CN107157781A - A kind of single-layer graphene repair membrane and preparation method - Google Patents
A kind of single-layer graphene repair membrane and preparation method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention relates to single-layer graphene repair membrane and preparation method field, a kind of single-layer graphene repair membrane and preparation method are disclosed, the raw material and weight ratio that single-layer graphene is repaired in film formulation are respectively：0.05 7.2 parts of single-layer graphene, 45 83.8 parts of water, 5 10 parts of Essence, 0 4.5 parts of magnesium carbonate, 0 3.2 parts of calcium carbonate, 0 1.5 parts of quaternary ammonium salt surface active agent.It is single-layer graphene repair membrane muting sensitive that the present invention is provided, safe efficient, harmless.Quickly bring nutritional ingredient needed for skin into skin deep layer and while metabolism rubbish, reaches the highest effect of maintenance, safeguard skin health.
Description
Technical field
The present invention relates to single-layer graphene repair membrane and preparation method field, more particularly to a kind of single-layer graphene repair membrane
And preparation method.
Background technology
It is new that British scientist in 2004 has prepared that the monoatomic layer connected by carbon atom with sp2 hydridization constituted first
Two-dimensional atomic crystal-graphene, its thickness only has 0.3354nm, is to find most thin material in the world at present.Graphene oxide
With low cost, raw material is easy to get, with good physical and chemical properties, such as higher specific surface energy, good hydrophily, good
Absorption property, and have preferable dispersiveness in water and organic solvent, be a kind of excellent composite filler.
Composite, is by two or more material of different nature, by method physically or chemically, in macroscopic view
Material of the composition with new capability on (microcosmic).Various materials make up for each other's deficiencies and learn from each other in performance, produce cooperative effect, make to be combined
The combination property of material is better than former composition material and meets a variety of requirements.Facial mask of the prior art, penetration is not strong,
Skin is absorbed less than application, after use time is long, easily causes skin loss.
The content of the invention
The present invention provides a kind of single-layer graphene repair membrane and preparation method, solves facial mask in the prior art, penetration is not
By force, skin is absorbed less than application, after use time is long, easily causes the technical problem of skin loss.
The purpose of the present invention is achieved through the following technical solutions：
Raw material and weight ratio in a kind of single-layer graphene repair membrane, formula are respectively：0.05-7.2 parts of single-layer graphene, water
45-83.8 parts, 5-10 parts of Essence, 0-4.5 parts of magnesium carbonate, 0-3.2 parts of calcium carbonate, 0-1.5 parts of quaternary ammonium salt surface active agent.
A kind of preparation method of single-layer graphene repair membrane, including：
The preparation of mono-layer graphite aqueous solution：Single-layer graphene is scattered in the aqueous solution under ultrasonication, ultrasonic time：5-
15min, temperature：10-55℃；
It is prepared by Essence：It will be added under the Essence stirring condition of ingredients weight parts in mono-layer graphite aqueous solution, temperature：20-
35 DEG C, time：25-45min；
At room temperature, magnesium carbonate, calcium carbonate and the quaternary ammonium salt surface active agent of respective components are added, is well mixed, it is equal through high pressure
Matter machine homogeneous, packaging is finished product.
The present invention provides a kind of single-layer graphene repair membrane and preparation method, and single-layer graphene repairs the raw material in film formulation
And weight ratio is respectively：0.05-7.2 parts of single-layer graphene, 45-83.8 parts of water, 5-10 parts of Essence, 0-4.5 parts of magnesium carbonate, carbon
Sour calcium 0-3.2 parts, 0-1.5 parts of quaternary ammonium salt surface active agent.Single-layer graphene repair membrane muting sensitive that the present invention is provided, safety,
Efficiently, it is harmless.Quickly bring nutritional ingredient needed for skin into skin deep layer and while metabolism rubbish, reaches the most efficient of maintenance
Really, skin health is safeguarded.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to institute in embodiment
The accompanying drawing needed to use is briefly described, it should be apparent that, drawings in the following description are only some implementations of the present invention
Example, for those of ordinary skill in the art, without having to pay creative labor, can also be obtained according to these accompanying drawings
Obtain other accompanying drawings.
Fig. 1 is a kind of flow chart of the preparation method of single-layer graphene repair membrane of the embodiment of the present invention.
Embodiment
In order to facilitate the understanding of the purposes, features and advantages of the present invention, it is below in conjunction with the accompanying drawings and specific real
Applying mode, the present invention is further detailed explanation.
Raw material and weight ratio in a kind of single-layer graphene repair membrane provided in the embodiment of the present invention, formula are respectively：
0.05-7.2 parts of single-layer graphene, 45-83.8 parts of water, 5-10 parts of Essence, 0-4.5 parts of magnesium carbonate, 0-3.2 parts of calcium carbonate, season
0-1.5 parts of ammonium type surfactant.
Wherein, the average thickness of the single-layer graphene is 0.5-5.5nm, and sheet size is 1-50 μm.
The composition of the Essence and corresponding parts by weight are that tower draws tree seed germ extract 2.3-2.5, compound marine alga
Extract 4.9-5.1, moon peach leaf plant extract 0.23-0.27, moon peach leaf plant extract 0.09-0.11, Thunder God and take root in extract
1~10, Single Roxburgh Rose Fruit extract thing 0.19-0.21, Chinese juniper another name for oil 2.95-3.05.
The composition of the Essence and corresponding parts by weight are that Chinese aloe leaf plants extract 2-2.3, natural seaweed sugar 4-5, rose
Rare liquid distilled from honeysuckle flowers or lotus leaves 0.5-0.73, water lock magnetite 0.1-0.31, NMF 1~6, sodium hyaluronate 2.95-3.05.
The present invention plays graphene as the leading superiority of new material, by flesh using graphene as carrier, using biotechnology as support
Nutritional ingredient needed for skin quickly brings skin deep layer into and while metabolism rubbish, reaches the effect of maintenance.Use natural plants simultaneously
Extract be main component, developed using high pressure low temperature.Single-layer graphene repair membrane muting sensitive that the present invention is provided, peace
Entirely, it is efficient, harmless.Quickly bring nutritional ingredient needed for skin into skin deep layer and while metabolism rubbish, reaches the highest of maintenance
Effect, safeguards skin health.
The repair membrane of different efficacies can be formed by the composition for changing Essence, for example：
（1）The constituent of light speckles, beautification and white smoothing wrinkle anti-aging repair membrane is as follows：
Tower draws the function of tree seed germ extract to be mainly that dual whitening, color spot subtract formation that is light, suppressing melanoblast；
The function of compound marine alga extract is mainly light scar, pore refining, sun-proof whitening；
The function that Taiwan month peach leaf plants extract is mainly delay aging；
The function that Thunder God takes root in extract is mainly treatment skin ulcer；
The function of Single Roxburgh Rose Fruit extract thing is mainly anti-aging：Contain superoxide dismutase (SOD)；
The function of peculiar Chinese juniper another name for oil is mainly promotion skin metabolism and pre- anti-aging, the colour of skin be not naturally ruddy obscure.
（2）The sun-proof constituent for repairing repair membrane of water lock is as follows：
The function that Chinese aloe leaf plants extract is mainly white moisturizing oil control and acne removal；It is toxin-expelling and face nourishing, sun-proof；
The function of natural seaweed sugar is mainly to keep cell viability and large biological molecule, form diaphragm；
The function of rose liquid distilled from honeysuckle flowers or lotus leaves be mainly heat-clearing disappear fire, beautifying face and moistering lotion；
The function of water lock magnetite is mainly to repair epidermal layer cells, lifting skin moisturizing ability；
The function of NMF is mainly the adsorptivity water-soluble substances of the moisture-keeping function in skin cuticula；
The function of sodium hyaluronate is mainly water lock moisturizing, carries more than 500 times of moisture.
As shown in figure 1, be a kind of preparation method of single-layer graphene repair membrane provided in an embodiment of the present invention, including：
The preparation of step 101, mono-layer graphite aqueous solution：Single-layer graphene is scattered in the aqueous solution under ultrasonication, ultrasound
Time：5-15min, temperature：10-55℃；
It is prepared by step 102, Essence：It will be added under the Essence stirring condition of ingredients weight parts in mono-layer graphite aqueous solution,
Temperature：20-35 DEG C, time：25-45min；
Step 103, at room temperature, adds magnesium carbonate, calcium carbonate and the quaternary ammonium salt surface active agent of respective components, is well mixed,
Through high pressure homogenizer homogeneous, packaging is finished product.
Wherein, step 102 can specifically include：
Step 102-1, tree seed germ extract 2.3-2.5, compound marine alga extract 4.9-5.1, moon peach leaf is drawn to plant and extract the tower
Take liquid 0.23-0.27, moon peach leaf to plant extract 0.09-0.11, Thunder God and take root in extract 1~10, Single Roxburgh Rose Fruit extract thing 0.19-
0.21st, Chinese juniper another name for oil 2.95-3.05 miscellas by weight proportion are added in pot, stir equal after being heated to 35 ± 2 DEG C of whole thawings
It is even, homogeneous 30 ± 5 minutes；
Step 102-2, treated material body is stirred under -0.02Mpa vacuum conditions mix and add after kaolin
Matter is handled 10-20 minutes, when being then cooled to 45 DEG C, is added flavor of raw material and is well mixed；
Step 102-3, continue to cool to 40 DEG C；Material body is filtered by 80 mesh；
Step 102-4, take supernatant.
Stoste level repair membrane prepared by the embodiment of the present invention, belongs to small molecule structure, cooperation single-layer graphene is carrier, is oozed
It is thoroughly fast, easily absorb, with repairing, moisten, releive, whitening, nti-freckle, smoothing wrinkle, reparation, cytothesis the effects such as, increase skin is supported
Drag, make skin get well it is moist, delicate it is net white, radiate the vigour of youth brilliance of having no time
The present invention is described in detail above, specific case used herein is entered to the principle and embodiment of the present invention
Elaboration is gone, the explanation of above example is only intended to the method and its core concept for helping to understand the present invention；Simultaneously for this
The those skilled in the art in field, according to the thought of the present invention, will change in specific embodiments and applications,
In summary, this specification content should not be construed as limiting the invention.
Claims (6)
1. a kind of single-layer graphene repair membrane, it is characterised in that raw material and weight ratio in formula are respectively：Single-layer graphene
0.05-7.2 parts, 45-83.8 parts of water, 5-10 parts of Essence, 0-4.5 parts of magnesium carbonate, 0-3.2 parts of calcium carbonate, quaternary ammonium salt surface
0-1.5 parts of activating agent.
2. single-layer graphene repair membrane according to claim 1, it is characterised in that the average thickness of the single-layer graphene
For 0.5-5.5nm, sheet size is 1-50 μm.
3. single-layer graphene repair membrane according to claim 2, it is characterised in that the composition of the Essence and corresponding
Parts by weight are that tower draws tree seed germ extract 2.3-2.5, compound marine alga extract 4.9-5.1, moon peach leaf to plant extract 0.23-
0.27th, moon peach leaf plant extract 0.09-0.11, Thunder God take root in extract 1~10, Single Roxburgh Rose Fruit extract thing 0.19-0.21, Chinese juniper wood
Essential oil 2.95-3.05.
4. single-layer graphene repair membrane according to claim 2, it is characterised in that the composition of the Essence and corresponding
Parts by weight be Chinese aloe leaf plant extract 2-2.3, natural seaweed sugar 4-5, rose liquid distilled from honeysuckle flowers or lotus leaves 0.5-0.73, water lock magnetite 0.1-0.31,
NMF 1~6, sodium hyaluronate 2.95-3.05.
5. a kind of preparation method of single-layer graphene repair membrane, it is characterised in that including：
The preparation of mono-layer graphite aqueous solution：Single-layer graphene is scattered in the aqueous solution under ultrasonication, ultrasonic time：5-
15min, temperature：10-55℃；
It is prepared by Essence：It will be added under the Essence stirring condition of ingredients weight parts in mono-layer graphite aqueous solution, temperature：20-
35 DEG C, time：25-45min；
At room temperature, magnesium carbonate, calcium carbonate and the quaternary ammonium salt surface active agent of respective components are added, is well mixed, it is equal through high pressure
Matter machine homogeneous, packaging is finished product.
6. the preparation method of single-layer graphene repair membrane according to claim 5, it is characterised in that prepared by the Essence
The step of, specifically include：
Tree seed germ extract 2.3-2.5, compound marine alga extract 4.9-5.1, moon peach leaf is drawn to plant extract 0.23- in tower
0.27th, moon peach leaf plant extract 0.09-0.11, Thunder God take root in extract 1~10, Single Roxburgh Rose Fruit extract thing 0.19-0.21, Chinese juniper wood
Essential oil 2.95-3.05 miscellas by weight proportion are added in pot, are stirred after being heated to 35 ± 2 DEG C of whole thawings, homogeneous 30
± 5 minutes；
Treated material body is stirred under -0.02Mpa vacuum conditions and mixes and add homogenization 10- after kaolin
20 minutes, when being then cooled to 45 DEG C, add flavor of raw material and be well mixed；
Continue to cool to 40 DEG C；Material body is filtered by 80 mesh；
Take supernatant.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710460866.4A CN107157781A (en) | 2017-06-18 | 2017-06-18 | A kind of single-layer graphene repair membrane and preparation method |
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| CN201710460866.4A CN107157781A (en) | 2017-06-18 | 2017-06-18 | A kind of single-layer graphene repair membrane and preparation method |
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| Publication Number | Publication Date |
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| CN107157781A true CN107157781A (en) | 2017-09-15 |
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ID=59820348
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710460866.4A Pending CN107157781A (en) | 2017-06-18 | 2017-06-18 | A kind of single-layer graphene repair membrane and preparation method |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104490702A (en) * | 2014-12-24 | 2015-04-08 | 杭州菲丝凯化妆品有限公司 | Herbal mask taking plant extract as anticorrosive antibacterial additive |
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
| CN106038324A (en) * | 2016-05-19 | 2016-10-26 | 燕园众欣纳米科技（北京）有限公司 | Preparation method of graphene heating facial mask |
-
2017
- 2017-06-18 CN CN201710460866.4A patent/CN107157781A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104490702A (en) * | 2014-12-24 | 2015-04-08 | 杭州菲丝凯化妆品有限公司 | Herbal mask taking plant extract as anticorrosive antibacterial additive |
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105997572A (en) * | 2016-05-19 | 2016-10-12 | 曾新民 | Cleansing milk containing nano graphene and preparation method thereof |
| CN106038324A (en) * | 2016-05-19 | 2016-10-26 | 燕园众欣纳米科技（北京）有限公司 | Preparation method of graphene heating facial mask |
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Application publication date: 20170915 |