CN104490702A - Herbal mask taking plant extract as anticorrosive antibacterial additive - Google Patents
Herbal mask taking plant extract as anticorrosive antibacterial additive Download PDFInfo
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Abstract
The invention relates to a herbal mask taking a plant extract as an anticorrosive antibacterial additive and aims at providing a mask with the effect of effectively nursing the facial skin. According to the technical scheme, the herbal mask taking the plant extract as the anticorrosive antibacterial additive comprises the following components: glyceryl polyether-26 and the like. The method for preparing the herbal mask taking the plant extract as the anticorrosive antibacterial additive comprises the following steps: (1) soaking the raw materials in advance until the materials are completely dissolved, heating and sterilizing; (2) heating, totally melting the materials, and uniformly stirring; (3) stirring and mixing the materials treated in the steps (1) and (2) under vacuum conditions, adding kaolin, homogenizing, reducing the temperature, adding essence raw materials, and uniformly mixing; (4) continuously cooling, and filtering the materials by virtue of an 80-mesh sieve; and (5) sampling and checking. The method for preparing the traditional Chinese medicine extract comprises the following steps: (1) mixing the raw materials according to the ratio; (2) obtaining the supernatant and separating out the extract; and (3) performing vacuum drying on the supernatant and the separated extract, thereby obtaining the dried extract.
Description
Technical field
The present invention relates to facial film of a kind of cosmetic field and preparation method thereof, particularly relate to a kind of with Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici be antisepsis and sterilization additive draft facial film and preparation method.
Background technology
The mask product of selling in the market, its material composition is a multitude of names according to kind difference on market, divides, can be divided into tear-pull facial film, blending paste film, cream profile film, fresh fruit self-made face pack, face patch profile film according to quality.The nutritional labelings such as deep-sea mud, various mineral, plants essential oil generally can be added in blending cream pack.It can not only effective cleaning skin, and moisture can be utilized to soften be blocked in the sclerosis sebum of pore mouth, makes acne and blackhead be pulled out easily.But in order to preserve the effective ingredient of wherein nutrient substance, often in product, add more sterilization antiseptic.And sterilization antiseptic is the main cause causing skin allergy.
Countries in the world have carried out limiting using to traditional preservatives antibacterial, as Ministry of environment of Denmark announces in December in 2010 on the 20th, will forbid that 3 years old to contain p-Hydroxybenzoate in purgation juvenile product.2011.5.4 French Lower House votes through one and forbids that product contains three motion of class chemical substance of o-benzoic acid salt, p-Hydroxybenzoate and alkyl phenol.2014.1 European Union newly advise, and are deleted by triclosan from regulation No1223/2009 annex V, and limit it and use as cosmetics preservative.Also prohibit the antiseptic that oxybenzene isobutyl ester etc. 5 kinds does not have security evaluation data simultaneously.
By stimulating anaphylaxis clinical investigation to antiseptic, 1937 patients are tested, to analyze the probability that series of standards antiseptic causes Contact hyper sensitization at 2000-2005 Nofer institute ofOccupation Medicine.(thimerosal, EuxylK400, formaldehyde, KathonCG, Quatemium 15, parabens) Preservative Technology for Personal Care 27 kinds, wherein 16 kinds can cause a positive reaction with other chemical substances.EuxylK400 is verified is anaphylactogen main in this serial cosmetics, causes the positive reaction of 21 (18.6%) name patients, but the patient of 17.7% can produce positive reaction to thimerosal simultaneously.The anaphylaxis patch test of cosmetics preservative, wherein 43.4% tester, at least one patch test presents the positive.Therefore market is studied low irritant antiseptic in recent years, doses 1,2-alkane diol and replace parabens in cosmetics.Propose without adding concept, simultaneously also as selling point.
For the consideration of safety, uphold nature, in recent years, along with the progressively enhancing of the health perception of people, the report adding cosmetics as additive by plant increased gradually, as Radix Ginseng, Aloe but be mostly used to such as to brighten at the effect improving skin.
It is the Pure natural mask that raw material makes that Chinese invention patent CN103110565A invention relates to Chinese medicine, by all kinds of medical herbs pulverizing, the Pure natural mask that inventing provides is light pale powder, to improve face pigmentation heavy, have acne or acne, little pimple effective, but this facial film use procedure inconvenience.CN201410241891 invention relates to a kind of pure natural nonirritant facial film and preparation method thereof, after using, there is skin oxygen supply, whitening simultaneously, brighten, anti-acne, speckle dispelling (except genetic), skin moisture-keeping and effect such as convergence pore etc., superfluous sebum secretion can also be suppressed.But foregoing invention Chinese herbal medicine used is all simple for improving the effect of skin.
In view of this, develop a kind of safety and environmental protection, good product quality and using plant as anticorrosion and bactericidal agent, for the cosmetics produced without adding zest antiseptic, and its industrialization is just seemed be even more important, its extensive use in cosmetic field can be played like this, meet the need of market.
Summary of the invention
The object of the invention is to overcome above-mentioned the deficiencies in the prior art, thering is provided a kind of take plant extract as the draft facial film of antisepsis and sterilization additive, this facial film should possess the effect of effectively nursing skin of face, can not health risk, and the quality guarantee period meets the regulation of national standard completely.
Technical scheme provided by the invention is: the draft facial film taking plant extract as antisepsis and sterilization additive, and the composition comprised and corresponding weight portion are:
Glycerin polyether-26 2.3-2.5, glycerol 4.9-5.1, xanthan gum 0.23-0.27, allantoin 0.09-0.11, Chinese medical concrete 1 ~ 10, glycyrrhizic acid dipotassium 0.19-0.21,
Caprylic/capric triglyceride 2.95-3.05, polydimethylsiloxane 1.95-2.05, cetearyl alcohol 5.1-5.3, ceteth-201.9-2.1, ceteareth-20.48-0.52, Butyrospermum parkii fruit fat 1.4-1.6, Dormant oils 2.5-3.5, Kaolin 5.0-7.0 and distilled water 63.3-65.8.
Described Chinese medical concrete is that Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, the Radix Gei japonici mixed according to the part by weight of 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2 extracts extractum; Preferred proportion is 1:1:2:1:2.
This draft facial film also configures essence 0.045-0.055.
The composition that described draft facial film comprises and corresponding weight portion are:
Glycerin polyether-262.4, glycerol 5.0, xanthan gum 0.25, allantoin 0.1, Chinese medical concrete 5, glycyrrhizic acid dipotassium 0.20, caprylic/capric triglyceride 3.0, polydimethylsiloxane 2.0, cetearyl alcohol 5.2, ceteth-202.0, ceteareth-20.5, Butyrospermum parkii fruit fat 1.5, Dormant oils 3.0, Kaolin 6.0, essence 0.05 and distilled water 64.7.
Take plant extract as the preparation method of the draft facial film of antisepsis and sterilization additive, carry out according to the following steps:
1) glycerin polyether-26, glycerol, xanthan gum, allantoin, Chinese medical concrete, glycyrrhizic acid dipotassium and distilled water are soaked in advance post-heating to dissolving completely, then be heated to 85 DEG C of sterilizing 25-36 minute;
2) caprylic/capric triglyceride, polydimethylsiloxane, cetearyl alcohol, ceteth-20, ceteareth-2, Butyrospermum parkii fruit fat and Dormant oils are added in pot, stir after being heated to 85 ± 2 DEG C of whole thawings, homogenizing 30 ± 5 minutes;
3) under-0.02Mpa vacuum condition by through step 1), 2) the material body that processes is uniformly mixed and homogenizing process 10-20 minute after adding Kaolin, when being then cooled to 45 DEG C, then adds flavor of raw material mix homogeneously;
4) continue to cool to 40 DEG C; Material body is filtered by 80 orders;
5) censorship is sampled.
Described polydimethylsiloxane need shift to an earlier date with cetearyl alcohol mixs homogeneously.
Described step 3) in homogenizing process be homogenizing blender with 2000-3000rpm homogenizing 5-6 minute, then add Kaolin homogenizing 15 ± 2 minutes, then cool to 50 ± 2 DEG C, continue to stir.
The preparation method of described Chinese medical concrete is:
1) Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici were pulverized 90-110 mesh sieve after drying, mixed by the part by weight of 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2;
2) by solid-liquid part by weight mixed solvent leaching 5-7 hour, the then reflux, extract, three times of 1:9-11, merge extractive liquid, steams solvent, obtains supernatant and separates out extractum;
3) supernatant and precipitation extractum obtain dry extract after vacuum drying.
Described mixed solvent is mixed by the volume ratio of 1:1 by 95% ethanol and ethyl acetate.
The invention has the beneficial effects as follows: owing to make use of the Flavonoid substances of plant itself, the sterilization of the material such as chlorogenic acid and plant polyphenol, bacteriostasis; not only ensure antisepsis and sterilization ability and the quality guarantee period (meeting the requirement of national Specification) of facial film; and instead of the use amount of the anticorrosion and bactericidal agent in facial film; and then significantly reduce the side effect that anticorrosion and bactericidal agent produces human body, environmental conservation is also of great importance.
Detailed description of the invention
Thinking of the present invention, be the materials such as Flavonoid substances, chlorogenic acid and the plant polyphenol utilizing plant itself to contain as antibacterial, provide a kind of draft facial film of environmental protection to contribute to consumer.
Described Flavonoid substances, chlorogenic acid and plant polyphenol are all harmless to the health, are easy to biodegradation, and have killing action to the common causative such as staphylococcus aureus and escherichia coli antibacterial, have obvious inhibitory action to fungus, yeast.With the facial film spending SHECAO in vain, Herba Portulacae Grandiflorae, Myrica rubra Dongkui root, Radix Gei japonici, Radix Actinidiae Chinensis are antisepsis and sterilization additive, except having antisepsis and sterilization effect, Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae also have enhancing non-specific immunity effect and antioxidation; Also certain curative effect is had to dermatosis such as skin furuncle and phyma skin infection, eczemas.
Herba Hedyotidis Diffusae: Herba Hedyotidis Diffusae is Rubiaceae plants of Hedyotis, all herbal medicine, has heat clearing away, detoxifies, invigorates blood circulation, effect of diuresis.Research in recent years shows, Herba Hedyotidis Diffusae has enhancing non-specific immunity effect and antioxidation, be used for the treatment of various cancer and inflammation clinically, its chemical composition is studied, herb is containing rubichloric acid., rubichloric acid. acid, remove acetic acid, the acid of base rubichloric acid., all square rafter glycoside acid, Herba Paederiae time glycoside, Herba Paederiae time glycoside methyl ester, 6-O-p-hydroxyl cinnamyl Herba Paederiae time glycoside methyl ester, 6-O-p-methoxyl group cinnamyl Herba Paederiae time glycoside methyl ester, 6-O-Resina Ferulae acyl Herba Paederiae time glycoside methyl ester, 2-methyl-3-hydroxyanthraquinone, 2-methyl-3-methoxy anthraquinone, 2-methyl-3-hydroxyl-4-methoxy anthraquinone, ursolic acid, cupreol, hentriacontane, stigmasterol, oleanolic acid, cupreol-β-glycoside, p-coumaric acid, iridoid, flavone, anthraquinone, p-coumaric acid, ferulic acid, oleanolic acid, scopoletin, Quercetin, kaempferol, the compositions such as daucosterol.
Function cures mainly: dyspnea and cough due to lung-heat; Laryngopharynx swelling and pain; Intestinal carbuncle; Furuncle and phyma skin infection; Venom; The puckery pain of pyretic stranguria; Edema; Dysentery; Intestinal is scorching; Jaundice due to damp-heat; Be good at the multiple cancerous protuberance for the treatment of.
Herba Scutellariae Barbatae: Portulaca grandilora is the plant of Portulacaceae Portulaca.Herb is containing carthamin (carthamidin), isocarthamidin (iso-carthamidin), high mountain baicalin (scutellarein), yellow official seal glycoside (scutel-larin) of high mountain, cupreol (β-sitosterol), stearic acid (steraricacid), alkaloid polysaccharide etc.According to another report, be separated from aerial parts and obtain wogonin (wogo-nin), rivularin (scutervulin), Herba Scutellariae Barbatae kind element (rivularin), naringenin (naringenin), apigenin (apigenin), dinatin (hispedulin), eriodictyol (eriodictyol), luteolin (suteolin), 5, 7, 4-trihydroxy-8-methoxy flavanone (5, 7,-trihydroxy-6-methoxyflavanone) 4-hydroxyl wogonin (4-hydroxywogonin), 7-gate of a lane base-5, 8-dimethoxy flavone (7-hy-droxy-5, 8-dimethoxyflavane), p-great base benzene first Tibet (p-hydroxyben-zaldehyde), p-great base benzylacetone (p-hydroxybenzylacetone), p-coumaric acid (p-coumaricaicd), protocatechuic acid (protocatechuicacid), energy fruit acid (ut-solicacid) plant sterol (phytosterol), plant sterol β-D-Glucose glycoside (phy-tosteryl-β-D-glucoside) etc.
Function cures mainly: have heat-clearing and toxic substances removing, blood circulation promoting and blood stasis dispelling, reducing swelling and alleviating pain, anticancer effect; Appendicitis curing, hepatitis, stomachache, early hepatocarcinoma, pulmonary carcinoma, cervical cancer, mastitis etc.; External is controlled pain furuncle and is treated, the diseases such as treating swelling and pain by traumatic injury.
Radix Actinidiae Chinensis: the root of Actinidiaceae plant Fructus actinidiae chinensis plant, containing triterpenoid compound, flavone compound, polysaccharide, Coumarins, (-)-epicatechin and (+)-catechin etc.
Function cures mainly: heat-clearing and toxic substances removing, clearing away heat-damp and promoting diuresis, and preventing tumor is anticancer, expelling wind and removing dampness, and diuresis is stopped blooding, removing toxic substances and promoting subsidence of swelling, the diseases such as dyspepsia, vomiting, rheumatic arthralgia, rheumatic ostalgia, Alimentary Tract Cancer, digestive tract tumor, carbuncle and ulcer furuncle, rheumatic ostalgia and jaundice.
Myrica rubra Dongkui root: the root of Myrica rubra Dongkui, containing flavonoid, chlorogenic acid; Tannin, dissociated anthraquinone
Function cures mainly: dampness treats skin ulcer, relieving diarrhea with astringents, promoting blood circulation and stopping pain etc.
Radix Gei japonici: be the root of dicotyledon medicine Maguireothamnus speciosus Astragalus tenuis, containing catechin compounds, ursolic acid, oleanolic acid, p sitosterol and alkaloid, glycoside compounds.
Function cures mainly: clearing away heat and expelling pathogen in the exterior; Promoting blood circulation and detoxication.Main cold, fever; Cough; Parotitis; Laryngopharynx swelling and pain; Hepatitis; Rheumatic arthritis; Wound hemorrhage.
Further illustrate below in conjunction with specific embodiment.
Embodiment 1
1) add aqueous phase pot after glycerin polyether-26 2.3, glycerol 5.1, xanthan gum 0.23, allantoin 0.11, Chinese medical concrete 3, glycyrrhizic acid dipotassium 0.21 and distilled water 64 being soaked in advance, be heated to dissolve completely simultaneously; Be heated to 85 DEG C of sterilizings 30 minutes.
2) caprylic/capric triglyceride 3.05, polydimethylsiloxane 1.95, cetearyl alcohol 5.3 (polydimethylsiloxane need shift to an earlier date mix homogeneously) with cetearyl alcohol, spermol 1.9, ceteareth-20.52, Butyrospermum parkii (BUTYROSPERMUM PARKII) fruit fat 1.4 and Dormant oils 3.5 are joined oil phase pot, be heated to 85 DEG C, after whole thawing, stir, homogenizing 30 minutes.
3) pull-up vacuum, first suction part aqueous phase material body in main cooker, then suck oil phase material body, finally suck aqueous phase material body, pulling vacuum is to-0.02Mpa, and then homogenizing is opened to 2500rpm, homogenizing 5 minutes, add Kaolin 7.0, homogenizing 15 minutes, notice taking out material body sees whether be uniformly dispersed, stir 15 minutes, froth breaking is thorough, opens cooling water, cool to 50 DEG C, stir, maintain vacuum, continue cooling, when 45 DEG C, add essence 0.045; Mix homogeneously.
4) continue to cool to 40 DEG C; Material body is placed into clean charging basket by 80 order filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete:
Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici were pulverized 100 mesh sieves after drying, mixed by the part by weight of 1:1:2:1:2; Then the solid-liquid part by weight mixed solvent (V of 1:10 is pressed
95% ethanol: V
ethyl acetate=50:50) soak 6 hours, reflux, extract, three times, merge extractive liquid, steams solvent, obtains supernatant and separates out extractum; Supernatant and precipitation extractum obtain dry extract after vacuum drying.
Embodiment 2
1) add aqueous phase pot after glycerin polyether-26 2.4, glycerol 5.0, xanthan gum 0.25, allantoin 0.10, Chinese medical concrete 5, glycyrrhizic acid dipotassium 0.20 and distilled water 64.7 being soaked in advance, be heated to dissolve completely simultaneously.Be heated to 85 DEG C of sterilizings 35 minutes.
2) caprylic/capric triglyceride 3.00, polydimethylsiloxane 2.00, cetearyl alcohol 5.20 (polydimethylsiloxane shift to an earlier date mix homogeneously) with cetearyl alcohol, spermol 2.00, ceteareth-20.50, Butyrospermum parkii fruit fat 1.50 and Dormant oils 3.00 are joined oil phase pot, be heated to 85 DEG C, after whole thawing, stir, homogenizing 30 minutes.
3) pull-up vacuum, first suction part aqueous phase material body in main cooker, then suck oil phase material body, finally suck aqueous phase material body, pulling vacuum is to-0.02Mpa, and then homogenizing is opened to 2500rpm, homogenizing 5 minutes, add Kaolin 6.0, homogenizing 15 minutes, notices that taking out material body sees whether be uniformly dispersed, and stirs 15 minutes, froth breaking is thorough, carries out next-step operation.Open cooling water, cool to 50 DEG C, stir, maintain vacuum, continue cooling, when 45 DEG C, add essence 0.05; Mix homogeneously.
4) continue to cool to 40 DEG C; Material body is placed into clean charging basket by 80 order filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete:
Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici were pulverized 90 mesh sieves after drying, mixed by the part by weight of 1:0.8:2.2:0.8:2.2; Then the solid-liquid part by weight mixed solvent (V of 1:9 is pressed
95% ethanol: V
ethyl acetate=50:50) soak 5 hours, reflux, extract, three times, merge extractive liquid, steams solvent, obtains supernatant and separates out extractum; Supernatant and precipitation extractum obtain dry extract after vacuum drying.
Embodiment 3
1) add aqueous phase pot after glycerin polyether-26 2.5, glycerol 4.9, xanthan gum 0.27, allantoin 0.09, Chinese medical concrete 10, glycyrrhizic acid dipotassium 0.19 and distilled water 62 being soaked in advance, be heated to dissolve completely simultaneously.Be heated to 85 DEG C of sterilizings 40 minutes.
2) caprylic/capric triglyceride 2.95, polydimethylsiloxane 2.05, cetearyl alcohol 5.1 (polydimethylsiloxane shift to an earlier date mix homogeneously) with cetearyl alcohol, ceteth-202.1, ceteareth-20.48, Butyrospermum parkii fruit fat 1.6 and Dormant oils 2.5 are joined oil phase pot, be heated to 84 DEG C, after whole thawing, stir, homogenizing 30 minutes.
3) pull-up vacuum, first suction part aqueous phase material body in main cooker, then suck oil phase material body, finally suck aqueous phase material body, pulling vacuum is to-0.02Mpa, and then homogenizing is opened to 2500rpm, homogenizing 5 minutes, add Kaolin 5.0, homogenizing 15 minutes, notices that taking out material body sees whether be uniformly dispersed, and stirs 15 minutes, froth breaking is thorough, carries out next-step operation.Open cooling water, cool to 50 DEG C, stir, maintain vacuum, continue cooling, when 45 DEG C, add essence 0.055; Mix homogeneously.
4) continue to cool to 40 DEG C; Material body is placed into clean charging basket by 80 order filters.
5) censorship is sampled.
The extracting method of Chinese medical concrete:
Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici were pulverized 110 mesh sieves after drying, mixed by the part by weight of 1:1.2:1.8:1.2:1.8; Then the solid-liquid part by weight mixed solvent (V of 1:11 is pressed
95% ethanol: V
ethyl acetate=50:50) soak 7 hours, reflux, extract, three times, merge extractive liquid, steams solvent, obtains supernatant and separates out extractum; Supernatant and precipitation extractum obtain dry extract after vacuum drying.
Each composition in above embodiment configures all by weight.
Reflux, extract, in the method for the invention, merge extractive liquid, steam solvent and vacuum drying is common process.
Comparison test
The cosmetics health specification issued with Ministry of Health of the People's Republic of China, for guidance standard, carries out Micro biological Tests to facial film.
Comparison test three products: No. 1 is blank, does not add Chinese medical concrete and anticorrosion and bactericidal agent; No. 2 for adding of the present invention product of Chinese medical concrete as antiseptic; No. 3 is mud film formulation, does not add Chinese medical concrete, adds the mineral mud of 5%, add 0.2% methyl hydroxybenzoate, 0.1% propyl hydroxybenzoate.
The product experimental result of harsh output is:
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | 3 | 0 | 0 | 0 | 0 |
| 2 | 2 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
After 1 year, test result is:
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | Cannot count (antibacterial is many) | 0 | 0 | 0 | Cannot count |
| 2 | 0 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
The test result of production after 2 years is:
The test result of production after 3 years is:
| Sequence number | Cosmetics total plate count | Go out excrement colibacillus group | Pseudomonas aeruginosa | Staphylococcus aureus | Yeast and mold sum |
| 1 | Cannot count (antibacterial is many) | 0 | 0 | 0 | Cannot count |
| 2 | 0 | 0 | 0 | 0 | 0 |
| 3 | 0 | 0 | 0 | 0 | 0 |
Claims (9)
1. be the draft facial film of antisepsis and sterilization additive with plant extract, the composition comprised and corresponding weight portion are:
Glycerin polyether-262.3-2.5, glycerol 4.9-5.1, xanthan gum 0.23-0.27, allantoin 0.09-0.11, Chinese medical concrete 1 ~ 10, glycyrrhizic acid dipotassium 0.19-0.21, caprylic/capric triglyceride 2.95-3.05, polydimethylsiloxane 1.95-2.05, cetearyl alcohol 5.1-5.3, ceteth-201.9-2.1, ceteareth-20.48-0.52, Butyrospermum parkii fruit fat 1.4-1.6, Dormant oils 2.5-3.5, Kaolin 5.0-7.0 and distilled water 63.3-65.8.
2. according to claim 1 take plant extract as the draft facial film of antisepsis and sterilization additive, it is characterized in that described Chinese medical concrete is that Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, the Radix Gei japonici mixed according to the part by weight of 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2 extracts extractum.
3. according to claim 1 and 2 take plant extract as the draft facial film of antisepsis and sterilization additive, it is characterized in that this draft facial film also configures essence 0.045-0.055.
4. according to claim 3 take plant extract as the draft facial film of antisepsis and sterilization additive, it is characterized in that the composition that described draft facial film comprises and corresponding weight portion are:
Glycerin polyether-262.4, glycerol 5.0, xanthan gum 0.25, allantoin 0.1, Chinese medical concrete 5, glycyrrhizic acid dipotassium 0.20, caprylic/capric triglyceride 3.0, polydimethylsiloxane 2.0, cetearyl alcohol 5.2, ceteth-202.0, ceteareth-20.5, Butyrospermum parkii fruit fat 1.5, Dormant oils 3.0, Kaolin 6.0, essence 0.05 and distilled water 64.7.
5. be the preparation method of the draft facial film of antisepsis and sterilization additive with plant extract, carry out according to the following steps:
1) glycerin polyether-26, glycerol, xanthan gum, allantoin, Chinese medical concrete, glycyrrhizic acid dipotassium and distilled water are soaked in advance post-heating to dissolving completely, then be heated to 85 DEG C of sterilizing 25-36 minute;
2) caprylic/capric triglyceride, polydimethylsiloxane, cetearyl alcohol, ceteth-20, ceteareth-2, Butyrospermum parkii fruit fat and Dormant oils are added in pot, stir after being heated to 85 ± 2 DEG C of whole thawings, homogenizing 30 ± 5 minutes;
3) under-0.02Mpa vacuum condition by through step 1), 2) the material body that processes is uniformly mixed and homogenizing process 10-20 minute after adding Kaolin, when being then cooled to 45 DEG C, then adds flavor of raw material mix homogeneously;
4) continue to cool to 40 DEG C; Material body is filtered by 80 orders;
5) censorship is sampled.
6. according to claim 5 take plant extract as the preparation method of the draft facial film of antisepsis and sterilization additive, it is characterized in that described polydimethylsiloxane need shift to an earlier date with cetearyl alcohol and mixs homogeneously.
7. according to claim 6 take plant extract as the preparation method of the draft facial film of antisepsis and sterilization additive, it is characterized in that described step 3) in homogenizing process be that homogenizing blender is with 2000-3000rpm homogenizing 5-6 minute, then Kaolin homogenizing is added 15 ± 2 minutes, then cool to 50 ± 2 DEG C, continue to stir.
8. according to claim 7 take plant extract as the preparation method of the draft facial film of antisepsis and sterilization additive, it is characterized in that the preparation method of described Chinese medical concrete is:
1) Herba Hedyotidis Diffusae, Herba Portulacae Grandiflorae, Radix Actinidiae Chinensis, Myrica rubra Dongkui root, Radix Gei japonici were pulverized 90-110 mesh sieve after drying, mixed by the part by weight of 1:0.8-1.2:1.8-2.2:0.8-1.2:1.8-2.2;
2) by solid-liquid part by weight mixed solvent leaching 5-7 hour, the then reflux, extract, three times of 1:9-11, merge extractive liquid, steams solvent, obtains supernatant and separates out extractum;
3) supernatant and precipitation extractum obtain dry extract after vacuum drying.
9. according to claim 8 take plant extract as the preparation method of the draft facial film of antisepsis and sterilization additive, it is characterized in that described mixed solvent is mixed by the volume ratio of 1:1 by 95% ethanol and ethyl acetate.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106806260A (en) * | 2015-11-27 | 2017-06-09 | 上海朗亿生物科技有限公司 | A kind of Chinese medicinal paste facial mask and preparation method thereof |
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| CN106806260A (en) * | 2015-11-27 | 2017-06-09 | 上海朗亿生物科技有限公司 | A kind of Chinese medicinal paste facial mask and preparation method thereof |
| CN107157781A (en) * | 2017-06-18 | 2017-09-15 | 黑龙江嘉能高科技开发有限责任公司 | A kind of single-layer graphene repair membrane and preparation method |
| CN107362102A (en) * | 2017-08-31 | 2017-11-21 | 昆明先康生物科技有限公司 | A kind of beautiful beauty mask of promise |
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|---|---|
| CN104490702B (en) | 2017-05-10 |
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