, and described fixative is WBL fixatives.
The present invention again so that a specific embodiment in, step E) described in control setting temperature be to shape Temperature control is 130-150 DEG C, and the described gait of march for controlling Final finishing cloth is to be by the gait of march control of Final finishing cloth 20-40m/min。
One of technique effect of technical scheme that the present invention is provided, because technical process is briefly and without extreme harsh work Skill requires and need not relied on special equipment, thus can meet industrial amplification production requirement；Two, used due to selecting by matching Comfort type inherent fire-retardant fiber, high fire-retardance inherent fire-retardant fiber and antistatic fibre three mixing that the close spinning process of network is obtained The yarn that is made of composite fibre, or the composite fibre mixed by both high fire-retardance inherent fire-retardant fiber and antistatic fibre The yarn being made, thus with excellent anti-flammability, antistatic behaviour and gas permeability；Three, because comfort type inherent flame retardant is fine Peacekeeping high fire-retardance inherent fire-retardant fiber selects the coloured fiber or dyed coloured fibre used and coloured through source liquid, thus can ensure that The stability of pH value during Final finishing and the stabilization and excellent color fastness for contributing to fiber self performance；Four, Due to padding liquid is made by the rational chemical defence auxiliary agent of the amount of selecting, synergist, bleeding agent and fixative, thus it can ensure what is finally given Fabric has excellent chemically-resistant splash abrasive effect and embodies ultimate attainment environmental safety.
Embodiment
Embodiment 1：
A) prepare yarn for weaving purpose line, use match the close spinning process of network by the quality % through original liquid coloring than for 19% it is fire-retardant Polyacrylic and polyester fiber and quality % that flame retardant polyester fiber that modified viscose fiber, quality % ratios are 40%, quality % ratios are 20% The composite fibre that the antistatic PET filament for being 1% than the aramid fiber 1313 for 20% and quality % ratios is mixed is spun into 20S one-ply yarn, obtains yarn for weaving purpose line, flame-retardant modified viscose rayon, the flame-resistant terylene of the original liquid coloring described in this step Fiber, polyacrylic and polyester fiber and aramid fiber 1313 refer to that fiber adds Masterbatch in spinning process in itself, without entering again The fiber of row dyeing, can both reduce later process, and can reduce the influence to environment, and original liquid coloring fiber can pass through commercially available channel Obtain；
B) weave, by by step A) obtained yarn for weaving purpose line weaved by rapier loom, obtains gram weight for 300g/m2 And breadth is 1.5m fabric；
C) pre-process, will be by step B) obtained fabric introduces the washing of overflow-type rinsing bowl in the form of yardage roll, and washing is warm Degree control is 60 DEG C, and the control of yardage roll rotating speed is 40rpm, and washing time control is 2h, draws fabric after washing terminates and washes Groove and debatching state and control cloth speed 50m/min speed under introducing drying unit such as drying machine drying, drying temperature For 70 DEG C, go out dryer and be transferred to gassing frame to singe, cloth is used with 150m/min speed by way of the burner of gassing frame by fire Mouth burn off cloth cover filoplume and floating hair, the burner temperature of the gassing frame is 190 DEG C, obtains semi-finished product cloth；
D) Final finishing, by by step C) obtained semi-finished product cloth introduces the padding machine equipped with padding liquid in padding liquor tank and soaked Roll, pad number of times and rolled for twice i.e. two leachings two, the temperature control of foregoing padding liquid is 30 DEG C, and the roll compacting power padded is i.e. to semi-finished product The Stress control that rolls of cloth is 0.02MPa, and the gait of march control of cloth is 60m/min, and pick-up control is 60%, goes out padding liquor tank and draws Enter dryer to be dried, drying temperature control is 105 DEG C, cloth speed control is 45m/min, is obtained in Final finishing cloth, this step The formula of described padding liquid is：Tried to win favour that Chemical Co., Ltd. of section produces by Guangdong province, China Dongguan and proposed in the application The trade mark in market sale was the anti-soda acid finishing agent 160g/L of FHA, produced by Shanghai Shanghai Yi Ke Chemical Co., Ltd.s in the past And the trade mark in market sale before the application proposition is Link synergist 10g/L, equally by Guangdong province, China's Dongguan City The trade mark that En Ke Chemical Co., Ltd.s produce and in market sale before the application proposition is DN infiltration wetting agents 0.6g/ L and by Jiangsu Province, China Suzhou City Xin Li chemical industry Co., Ltd produce and the application proposition before in market sale The trade mark be WBL fixative 2g/L, the preparation process of padding liquid is：The anti-soda acid finishing agent 160g/L of FHA are first put into padding liquor tank And stir, then Link synergist 10g/L is put into padding liquor tank and stirred, DN is then permeated into wetting agent 0.6g/L and thrown Enter padding liquor tank and stir, WBL fixatives 2g/L is then put into padding liquor tank and stirred；
E) shape, will be by step D) obtained Final finishing cloth introduces forming machine sizing, and setting temperature is 150 DEG C, and cloth speed is 20m/min, goes out forming machine, obtains chemically-resistant splash inflaming retarding fabric.
Embodiment 2：
A) prepare yarn for weaving purpose line, use match the close spinning process of network by dyed quality % than for 20% it is flame-retardant modified The antistatic PET filament that the Fanglun l414 fiber and quality % ratios that viscose rayon and quality % ratios are 75% are 5% is mixed Composite fibre be spun into 60S double strand yarn, obtain yarn for weaving purpose line；
B) weave, by by step A) obtained yarn for weaving purpose line weaved by rapier loom, obtains gram weight for 170g/m2 And breadth is 1.6m fabric；
C) pre-process, will be by step B) obtained fabric introduces the washing of overflow-type rinsing bowl in the form of yardage roll, and washing is warm Degree control is 90 DEG C, and the control of yardage roll rotating speed is 30rpm, and washing time control is 3h, draws fabric after washing terminates and washes Groove and debatching state and control cloth speed 70m/min speed under introducing drying unit such as drying machine drying, drying temperature For 90 DEG C, go out dryer and be transferred to gassing frame to singe, cloth is used with 135m/min speed by way of the burner of gassing frame by fire Mouth burn off cloth cover filoplume and floating hair, the burner temperature of the gassing frame is 180 DEG C, obtains semi-finished product cloth；
D) Final finishing, by by step C) obtained semi-finished product cloth introduces the padding machine equipped with padding liquid in padding liquor tank and soaked Roll, pad number of times and rolled for twice i.e. two leachings two, the temperature control of foregoing padding liquid is 25 DEG C, and the roll compacting power padded is i.e. to semi-finished product The Stress control that rolls of cloth is 0.05MPa, and the gait of march control of cloth is 30m/min, and pick-up control is 80%, goes out padding liquor tank and draws Enter dryer to be dried, drying temperature control is 130 DEG C, cloth speed control is 30m/min, is obtained in Final finishing cloth, this step The formula of described padding liquid is：Tried to win favour that Chemical Co., Ltd. of section produces by Guangdong province, China Dongguan and proposed in the application The trade mark in market sale was the anti-soda acid finishing agent 120g/L of FHA, produced by Shanghai Shanghai Yi Ke Chemical Co., Ltd.s in the past And the trade mark in market sale before the application proposition is Link synergist 40g/L, equally by Guangdong province, China's Dongguan City The trade mark that En Ke Chemical Co., Ltd.s produce and in market sale before the application proposition is DN infiltration wetting agents 0.2g/ L and by Jiangsu Province, China Suzhou City Xin Li chemical industry Co., Ltd produce and the application proposition before in market sale The trade mark be WBL fixative 1.2g/L, the preparation process of padding liquid is：The anti-soda acid finishing agent 120g/L of FHA are first put into mangle Groove is simultaneously stirred, then Link synergist 40g/L is put into padding liquor tank and stirred, and DN then is permeated into wetting agent 0.2g/L Input padding liquor tank is simultaneously stirred, and WBL fixatives 1.2g/L then is put into padding liquor tank and stirred；
E) shape, will be by step D) obtained Final finishing cloth introduces forming machine sizing, and setting temperature is 130 DEG C, and cloth speed is 30m/min, goes out forming machine, obtains chemically-resistant splash inflaming retarding fabric.
Embodiment 3：
A yarn for weaving purpose line) is prepared, will be through original liquid coloring using the match close spinning process of network (with the explanation to embodiment 1) The aramid fiber 1313 and quality % ratios that the flame retardant polyester fiber and quality % ratios that quality % ratios are 48% are 49% are 3% The composite fibre that antistatic PET filament is mixed is spun into 30S double strand yarn, obtains yarn for weaving purpose line；
B) weave, by by step A) obtained yarn for weaving purpose line weaved by rapier loom, obtains gram weight for 240g/m2 And breadth is 1.4m fabric；
C) pre-process, will be by step B) obtained fabric introduces the washing of overflow-type rinsing bowl in the form of yardage roll, and washing is warm Degree control is 75 DEG C, and the control of yardage roll rotating speed is 20rpm, and washing time control is 2.5h, and fabric is drawn into water after washing terminates Washing trough simultaneously introduces drying unit such as drying machine drying in debatching state and under control cloth speed 60m/min speed, dries temperature Spend for 80 DEG C, go out dryer and be transferred to gassing frame to singe, make cloth with 120m/min speed by way of the burner of gassing frame use by Burner burn off cloth cover filoplume and floating hair, the burner temperature of the gassing frame is 200 DEG C, obtains semi-finished product cloth；
D) Final finishing, by by step C) obtained semi-finished product cloth introduces the padding machine equipped with padding liquid in padding liquor tank and soaked Roll, pad number of times and rolled for twice i.e. two leachings two, the temperature control of foregoing padding liquid is 35 DEG C, and the roll compacting power padded is i.e. to semi-finished product The Stress control that rolls of cloth is 0.022MPa, and the gait of march control of cloth is 45m/min, and pick-up control is 70%, goes out padding liquor tank Introduce dryer to be dried, drying temperature control is 120 DEG C, cloth speed control is 60m/min, obtains Final finishing cloth, this step Described in the formula of padding liquid be：Tried to win favour that Chemical Co., Ltd. of section produces by Guangdong province, China Dongguan and carried in the application Go out and be the anti-soda acid finishing agent 80g/L of FHA, produced by Shanghai Shanghai Yi Ke Chemical Co., Ltd.s in the trade mark of market sale in the past And the trade mark in market sale before the application proposition is Link synergist 25g/L, equally by Guangdong province, China's Dongguan City The trade mark that En Ke Chemical Co., Ltd.s produce and in market sale before the application proposition is DN infiltration wetting agents 1g/L With it is being produced by Jiangsu Province, China Suzhou City Xin Li chemical industry Co., Ltd and the application proposition before in market sale The trade mark be WBL fixative 0.5g/L, the preparation process of padding liquid is：The anti-soda acid finishing agent 80g/L of FHA are first put into padding liquor tank And stir, then Link synergist 25g/L is put into padding liquor tank and stirred, DN then is permeated into wetting agent 1g/L puts into Padding liquor tank is simultaneously stirred, and WBL fixatives 0.5g/L then is put into padding liquor tank and stirred；
E) shape, will be by step D) obtained Final finishing cloth introduces forming machine sizing, and setting temperature is 140 DEG C, and cloth speed is 40m/min, goes out forming machine, obtains chemically-resistant splash inflaming retarding fabric.
Embodiment 4：
Only by step A) in raw material and its quality % ratios be changed to 95% aramid fiber 1313 and quality % ratios be 5% Antistatic fibre, remaining is with the description to embodiment 1.
Embodiment 5：
Only by step A) in raw material and its quality % ratios be changed to 99% Fanglun l414 and quality % than for 1% it is anti- Electrostatic fibre, remaining is with the description to embodiment 2.
Implement 6：
Only by step A) in raw material and its quality % ratios be changed to 97% aramid fiber 1313 and quality % ratios be 3% Antistatic fibre, remaining is with the description to embodiment 3.
Chemically-resistant splash inflaming retarding fabric is obtained as above-described embodiment 1 to 6 after tested with the technique effect shown in following table：
In addition, according to the standard testings of EN 13034, the chemically-resistant splash inflaming retarding fabric that the present embodiment 1 to 6 is obtained can expire Sufficient standard requirement, specifically as shown in following table：

Claims (10)

1. a kind of preparation method of chemically-resistant splash inflaming retarding fabric, it is characterised in that comprise the following steps：
A yarn for weaving purpose line) is prepared, uses the match close spinning process of network will be more fine than the comfort type inherent flame retardant for 20-79% by quality % The composite fibre of the antistatic fibre three mixing of dimension, 20-79% high fire-retardance inherent fire-retardant fiber and 1-5% will be by matter Amount % is spun into than the composite fibre that both high fire-retardance inherent fire-retardant fibers and 1-5% antistatic fibre for 95-99% are mixed One-ply yarn or double strand yarn, obtain yarn for weaving purpose line；Wherein：Described high fire-retardance inherent fire-retardant fiber and comfort type inherent flame retardant are fine Tie up as the coloured fiber through original liquid coloring or dyed colored fibre；
B) weave, will be by step A）Obtained yarn for weaving purpose line is weaved by loom, obtains fabric；
C) pre-process, will be by step B）Obtained fabric introduced in the form of yardage roll rinsing bowl wash and control washing temperature, Yardage roll rotating speed and control washing time are controlled, washing goes out rinsing bowl after terminating and dried successively under yardage roll debatching state With singe, control drying temperature and control cloth speed, obtain semi-finished product cloth；
D) Final finishing, will be by step C）Obtained semi-finished product cloth introduces the padding machine equipped with padding liquid in padding liquor tank and padded simultaneously And the temperature of control padding liquid, the roll compacting power for controlling double of finished fabric of padding machine, the gait of march of control semi-finished product cloth and control are rolled Remaining rate, goes out padding liquor tank and is dried and control drying temperature and control cloth speed, obtain Final finishing cloth, wherein：The padding liquid Formula be：Chemical defence auxiliary agent 80-160g/L, synergist 10-40g/L, bleeding agent 0.2-1g/L and fixative 0.5-2g/L；
E) shape, will be by step D）Obtained Final finishing cloth introduces forming machine and shapes and control setting temperature and control Final finishing The gait of march of cloth, obtains chemically-resistant splash inflaming retarding fabric.
2. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step A）Described in Comfort type inherent fire-retardant fiber be flame-retardant modified viscose rayon, polyacrylic and polyester fiber and flame retardant polyester fiber in one kind or several Kind, described high fire-retardance inherent fire-retardant fiber is aramid fiber 1313 or Fanglun l414 fiber, and described antistatic fibre is anti- Electrostatic nylon fiber, antistatic PET filament or antistatic acrylic fiber fiber；Described one-ply yarn and the number of double strand yarn are 20- 60s。
3. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step B）Described in The grammes per square metre of fabric is 170-300g/m2, breadth is 1.4-1.6m.
4. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step C）Described in Control washing temperature be by washing temperature control be 60-90 DEG C, it is described to control yardage roll rotating speed to be to be by the control of yardage roll rotating speed 20-40rpm, described controls washing time to be to control washing time to be 2-3h.
5. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step C）Described in The temperature of drying is 70-90 DEG C, it is described control cloth speed be by cloth speed control be 50-70m/min, described singing be make cloth with 120-150m/min speed is used by burner burn off cloth cover filoplume and floating hair, the temperature of the burner by way of the burner of gassing frame Spend for 180-200 DEG C.
6. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step D）Described in The temperature for controlling padding liquid be by the temperature control of padding liquid be 25-35 DEG C, the roll compacting power of described double of finished fabric of control It is that will roll Stress control for 0.02-0.025MPa, the described gait of march for controlling semi-finished product cloth is to be by gait of march control 30-60m/min, described controls pick-up to be to control pick-up to be 60-80%, and described control drying temperature is to dry Temperature control is 105-130 DEG C, and described controls cloth speed to be to control cloth speed to be 30-60m/min.
7. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step D）Described in Pad and two rolled for two leachings.
8. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step D）Described in Padding liquid be such to prepare, in the padding liquor tank of water is filled, first will the chemical defence auxiliary agent 80-160g/L put into described in roll Liquid bath is simultaneously stirred, then synergist 10-40g/L input padding liquor tanks are stirred, then by bleeding agent 0.2-1g/L Input padding liquor tank stirs, and then fixative 0.5-2g/L input padding liquor tanks stir, padding liquid is obtained.
9. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 8, it is characterised in that described chemical defence is helped Agent is the anti-soda acid finishing agents of FHA, and described synergist is Link synergist, and described bleeding agent permeates wetting agent for DN, described Fixative be WBL fixatives.
10. the preparation method of chemically-resistant splash inflaming retarding fabric according to claim 1, it is characterised in that step E）Described in Control setting temperature be by setting temperature control be 130-150 DEG C, the gait of march of described control Final finishing cloth is will be rear The gait of march control for arranging cloth is 20-40m/min.
CN201710551194.8A 2017-07-07 2017-07-07 The preparation method of chemically-resistant splash inflaming retarding fabric Pending CN107201644A (en)

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