CN106699910A - 一种玉米变性淀粉的制备方法 - Google Patents
一种玉米变性淀粉的制备方法 Download PDFInfo
- Publication number
- CN106699910A CN106699910A CN201611170168.2A CN201611170168A CN106699910A CN 106699910 A CN106699910 A CN 106699910A CN 201611170168 A CN201611170168 A CN 201611170168A CN 106699910 A CN106699910 A CN 106699910A
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- CN
- China
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- weight
- cornstarch
- preparation
- corn starch
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002472 Starch Polymers 0.000 title claims abstract description 30
- 235000019698 starch Nutrition 0.000 title claims abstract description 30
- 239000008107 starch Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 240000008042 Zea mays Species 0.000 title abstract description 18
- 235000002017 Zea mays subsp mays Nutrition 0.000 title abstract description 18
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 title abstract description 17
- 235000005822 corn Nutrition 0.000 title abstract description 17
- 229920002261 Corn starch Polymers 0.000 claims abstract description 69
- 239000008120 corn starch Substances 0.000 claims abstract description 69
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000002002 slurry Substances 0.000 claims abstract description 25
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004382 Amylase Substances 0.000 claims abstract description 11
- 102000013142 Amylases Human genes 0.000 claims abstract description 11
- 108010065511 Amylases Proteins 0.000 claims abstract description 11
- 235000019418 amylase Nutrition 0.000 claims abstract description 11
- FDRCDNZGSXJAFP-UHFFFAOYSA-M sodium chloroacetate Chemical compound [Na+].[O-]C(=O)CCl FDRCDNZGSXJAFP-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 10
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 239000003054 catalyst Substances 0.000 claims abstract description 5
- 230000003647 oxidation Effects 0.000 claims abstract description 5
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 5
- 229940099112 cornstarch Drugs 0.000 claims description 65
- 239000002994 raw material Substances 0.000 claims description 34
- 229920000881 Modified starch Polymers 0.000 claims description 20
- -1 hydroxypropyl Chemical group 0.000 claims description 11
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical group [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 10
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims description 8
- 230000033228 biological regulation Effects 0.000 claims description 5
- 238000005119 centrifugation Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 238000009991 scouring Methods 0.000 claims description 5
- ANOBYBYXJXCGBS-UHFFFAOYSA-L stannous fluoride Chemical compound F[Sn]F ANOBYBYXJXCGBS-UHFFFAOYSA-L 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- LRWZZZWJMFNZIK-UHFFFAOYSA-N 2-chloro-3-methyloxirane Chemical compound CC1OC1Cl LRWZZZWJMFNZIK-UHFFFAOYSA-N 0.000 claims description 4
- 229910019213 POCl3 Inorganic materials 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000004132 cross linking Methods 0.000 claims 1
- 235000013372 meat Nutrition 0.000 abstract description 15
- 238000003860 storage Methods 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract 2
- 229920003012 Hydroxypropyl distarch phosphate Polymers 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000001310 hydroxy propyl distarch phosphate Substances 0.000 abstract 1
- 235000013825 hydroxy propyl distarch phosphate Nutrition 0.000 abstract 1
- DVROLKBAWTYHHD-UHFFFAOYSA-N hydroxy propyl distarch phosphate Chemical compound OC1C(O)C(OC)OC(CO)C1OC(O)CCOC1C(OC2C(C(O)C(OC3C(C(OP(O)(=O)OC4C(C(O)C(OC)OC4CO)O)C(C)OC3CO)O)OC2COC2C(C(O)C(OC)C(CO)O2)O)O)OC(CO)C(OC)C1O DVROLKBAWTYHHD-UHFFFAOYSA-N 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 7
- 239000013049 sediment Substances 0.000 description 7
- 229910019142 PO4 Inorganic materials 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 5
- 239000010452 phosphate Substances 0.000 description 5
- 238000004925 denaturation Methods 0.000 description 4
- 230000036425 denaturation Effects 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 235000015277 pork Nutrition 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical compound OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 description 3
- 229940005991 chloric acid Drugs 0.000 description 3
- 235000013622 meat product Nutrition 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 238000007654 immersion Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 102000005525 fibrillarin Human genes 0.000 description 1
- 108020002231 fibrillarin Proteins 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 235000009973 maize Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B31/00—Preparation of derivatives of starch
- C08B31/18—Oxidised starch
- C08B31/185—Derivatives of oxidised starch, e.g. crosslinked oxidised starch
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B31/00—Preparation of derivatives of starch
- C08B31/16—Ether-esters
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cereal-Derived Products (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611170168.2A CN106699910B (zh) | 2016-12-16 | 2016-12-16 | 一种玉米变性淀粉的制备方法 |
Applications Claiming Priority (1)
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CN201611170168.2A CN106699910B (zh) | 2016-12-16 | 2016-12-16 | 一种玉米变性淀粉的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN106699910A true CN106699910A (zh) | 2017-05-24 |
CN106699910B CN106699910B (zh) | 2019-10-25 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201611170168.2A Active CN106699910B (zh) | 2016-12-16 | 2016-12-16 | 一种玉米变性淀粉的制备方法 |
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CN (1) | CN106699910B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110194854A (zh) * | 2019-05-21 | 2019-09-03 | 广西高源淀粉有限公司 | 一种复合变性淀粉及其制备方法 |
CN110372806A (zh) * | 2019-07-30 | 2019-10-25 | 诸城兴贸玉米开发有限公司 | 一种乳胶手套隔离剂用变性淀粉 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101104642A (zh) * | 2007-07-26 | 2008-01-16 | 江门市科恒实业有限责任公司 | 复合变性淀粉的制备方法 |
CN101195692A (zh) * | 2008-01-04 | 2008-06-11 | 广西明阳生化科技股份有限公司 | 多元化预混法变性淀粉及其生产方法 |
CN101775161A (zh) * | 2009-01-12 | 2010-07-14 | 四川省蓬溪县弘桥实业有限公司 | 用微波远红外方法生产变性淀粉的工艺 |
CN102391797A (zh) * | 2011-07-09 | 2012-03-28 | 山西大学 | 建筑用玉米淀粉胶粘剂及其制备方法 |
CN104543663A (zh) * | 2014-11-28 | 2015-04-29 | 安徽紫山农业科技有限公司 | 一种玉米变性淀粉 |
CN106008728A (zh) * | 2016-06-30 | 2016-10-12 | 陈灼 | 一种变性淀粉的制备方法 |
-
2016
- 2016-12-16 CN CN201611170168.2A patent/CN106699910B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101104642A (zh) * | 2007-07-26 | 2008-01-16 | 江门市科恒实业有限责任公司 | 复合变性淀粉的制备方法 |
CN101195692A (zh) * | 2008-01-04 | 2008-06-11 | 广西明阳生化科技股份有限公司 | 多元化预混法变性淀粉及其生产方法 |
CN101775161A (zh) * | 2009-01-12 | 2010-07-14 | 四川省蓬溪县弘桥实业有限公司 | 用微波远红外方法生产变性淀粉的工艺 |
CN102391797A (zh) * | 2011-07-09 | 2012-03-28 | 山西大学 | 建筑用玉米淀粉胶粘剂及其制备方法 |
CN104543663A (zh) * | 2014-11-28 | 2015-04-29 | 安徽紫山农业科技有限公司 | 一种玉米变性淀粉 |
CN106008728A (zh) * | 2016-06-30 | 2016-10-12 | 陈灼 | 一种变性淀粉的制备方法 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110194854A (zh) * | 2019-05-21 | 2019-09-03 | 广西高源淀粉有限公司 | 一种复合变性淀粉及其制备方法 |
CN110372806A (zh) * | 2019-07-30 | 2019-10-25 | 诸城兴贸玉米开发有限公司 | 一种乳胶手套隔离剂用变性淀粉 |
Also Published As
Publication number | Publication date |
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CN106699910B (zh) | 2019-10-25 |
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PB01 | Publication | ||
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TA01 | Transfer of patent application right | ||
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Effective date of registration: 20190926 Address after: 235200 Xuezhuang village, Shengquan Township, Xiao County, Suzhou City, Anhui Province Applicant after: Anhui Golden Maize Agricultural Science and Technology Development Co.,Ltd. Address before: The six row West Town Road 547399 the Guangxi Zhuang Autonomous Region Tian'e County Hechi City No. 42 Applicant before: TIAN'E COUNTY QUANSHENG BEE INDUSTRY TECHNOLOGY Co.,Ltd. |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of corn modified starch Effective date of registration: 20211217 Granted publication date: 20191025 Pledgee: Suzhou SME financing Company limited by guarantee Pledgor: Anhui Golden Maize Agricultural Science and Technology Development Co.,Ltd. Registration number: Y2021980015278 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20221110 Granted publication date: 20191025 Pledgee: Suzhou SME financing Company limited by guarantee Pledgor: Anhui Golden Maize Agricultural Science and Technology Development Co.,Ltd. Registration number: Y2021980015278 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Preparation Method of Corn Modified Starch Effective date of registration: 20221125 Granted publication date: 20191025 Pledgee: Suzhou SME financing Company limited by guarantee Pledgor: Anhui Golden Maize Agricultural Science and Technology Development Co.,Ltd. Registration number: Y2022980023589 |
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