CN102813607A - Oil-in-water type fucoidan skin cream and preparation method thereof - Google Patents
Oil-in-water type fucoidan skin cream and preparation method thereof Download PDFInfo
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- CN102813607A CN102813607A CN2012102762373A CN201210276237A CN102813607A CN 102813607 A CN102813607 A CN 102813607A CN 2012102762373 A CN2012102762373 A CN 2012102762373A CN 201210276237 A CN201210276237 A CN 201210276237A CN 102813607 A CN102813607 A CN 102813607A
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Abstract
The invention belongs to the field of cosmetics, and in particular relates to an oil-in-water type fucoidan skin cream and a preparation method thereof. The formula of the skin cream comprises the following components by weight: 5-10 percent of fucoidan, 10-15 percent of grease, 2-10 percent of humectant, 0.5-2 percent of surfactant, 0.5-2 percent of antioxidant, 0.01-3 percent of preservative, 0.05-0.5 percent of essence and the balance of deionized water. The preparation steps comprise (1) preparation of an oil phase; (2) preparation of a water phase; (3) emulsification and cooling; and (4) hot-filling. The obtained product contains active fucoidan achieving 5-10 percent so that skin can be softened, the immunity of the skin is improved, the elasticity and gloss of the skin are enhanced, and ultraviolet injury of the skin can be repaired; in addition, the cream is fine and smooth, is easy to apply, can be quickly absorbed and has durable effects. The oil-in-water type fucoidan skin cream is simple in the preparation process, and can be produced by using traditional manufacturing processes and equipment.
Description
Technical field
The invention belongs to cosmetic field, relate in particular to a kind of oil-in-water type fucoidan cold cream and preparation method thereof.
Background technology
Along with the develop rapidly of fine chemistry industry, bioscience, material science, cell science going deep in dermatology, and human genome project's starting make cosmetics develop towards the direction that more is rich in the degree of depth and range.The cosmetics that the active component that from natural biological, extracts is processed day by day receive people's favor, are leading the trend of cosmetics.Fucoidan; English name Fucoidan; Be also referred to as fucoidan, sulfated fucan, fucosan, fucoidin etc.; Fucoidan is a kind of good health food, pharmaceutical raw material, because of the natural sulfate radical that contains, thereby has the characteristic of anionic polymer chemical compound.Research shows that fucoidan is a kind of macrophage, T cell to be had direct acting immunomodulator; Pharmacological activity with tangible anticoagulation and fibrinolysis enhancing: comprise fucose or its degradation product ability cancer cell specific induction of apoptosis of sulfate, can be used as inducer of apoptosis and anticarcinogen; Can bring out the generation of cell growth factor, thereby promote various cell growths, reparation is damaged or hypothyroid organ and tissue.The pharmacologically active of fucoidan is suitable for being applied to cosmetic field protection skin.
Summary of the invention
The objective of the invention is this natural biological extraction of substance of fucoidan is processed cold cream; This cold cream can soft skin, promote skin immunity, Laminaria Digtatitat, reparation ultraviolet injury; Improve Skin Cell living environment and the metabolism that promotes skin histology; Deeply repair skin tissue, improve the skin quality from inside to outside, the state that skin is kept fit constantly.
Technical scheme of the present invention is; A kind of oil-in-water type fucoidan cold cream; It is characterized in that: count by weight percentage, prescription comprises following component: fucoidan 5%-10%, oils and fats 10%-15%, wetting agent 2%-10%, surfactant 0.5%-2%, antioxidant 0.5%-2%, antiseptic 0.01%-3%, essence 0.05-0.5%, all the other are deionized water.
Described oils and fats is one or more mixture in tristerin, kitol, vaseline, liquid lanolin, Cera Flava, Jojoba oil, olive oil, Oleum Cocois, the squalane.
Said wetting agent is one or more in fish scale collagen, glycerol, Sorbitol, the propylene glycol.
Said surfactant is one or more in sodium hexadecyl sulfate, sorbester p17, Tween 80, the polysorbate65.
Said antioxidant is one or more in vitamin C, vitamin E, beta glucan, phylloxanthin, the Thioctacid.
Said antiseptic is one or more in methyl hydroxybenzoate, propylparaben, Borax, benzyl alcohol, the butylhydroxy anisole.
Described essence is the spice that allows usefulness in the cosmetics.
A kind of oil-in-water type fucoidan cold cream, its preparation method comprises the steps:
(1) preparation of oil phase: the oils and fats in the component and other thermal stabilization oil property compositions are added in the chuck dissolving pan, open Steam Heating, constantly be heated to 70-75 ℃ under the stirring condition, it is fully melted or dissolve evenly for use;
(2) preparation of water: earlier deionized water is added in the chuck dissolving pan, more thermally-stabilised water soluble ingredient is added wherein, stir down and be heated to 90-100 ℃, keep 20min and sterilize, be cooled to then 70～75 ℃ for use;
(3) emulsifying and cooling: above-mentioned oil phase and water are filtered the back with filter respectively add in the emulsifying pot, add fashionablely, earlier water is added; Then at 70-75 ℃; Oil phase is slowly joined aqueous phase, and the limit edged stirs and makes its emulsifying, and the fucoidan in the prescription, essence and other easy compositions that decomposes are then after emulsifying; When dropping to 50 ℃ ± 2 ℃, temperature adds, to guarantee its activity.After the emulsifying, emulsification system will be cooled to 40-45 ℃.The type of cooling is in the chuck with the logical people's emulsifying pot of cooling water, and stir on the limit, the limit cooling.
(4) hot filling: the cooled product of emulsifying is used the filling machine hot filling.
The invention has the beneficial effects as follows that active fucoidan can reach 5-10% in the product, the soft skin of ability, lifting skin immunity, Laminaria Digtatitat, reparation ultraviolet injury; Mastic is fine and smooth, is easy to be coated with exhibition, absorbs soon, and persistency is strong.Oil-in-water type fucoidan cold cream preparation technology of the present invention is simple, uses conventional fabrication processes and equipment to produce.
The specific embodiment
Embodiment 1
Method for preparing
At first take by weighing each component by above prescription; Then 2.-5., 10.-
these 7 kinds of thermal stabilization oil phase constituents all add in the chuck dissolving pan; Open Steam Heating; Constantly being heated to 70-75 ℃ under the stirring condition, it is fully melted or dissolves uniform preparation to become oil phase for use;
deionized water is added in the chuck dissolving pan; Again with thermally-stabilised water soluble ingredient 6.-8.,
add wherein; Be heated to 90-100 ℃ under stirring; Keep 20min sterilization, being cooled to 70～75 ℃ then, to be prepared into water for use; After filter filters, add above-mentioned oil phase and water in the emulsifying pot; Add fashionable, first with the water adding, then at 70-75 ℃; Oil phase is slowly joined aqueous phase; The limit edged stirs and makes its emulsifying, and the 1. fucoidan in the prescription,
Oleum Rosae Rugosae, 9. Vc then after emulsifying, adds when temperature drops to 50 ℃ ± 2 ℃; After the emulsifying; In the chuck with the logical people's emulsifying pot of cooling water, cooling while stirring, emulsification system will be cooled to 40-45 ℃; The cooled product of emulsifying is used the filling machine hot filling.
Embodiment 2
Method for preparing
At first take by weighing each component by above prescription; Then 2.-5., 9.,
these 8 kinds of thermal stabilization oil phase constituents all add in the chuck dissolving pan; Open Steam Heating; Constantly being heated to 70-75 ℃ under the stirring condition, it is fully melted or dissolves uniform preparation to become oil phase for use;
deionized water is added in the chuck dissolving pan; Again 6.-8. thermally-stabilised water soluble ingredient is added wherein; Be heated to 90-100 ℃ under stirring; Keep 20min sterilization, being cooled to 70～75 ℃ then, to be prepared into water for use; After filter filters, add above-mentioned oil phase and water in the emulsifying pot; Add fashionable, first with the water adding, then at 70-75 ℃; Oil phase is slowly joined aqueous phase; The limit edged stirs and makes its emulsifying, and the 1. fucoidan in the prescription,
jasmin essence, 10. phylloxanthin then after emulsifying, adds when temperature drops to 50 ℃ ± 2 ℃; After the emulsifying; In the chuck with the logical people's emulsifying pot of cooling water, cooling while stirring, emulsification system will be cooled to 40-45 ℃; The cooled product of emulsifying is used the filling machine hot filling.
Embodiment 3
Method for preparing
At first take by weighing each component by above prescription; Then 2.-6., 10.,
these 10 kinds of thermal stabilization oil phase constituents all add in the chuck dissolving pan; Open Steam Heating; Constantly being heated to 70-75 ℃ under the stirring condition, it is fully melted or dissolves uniform preparation to become oil phase for use;
deionized water is added in the chuck dissolving pan; Again 7.-9. thermally-stabilised water soluble ingredient is added wherein; Be heated to 90-100 ℃ under stirring; Keep 20min sterilization, being cooled to 70～75 ℃ then, to be prepared into water for use; After filter filters, add above-mentioned oil phase and water in the emulsifying pot; Add fashionable; Earlier water is added; So at 70-75 ℃, oil phase is slowly joined aqueous phase, the limit edged stirs and makes its emulsifying; 1. fucoidan in the prescription,
jasmin essence,
Thioctacid are then after emulsifying; When dropping to 50 ℃ ± 2 ℃, temperature adds, after the emulsifying, in the chuck with the logical people's emulsifying pot of cooling water; Cooling while stirring, emulsification system will be cooled to 40-45 ℃; The cooled product of emulsifying is used the filling machine hot filling.
Claims (8)
1. oil-in-water type fucoidan cold cream; It is characterized in that: count by weight percentage, prescription comprises following component: fucoidan 5%-10%, oils and fats 10%-15%, wetting agent 2%-10%, surfactant 0.5%-2%, antioxidant 0.5%-2%, antiseptic 0.01%-3%, essence 0.05-0.5%, all the other are deionized water.
2. described oil-in-water type fucoidan cold cream according to claim 1 is characterized in that: said oils and fats is one or more mixture in tristerin, kitol, vaseline, liquid lanolin, Cera Flava, Jojoba oil, olive oil, Oleum Cocois, the squalane.
3. described oil-in-water type fucoidan cold cream according to claim 1, it is characterized in that: said wetting agent is one or more in fish scale collagen, glycerol, Sorbitol, the propylene glycol.
4. described oil-in-water type fucoidan cold cream according to claim 1, it is characterized in that: said surfactant is one or more in sodium hexadecyl sulfate, sorbester p17, Tween 80, the polysorbate65.
5. described oil-in-water type fucoidan cold cream according to claim 1, it is characterized in that: said antioxidant is one or more in vitamin C, vitamin E, beta glucan, phylloxanthin, the Thioctacid.
6. described oil-in-water type fucoidan cold cream according to claim 1, it is characterized in that: said antiseptic is one or more in methyl hydroxybenzoate, propylparaben, Borax, benzyl alcohol, the butylhydroxy anisole.
7. described oil-in-water type fucoidan cold cream according to claim 1 is characterized in that: described essence is the spice that allows usefulness in the cosmetics.
8. according to any described oil-in-water type fucoidan cold cream of claim 1-7, it is characterized in that its preparation method comprises the steps:
(1) preparation of oil phase: the oils and fats in the component and other thermal stabilization oil property compositions are added in the chuck dissolving pan, open Steam Heating, constantly be heated to 70-75 ℃ under the stirring condition, it is fully melted or dissolve evenly for use;
(2) preparation of water: earlier deionized water is added in the chuck dissolving pan, more thermally-stabilised water soluble ingredient is added wherein, stir down and be heated to 90-100 ℃, keep 20min and sterilize, be cooled to then 70～75 ℃ for use;
(3) emulsifying and cooling: above-mentioned oil phase and water are filtered the back with filter respectively add in the emulsifying pot, add fashionablely, earlier water is added; At 70-75 ℃, oil phase is slowly joined aqueous phase then, the limit edged stirs and makes its emulsifying; Fucoidan in the prescription, essence and other easy compositions that decomposes are then after emulsifying; Add when temperature drops to 50 ℃ ± 2 ℃, after the emulsifying, emulsification system is cooled to 40-45 ℃;
(4) hot filling: the cooled product of above emulsifying is used the filling machine hot filling.
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| CN2012102762373A CN102813607A (en) | 2012-08-06 | 2012-08-06 | Oil-in-water type fucoidan skin cream and preparation method thereof |
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| CN2012102762373A CN102813607A (en) | 2012-08-06 | 2012-08-06 | Oil-in-water type fucoidan skin cream and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038355A (en) * | 2016-07-21 | 2016-10-26 | 中国科学院海洋研究所 | Application of highly sulfated seaweed polysaccharide to post-basking repair mask |
| CN107184408A (en) * | 2017-05-22 | 2017-09-22 | 邵洁明 | A kind of mildy wash and preparation method |
| CN109464295A (en) * | 2018-10-29 | 2019-03-15 | 名臣健康用品股份有限公司 | A kind of skin care compositions and methods of the fucose containing low molecular weight |
| CN111135113A (en) * | 2020-02-26 | 2020-05-12 | 钟达金 | Moisturizing and antioxidant composition and preparation method thereof |
| CN111450297A (en) * | 2020-04-26 | 2020-07-28 | 青岛明月海藻生物健康科技集团有限公司 | Marine fucoidin herbal atomizing agent and preparation method thereof |
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| CA2278766A1 (en) * | 1997-02-07 | 1998-08-13 | Henkel Kommanditgesellschaft Auf Aktien | Skin care product |
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| CN101406429A (en) * | 2008-11-25 | 2009-04-15 | 上海应用技术学院 | Oil-in-water emulsion and preparation method thereof |
| CN101999992A (en) * | 2010-10-26 | 2011-04-06 | 威海市宇王集团有限公司 | Fish scale collagen cosmetic |
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2012
- 2012-08-06 CN CN2012102762373A patent/CN102813607A/en active Pending
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| CA2278766A1 (en) * | 1997-02-07 | 1998-08-13 | Henkel Kommanditgesellschaft Auf Aktien | Skin care product |
| US20060093566A1 (en) * | 1999-11-30 | 2006-05-04 | Shigetoshi Mizutani | Fucoidan-containing cosmetics |
| JP2001335457A (en) * | 2000-05-26 | 2001-12-04 | Yakult Honsha Co Ltd | Antioxidant and skin care preparation containing the same |
| WO2006093175A1 (en) * | 2005-03-01 | 2006-09-08 | Ube Industries, Ltd. | High-molecular fucoidan, method of producing the same and cosmetic composition |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038355A (en) * | 2016-07-21 | 2016-10-26 | 中国科学院海洋研究所 | Application of highly sulfated seaweed polysaccharide to post-basking repair mask |
| CN107184408A (en) * | 2017-05-22 | 2017-09-22 | 邵洁明 | A kind of mildy wash and preparation method |
| CN109464295A (en) * | 2018-10-29 | 2019-03-15 | 名臣健康用品股份有限公司 | A kind of skin care compositions and methods of the fucose containing low molecular weight |
| CN109464295B (en) * | 2018-10-29 | 2021-12-28 | 名臣健康用品股份有限公司 | Skin care composition containing low molecular weight fucooligosaccharide |
| CN111135113A (en) * | 2020-02-26 | 2020-05-12 | 钟达金 | Moisturizing and antioxidant composition and preparation method thereof |
| CN111450297A (en) * | 2020-04-26 | 2020-07-28 | 青岛明月海藻生物健康科技集团有限公司 | Marine fucoidin herbal atomizing agent and preparation method thereof |
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