CN1069256A - A kind of efficient, multifunctional foliage fertilizer and preparation method thereof - Google Patents

A kind of efficient, multifunctional foliage fertilizer and preparation method thereof Download PDF

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CN1069256A
CN1069256A CN 92109659 CN92109659A CN1069256A CN 1069256 A CN1069256 A CN 1069256A CN 92109659 CN92109659 CN 92109659 CN 92109659 A CN92109659 A CN 92109659A CN 1069256 A CN1069256 A CN 1069256A
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foliage fertilizer
phytocytomine
weight
plant
fertilizer according
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CN1025115C (en
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叶爱珍
翦敦荣
甘美华
周德霖
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GUILIN INST OF AGRICULTUREAL SCIENCE
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Abstract

The present invention relates to foliage fertilizer and preparation method thereof.This foliage fertilizer is by Plant hormones regulators,gibberellins, phytocytomine, αNai Yisuan, phenoxy acetic acid, 2, and 4-D, vitamins C, strysolin newly, and micronutrient element and macronutrient and tensio-active agent are formed.
This foliage fertilizer has significant effect of increasing production, and the paddy rice big area is used and increased by 9-12%, corn 11.2%; Wheat 8.8%, peanut 11.3%, sugarcane 18.0%, vegetables 20% are with first-class.This product consumption is few, and cost is low, safety non-toxic, and effect stability is reliable, and using method is easy.Have tangible economic benefit and social benefit.

Description

A kind of efficient, multifunctional foliage fertilizer and preparation method thereof
The present invention relates to the chemical fertilizer field, especially relate to foliage fertilizer and preparation method thereof.
People know that the normal growth of crop is grown, grown up strong and sturdy, and obtain good harvest at last, are the results of various plants growth regulator effect in the growing process, also are the results who has satisfied the required various nutritive elements of plant-growth.The history of foliage top dressing, can trace back to more than 100 year before.The discovery of plant endogenous growth regulator and external source growth regulator and application, the history that also arranged decades, but still be in the starting stage so far, some domestic and international experts and scholars think: the research of plant-growth regulator will become one of four big high-new art in the 21st century agriculture field with application.
At present, the application of plant-growth regulator is applied as the master with single, for example single with Plant hormones regulators,gibberellins in fruit tree, play the effect of flower and fruit protecting, but cause negative effect again simultaneously, make the pericarp thickening, quality and grade reduce.Single paclobutrazol of using can suppress rice shoot excessive growth in raising rice seedlings, and promotion is divided and bred short strong sprout, but its root system development also is suppressed.In addition, usually lack certain or certain several trace element in the soil, if any regional soil seriously lack the zinc boron deficiency, when lacking zinc, the plant leaf chlorosis, photosynthesis weakens, internode shortens, plant is short and small, growth is suppressed, output reduces.During boron deficiency, farm crop easily lodge, the crop that has the not result of only blooming, the serious underproduction.In this case, even other various nutritive element abundances, cultivation step is scientific and reasonable, and its crop is poor growth still, even loses and receive.
Therefore, the object of the present invention is to provide a kind of foliage fertilizer that contains various plants growth regulator and micronutrient element, and the preparation method of this foliage fertilizer.
This foliage fertilizer (being commonly called as unsurpassed volume increase agent) is according in the plant-growth cycle, the principle of the whole vital process of forming by the various plants growth regulator of regulation system controlling plant, of equal importance and the not replaceable principle of plant nutrition considers that simultaneously the effective constituent specific absorption is succeeded in developing by the influence of tensio-active agent and surface adhering agent in foliage fertilizer spraying effect and the leaf fertilizer.
The major technique content of this foliage fertilizer and preparation method thereof:
1. high-efficiency multi-function foliage fertilizer is characterized in that it is made up of plant growth conditioning agent, antibiotic, micronutrient element, macronutrient and tensio-active agent:
Described plant growth conditioning agent is Plant hormones regulators,gibberellins, phytocytomine, αNai Yisuan, phenoxy acetic acid, 2,4-D, vitamins C, and its corresponding parts by weight are: 0-20,50-400,1-20,10-50,0-6,0-20;
Described antibiotic is Xin Meisu, and its parts by weight are 0-100;
Described micronutrient element is boron, zinc, manganese, magnesium, copper, molybdenum, and its corresponding parts by weight are 70-250,70-250,30-100,10-100,0-150,0-20;
Described macronutrient is nitrogen, phosphorus, potassium, and its corresponding parts by weight are respectively 5-60,50-100,70-120;
Described tensio-active agent is that Sodium dodecylbenzene sulfonate, OP-10, tween 20, its parts by weight are 5-20.
2. according to above-mentioned 1 described foliage fertilizer, it is characterized in that Plant hormones regulators,gibberellins, phytocytomine, αNai Yisuan, phenoxy acetic acid, 2,4-D, ascorbic parts by weight are respectively: 0-10,100-250,2-10,15-40,0-4,0-10.
3. according to above-mentioned 2 described foliage fertilizers, it is characterized in that Plant hormones regulators,gibberellins, phytocytomine, α-Nai Yisuan, phenoxy acetic acid, 2,4-D, ascorbic parts by weight are respectively: 0-5,100-200,4-10,15-30,1-3,0-8.
4. according to above-mentioned 1 described foliage fertilizer, it is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
5. according to above-mentioned 2 described foliage fertilizers, it is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
6. according to above-mentioned 3 described foliage fertilizers, it is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
7. according to above-mentioned 1 described foliage fertilizer, it is characterized in that micronutrient element is vitriol, nitrate, muriate, carbonate form, boron then is the borate form.
8. according to above-mentioned 1 described foliage fertilizer, it is characterized in that macronutrient is potassium primary phosphate, vitriolate of tartar, Repone K, urea, ammonium nitrate, volatile salt, ammonium sulfate, ammonium chloride, Secondary ammonium phosphate, primary ammonium phosphate, potassium-ammonium phosphate.
9. according to the preparation method of the described foliage fertilizer of above-mentioned 1-8, it is characterized in that:
(1) zinc, manganese, magnesium, copper, nitrogen, phosphorus, potassium compound raw material are mixed, under 70-100 ℃ of temperature dry 1-4 hour, pulverize, analyse through 80 mesh sieves and obtain work in-process (I);
(2) boric acid mixes with phytocytomine, grinds to reach 0.4-1.5 hour, and its work in-process (II) reach pH5-8;
(3) at Plant hormones regulators,gibberellins, phytocytomine, α-Nai Yisuan, phenoxy acetic acid, 2, in 4-D, vitamins C, the antibiotic mixture, add small amount of ethanol, grind evenly, obtain work in-process (III);
(4) above-mentioned work in-process (I) (II) (III) are mixed after, granularity is joined in the said mixture less than 100 purpose tensio-active agents, the limit edged stirs, up to the yellowish-yellow powder product that obtains good fluidity.
This foliage fertilizer contains five plant growth regulators, and wherein Plant hormones regulators,gibberellins has the function of very big stimulating growth to many live plants, can also stimulate the natural synthetic or secretion of many enzymes.Phytokinin is the plant hormone that a kind of pair cell division and differentiation play an important role, and its major function is in the presence of growth hormone, can promote the division of cell, suppresses or delay the aging of leaf tissue, impels plant sturdy, strengthens photosynthesis; αNai Yisuan can add excitometabolic, promotes the growth of root system of plant, strengthens receptivity and the resistance of plant to soil nutrient and moisture; P-Iodophenoxyacetic acid, 2,4-D(2,4-dichlorphenoxyacetic acid) be auxin substance, the former can promote the running and the enzyme effect of nutrient in the plant materials, the latter can promote plant-growth, prevents fruit drop, quickens young fruit development.This five plant growth regulators is by optimizing, and indoor and field is simultaneous test and preferably coming out repeatedly.The application's foliage fertilizer also comprises multiple micronutrient element.Great majority are integral parts of enzyme or coenzyme in the trace element, and very active in plant, its physiological function has very strong specificity.When micronutrient element was supplied with and can not be satisfied the plant needs in the soil, the characteristic symptom of trace element appearred lacking in the poor growth of plant sometimes, causes crop production reduction or quality to reduce, when serious even No kernels or seeds are gathered, as in a year of scarcity.As the conversion and the conveying of boron involved in sugar part and starch in plant materials, regulate moisture content absorption and nutrient balance and redox processes, be yield positive results and vegetative point (comprising root system) growth essential; Zinc is the necessary component and the activator of some enzyme, to synthetic, the photosynthesis of chlorophyll in the plant and growth hormone, respiratory and redox processes all are essential, and zinc can impel the synthetic of protein and ribose, and participate in the conversion of carbohydrate, and influence the maturing rate of plant and seed thereof; Manganese is relevant with the activity of many enzymes, participate in conversion and some redox processeses of photosynthesis, nitrogen, the conversion or the metabolic process of molybdenum and nitrogen, phosphorus and carbohydrate have confidential relation, and with ascorbic synthetic relevant, copper is that plant formation chlorophyll is necessary, also be some oxidasic composition, improve the respiratory intensity of plant, the content of vitamin A and C in the enhancing plant.Because the regulation system that the various plants growth regulator is formed in this foliage fertilizer can be regulated the whole vital process of controlling plant, various nutrient elements involved in plant body is formed, regulate the life process of plant materials, so this foliage fertilizer plays optimum regulating effect to plant-growth, improved the nutritional status of crop, thereby promoted crop seed sprouting, long root, branch evil, bloom, the result.Can also delay chlorophyll and decompose, prolong the chlorophyllous life-span, strengthen crop photosynthesis action intensity and energy metabolism level, in general, the chlorophyll increase reaches 10.7-36.4%, and photosynthesis strengthens 19.82-57.88%; Can also improve the activity of amylase, saccharase etc., help the running and the accumulation of carbohydrate in the crop, vitality of nitrate reductase is had remarkable promoter action, thereby useful influence is taken place yield and quality, can also reduce simultaneously the activity of cellulase, make crop reduce fruit drop; Can also improve oxidasic vigor, thereby strengthen the resistance of crop, can make crop growth healthy and strong.
The concrete preparation method of this foliage fertilizer is as follows: at first take by weighing a certain amount of zinc sulfate, manganous sulfate, ammonium molybdate, sal epsom, copper sulfate, borax and place baking oven to dry, its oven temperature is controlled at 1-4 hour 70-100 ℃ of time of drying, after the drying, treat the above-mentioned raw materials cool to room temperature, in mortar, pulverize again, grind, cross 60 mesh sieves, obtain work in-process (I).
Then a certain amount of boric acid is mixed with phytocytomine, grinding reaches 0.4-1.5 hour, and its work in-process (II) reach pH5-8.
Take by weighing a certain amount of red enzyme element, α-Nai Yisuan, phenoxy acetic acid, 2 again, 4-D, vitamins C, the plain mixing of planting enzyme add small amount of ethanol and grind evenly, obtain work in-process (III).
Get after above-mentioned work in-process (I) and (II) mix, add work in-process (III) again and be mixed together, place and add tensio-active agent again after for some time and grind evenly, promptly obtain the yellowish-yellow powder product of good fluidity.
To explain the present invention by embodiment below, but not be further restriction of the present invention.
Embodiment 1
At first taking by weighing Zincomed 70 gram, anhydrous manganous sulfate 40 grams, ammonium molybdate 6 grams, anhydrous magnesium sulfate 20 grams, potassium primary phosphate 280 grams, ammonium sulfate 220 grams places baking oven to dry, oven temperature is controlled at 100 ℃, 4 hours time, behind dry the end, treat the above-mentioned raw materials cool to room temperature, pulverizing, levigate reaching more than 60 orders in mortar are crossed 60 mesh sieves again, and screen underflow is work in-process (I).
Take by weighing boric acid 110 gram, zeatin 200 grams, mixed grinding half an hour, measure its work in-process (II) pH value and reach 6.8.
Take by weighing plain 1 gram of red enzyme, α-Nai Yisuan 4 grams, phenoxy acetic acid 20 grams, 2 again, 4-D3 gram, vitamins C 5 grams add 1 milliliter of ethanol in its mixture, and stirring and evenly mixing under 250 rev/mins of rotating speeds obtains work in-process (III) through grinding again.
Get after above-mentioned work in-process (I) and (II) mix, add work in-process (III) again and be mixed together, add 10 gram Sodium dodecylbenzene sulfonatees again after placing for some time, grind and evenly obtain its product.
Its group of products becomes N, P by analysis, K is a 20%(weight); Micronutrient element Zn, Mo, B, Mg are 7%(weight); Plant-growth regulator is a 3%(weight).Color is faint yellow.
Adopt this product and blade face treasured, 920, yield increasing fungus, clear water (contrast) rice test.The base fertilizer that uses in the test is identical, and the condition of test liquid fertilizer sees Table I.Test-results sees Table II.
Figure 921096593_IMG1
Figure 921096593_IMG2
Embodiment 2
At first take by weighing Zincomed 250 grams, anhydrous manganous sulfate 30 grams, five water magnesium sulfates, 30 grams, potassium primary phosphate 350 grams, ammonium sulfate 300 grams, its treatment process is with embodiment 1.
Take by weighing boric acid 175 gram, zeatin 100 grams, mixed grinding half an hour, measure its work in-process (II) pH value and reach 6.2.
Take by weighing plain 4 grams of red enzyme, α-Nai Yisuan 4 grams, phenoxy acetic acid 20 all the other treatment processs of gram again with embodiment 1.
Its group of products becomes N, P by analysis, K is a 20%(weight); Micronutrient element Zn, Mo, B, Mg are 11%(weight); Plant-growth regulator is a 10%(weight).Color is faint yellow.
Adopt this product and blade face treasured, potassium primary phosphate, clear water to do the corn test.Test-results sees Table III.
Table III corn test-results
Handle replicated plot area cell production per mu yield mu volume increase stimulation ratio
(mu) (jin) (jin) (jin) %
Leaf 1 0.120 10.23 852.5
Face 2 0.120 11.00 916.7 55.6 6.95
Precious 3 0.120 9.57 797.5
Average 0.120 10.27 855.6
Phosphorus 1 0.120 10.00 833.3
Acid 2 0.120 9.84 820.0 18.0 2.25
23 0.120 9.61 800.8
Hydrogen
Potassium average 0.120 9.82 818.0
These are 1 0.120 11.16 930.0 years old
Produce 2 0.120 10.27 855.8 89.2 11.15
Product 3 0.120 10.58 881.7
Average 0.120 10.80 889.2
Clear 1 0.120 10.27 855.8
Water 2 0.120 8.92 743.3
3 0.120 9.61 800.8
Average 0.120 9.60 800.0
Embodiment 3
At first take by weighing Zincomed 120 grams, anhydrous manganous sulfate 50 grams, anhydrous magnesium sulfate 60 grams, anhydrous cupric sulfate 140 grams, other treatment processs are with embodiment 1.
Take by weighing borax 140 gram, kinetin 175 grams, mixed grinding half an hour, measure its work in-process (II) pH value and reach 7.2.
Take by weighing plain 1 gram of red enzyme, α-Nai Yisuan 6 grams, phenoxy acetic acid 20 grams, vitamins C 3 grams again, all the other treatment processs are with embodiment 1.
Get after above-mentioned work in-process (I) and (II) mix, add work in-process (III) again and be mixed together, add 5 gram OP-10 again after placing for some time, grind and evenly obtain its product.
Its group of products becomes N, P by analysis, K is a 16%(weight); Micronutrient element Zn, Mn, Mg, Cu are 11%(weight); Plant-growth regulator is a 15%(weight).Color is yellow.
Adopt this product and the watermelon of vitriolate of tartar, phytokinin etc. to test, the base fertilizer that uses in the test is identical.Its test-results sees Table IV.
Table IV watermelon rational application of fertilizers test-results
Handle sub-district area cell production comparison according to volume increase
Contrast (25 kilograms/mu of fertilizer+composite fertilizers) (M1) 1.7 278.0/
10 kilograms/mu of vitriolate of tartar (M2), (M1+M2) 1.7 350.0 25.9
Phytokinin 200 gram/mus+M2 1.7 352.5 26.8
This product 30 gram/mus+M2 1.7 353.5 27.2
Zinc sulfate 200 gram/mus+borax 200 gram/mus+M2 1.7 346.0 24.5
Adopt the sweet osmanthus seedling test of this product and clear water (contrast), the base fertilizer that uses in the test is identical, and test-results is listed in the table V
Figure 921096593_IMG3
Embodiment 4
Take by weighing Zincomed 100 grams, anhydrous manganous sulfate 40 grams, ammonium molybdate 10 grams, anhydrous magnesium sulfate 60 grams, potassium primary phosphate 400 grams, ammonium sulfate 50 its treatment processs of gram with embodiment 1.
Take by weighing borax 150 gram, zeatin 200 grams again, mixed grinding half an hour, measure its work in-process (II) pH value and reach 6.5.
Take by weighing α-Nai Yisuan 4 grams, phenoxy acetic acid 25 grams, 2 then, the 4-D1 gram, its treatment process is with corresponding step among the embodiment 1.
Get after above-mentioned work in-process (I) and (II) mix, add work in-process (III) again and be mixed together, add 5 gram polysorbas20s grams again after placing for some time, grind and evenly obtain its product.
Its group of products becomes N, P by analysis, K is a 21%(weight); Micronutrient element Zn, Mn, B, Mg, Mo are 20%(weight); Plant-growth regulator is a 22%(weight).Product colour is yellow.
The test of adopting this product and rare earth, clear water that sucrose part is influenced.The base fertilizer that uses in the test is identical.Test-results is listed in the table VII.
Figure 921096593_IMG4
In the past few years, test, demonstrate and promote more than totally 100 ten thousand mu times in more than 60 test point, 15 provinces and regions, the whole nation, the result shows:
This foliage fertilizer has significant effect of increasing production, and as paddy rice plot experiment output volume increase 14.8%, big area is used and increased 9-12%, corn 11.2%; Wheat 8.8%, peanut 11.3%, sugarcane 18.0%, vegetables 20% are with first-class, than several like product obvious effect of increasing production commonly used in the present production.
This product consumption is few, and cost is low, safety non-toxic, and effect stability is reliable, and using method is easy.
Have tangible economic benefit and social benefit, be subjected to the consistent of agricultural sector and welcome.

Claims (9)

1, a kind of high-efficiency multi-function foliage fertilizer is characterized in that it is made up of plant growth conditioning agent, antibiotic, micronutrient element, macronutrient and tensio-active agent:
Described plant growth conditioning agent is Plant hormones regulators,gibberellins, phytocytomine, αNai Yisuan, phenoxy acetic acid, 2,4-D, vitamins C, and its corresponding parts by weight are: 0-20,50-400,1-20,10-50,0-6,0-20;
Described antibiotic is new strysolin, and its parts by weight are 0-100;
Described micronutrient element is boron, zinc, manganese, magnesium, copper, molybdenum, and its corresponding parts by weight are 70-250,70-250,30-100,10-100,0-150,0-20;
Described macronutrient is nitrogen, phosphorus, potassium, and its corresponding parts by weight are respectively 5-60,50-100,70-120;
Described tensio-active agent is sodium dodecyl benzenylsulfonate, OP-10, tween 20, and its parts by weight are 5-20.
2, foliage fertilizer according to claim 1 is characterized in that Plant hormones regulators,gibberellins, phytocytomine, αNai Yisuan, phenoxy acetic acid, 2, and 4-D, ascorbic parts by weight are respectively: 0-10,100-250,2-10,15-40,0-4,0-10.
3, foliage fertilizer according to claim 2 is characterized in that Plant hormones regulators,gibberellins, phytocytomine, α-Nai Yisuan, phenoxy acetic acid, 2, and 4-D, ascorbic parts by weight are respectively: 0-5,100-200,4-10,15-30,1-3,0-8.
4, foliage fertilizer according to claim 1 is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
5, foliage fertilizer according to claim 2 is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
6, foliage fertilizer according to claim 3 is characterized in that phytocytomine is zeatin, kinetin, benzyladenine.
7, foliage fertilizer according to claim 1 is characterized in that micronutrient element is vitriol, nitrate, muriate, carbonate form, and boron then is the borate form.
8, foliage fertilizer according to claim 1 is characterized in that macronutrient is potassium primary phosphate, vitriolate of tartar, Repone K, urea, ammonium nitrate, volatile salt, ammonium sulfate, ammonium chloride, Secondary ammonium phosphate, primary ammonium phosphate, potassium-ammonium phosphate.
9, according to the preparation method of the described foliage fertilizer of claim 1-8, it is characterized in that:
(1) zinc, manganese, magnesium, copper, nitrogen, phosphorus, potassium compound raw material are mixed, under 70-100 ℃ of temperature dry 1-4 hour, pulverize, analyse through 80 mesh sieves and obtain work in-process (I);
(2) boric acid mixes with phytocytomine, grinds to reach 0.4-1.5 hour, and its work in-process (II) reach pH5-8;
(3) at Plant hormones regulators,gibberellins, phytocytomine, α-Nai Yisuan, phenoxy acetic acid, 2, in 4-D, vitamins C, the antibiotic mixture, add small amount of ethanol, grind evenly, obtain work in-process (III);
(4) above-mentioned work in-process (I) (II) (III) are mixed after, granularity is joined in the said mixture less than 100 purpose tensio-active agents, the limit edged stirs, up to the yellowish-yellow powder product that obtains good fluidity.
CN 92109659 1992-08-25 1992-08-25 Multi-functional high efficiency leave-fertilizer and related prepn. method Expired - Fee Related CN1025115C (en)

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