CN106387605A - Special compound liquid preservative for foods - Google Patents

Special compound liquid preservative for foods Download PDF

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Publication number
CN106387605A
CN106387605A CN201610769569.3A CN201610769569A CN106387605A CN 106387605 A CN106387605 A CN 106387605A CN 201610769569 A CN201610769569 A CN 201610769569A CN 106387605 A CN106387605 A CN 106387605A
Authority
CN
China
Prior art keywords
hydroxybenzoate
parts
liquid preservative
food
tea
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610769569.3A
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Chinese (zh)
Inventor
茆振斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUHU HUAHAI BIOLOGY ENGINEERING Co Ltd
Original Assignee
WUHU HUAHAI BIOLOGY ENGINEERING Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WUHU HUAHAI BIOLOGY ENGINEERING Co Ltd filed Critical WUHU HUAHAI BIOLOGY ENGINEERING Co Ltd
Priority to CN201610769569.3A priority Critical patent/CN106387605A/en
Publication of CN106387605A publication Critical patent/CN106387605A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3481Organic compounds containing oxygen
    • A23L3/3508Organic compounds containing oxygen containing carboxyl groups
    • A23L3/3517Carboxylic acid esters
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3472Compounds of undetermined constitution obtained from animals or plants
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3481Organic compounds containing oxygen
    • A23L3/349Organic compounds containing oxygen with singly-bound oxygen
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Botany (AREA)
  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a special compound liquid preservative for foods. The special compound liquid preservative is prepared from the following components in parts by weight: 1.2-1.5 parts of methyl 4-hydroxybenzoate, 0.5-0.9 part of ethyl p-hydroxybenzoate, 0.2-0.5 part of propylparaben, 1-1.5 parts of butylphydroxybenzoate, 0.6-0.8 part of isobutyl p-hydroxybenzoate, 2-3 parts of phenoxyethanol and 2-6 parts of a tea leaf extracting solution. The special compound liquid preservative disclosed by the invention is compounded from the methyl 4-hydroxybenzoate, the ethyl p-hydroxybenzoate, the propylparaben, the butylphydroxybenzoate, the isobutyl p-hydroxybenzoate and the phenoxyethanol, and various substances have good synergistic effects, so that the special compound liquid preservative is better in antiseptic effects, the solubility is improved, antibacterial properties are excellent, the applicable pH range is wide, and the special compound liquid preservative has the advantages of being small in dosage, good in antiseptic effects and small in toxicity.

Description

A kind of special compounding liquid preservative of food
Technical field
The present invention relates to food preservative technical field, the special compounding liquid preservative of specifically a kind of food.
Background technology
With the reform of China's economic system, the yield of the various agricultural byproducts such as water fruits and vegetables is significantly increased production, for China The development of food industry, provides wide raw materials market, and this is diversified, flavoured, efficient with regard to an urgent demand food and drink Change and storage-stable etc..The great variety of this structure be unable to do without the additive of food and drink, such as flavorant, fortification Agent, food quality modifying agent, food preservative etc..Wherein food preservative is that a class is important, and is the maximum food of consumption Product additive.The food preservative that countries in the world use at present is planted more than more than 50, as many as existing 25 kinds of Japan, and with to hydroxyl Based on yl benzoic acid esters and sorbic acid.China is at present still based on Sodium Benzoate and potassium sorbate.Kind is dull, antiseptic effect Difference, is China's subject matter that food preservative market exists at present.Therefore, research and development and application scope is wide, favorable anti-corrosion effect, Small toxicity, the low Novel series preservative of integrated cost, to adapt to the needs of Chinese food industrial development, imperative.
Parabens is one of preservative of commonly using.It can suppress the breathing enzyme system of microbial cell with The activity of transmission enzyme system, and destroy the cell membrane mechanism of microorganism, thus there is extensive antibacterial to make to mould, yeast and bacterium With.Its antibacterial ability is stronger than sorbic acid and benzoic acid, and antibacterial action is affected less by ph value, imitates in the range of ph value 4~8 Fruit is all good.
Methyl p-hydroxybenzoate, is methyl hydroxybenzoate, white crystalline powder or colourless crystallization again, is soluble in alcohol, ether and Acetone, atomic is dissolved in water, 270-280 DEG C of boiling point.It is mainly used as organic synthesis, food, cosmetics, the sterilization antiseptic of medicine, Also serve as in feed anticorrosion agent.
Phenoxyethanol, is medicine name, and English name is:Phenoxyethanol, Chinese name is two phenoxetols, benzene again Ethoxy-ethanol etc., molecular formula is:C8H10O2, Phenoxyethanol belongs to organic synthesis thing, is colourless slightly band viscous liquid, micro-perfume, puckery. Water insoluble, arbitrarily can mix with acetone, ethanol and glycerine.
Content of the invention
It is an object of the invention to provide a kind of special compounding liquid preservative of food.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of special compounding liquid preservative of food is it is characterised in that be grouped into by the group of following weight portion:Para hydroxybenzene Methyl formate 1.2-1.5 part, ethyl-para-hydroxybenzoate 0.5-0.9 part, propylparaben 0.2-0.5 part, to hydroxyl Butyl benzoate 1-1.5 part, p-Hydroxybenzoic acid isobutyl ester 0.6-0.8 part, Phenoxyethanol 2-3 part, tea extract 2-6 part.
Scheme, is grouped into by the group of following weight portion further:1.3 parts of methyl p-hydroxybenzoate, P-hydroxybenzoic acid 0.7 part of ethyl ester, 0.4 part of propylparaben, 1.3 parts of butyl p-hydroxybenzoate, p-Hydroxybenzoic acid isobutyl ester 0.7 Part, 2.5 parts of Phenoxyethanol, 4 parts of tea extract.
Scheme further, described tea extract is obtained by following methods:80 mesh sieves pulverized by tealeaves, by 1: 20 tea Weight part ratio adds distilled water, and 60min, centrifugation, filtration are extracted in stirring at a temperature of 40-60 DEG C, obtain tea extract.
Further scheme, described tealeaves is green tea, at least one in black tea.
The present invention also provides a kind of application in food fresh keeping for compounding liquid preservative.
Beneficial effects of the present invention:The present invention compounds liquid preservative by methyl p-hydroxybenzoate, P-hydroxybenzoic acid Ethyl ester, propylparaben, butyl p-hydroxybenzoate, p-Hydroxybenzoic acid isobutyl ester, Phenoxyethanol compound and form, respectively Plant material and there is good synergy, there is more preferable antiseptic effect, increase solubility, excellent, the applicable pH of anti-microbial property Scope is wide, and it is few to have a consumption, favorable anti-corrosion effect, the advantage of small toxicity.
Specific embodiment
With reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
A kind of special compounding liquid preservative of food, is grouped into by the group of following weight portion:Methyl p-hydroxybenzoate 1.2 Part, 0.9 part of ethyl-para-hydroxybenzoate, 0.5 part of propylparaben, 1 part of butyl p-hydroxybenzoate, para hydroxybenzene first 0.6 part of sour isobutyl ester, 2 parts of Phenoxyethanol, 6 parts of tea extract.
Tea extract is obtained by following methods:Black tea leaf pulverized 80 mesh sieves, added by 1: 20 tea weight part ratio Enter distilled water, 60min, centrifugation, filtration are extracted in stirring at a temperature of 60 DEG C, obtain tea extract.
Embodiment 2
A kind of special compounding liquid preservative of food, is grouped into by the group of following weight portion:Methyl p-hydroxybenzoate 1.5 Part, 0.5 part of ethyl-para-hydroxybenzoate, 0.2 part of propylparaben, 1.5 parts of butyl p-hydroxybenzoate, para hydroxybenzene 0.8 part of iso-butyl formate, 3 parts of Phenoxyethanol, 2 parts of tea extract.
Tea extract is obtained by following methods:Green tea pulverized 80 mesh sieves, added by 1: 20 tea weight part ratio Enter distilled water, 60min, centrifugation, filtration are extracted in stirring at a temperature of 50 DEG C, obtain tea extract.
Embodiment 3
A kind of special compounding liquid preservative of food, is grouped into by the group of following weight portion:Methyl p-hydroxybenzoate 1.3 Part, 0.7 part of ethyl-para-hydroxybenzoate, 0.4 part of propylparaben, 1.3 parts of butyl p-hydroxybenzoate, para hydroxybenzene 0.7 part of iso-butyl formate, 2.5 parts of Phenoxyethanol, 4 parts of tea extract.
Tea extract is obtained by following methods:Black tea and green tea, with 1: 1 weight ratio mixing, pulverized 80 mesh sieves, by 1 : 20 tea weight part ratio adds distilled water, and 60min, centrifugation, filtration are extracted in stirring at a temperature of 40-60 DEG C, obtain tealeaves and extract Liquid.
The preservatives such as the compounding liquid preservative of embodiment 1-3 preparation, potassium sorbate, calcium propionate and Sodium Benzoate are carried out Test and comparison.
Test material:Soybean vegetarian, halogen asparagus, spiced egg, add preservative, finished product food
Wherein, the addition of preservative is 0.1wt%.
Finished product food is placed in 30 DEG C through vacuum packaging, under relative humidity 85% environment.Concrete data, is shown in Table 1.
Table 1
The present invention compounds the time that liquid preservative significantly improves food antiseptic.
The above-mentioned description to embodiment is to be understood that for ease of those skilled in the art and apply this Bright.Person skilled in the art obviously easily can make various modifications to case study on implementation, and described herein one As principle be applied in other embodiment without through performing creative labour.Therefore, the invention is not restricted to enforcement case here Example, according to the announcement of the present invention, the improvement made without departing from scope and modification all should be for those skilled in the art Within protection scope of the present invention.

Claims (5)

1. a kind of special compounding liquid preservative of food is it is characterised in that be grouped into by the group of following weight portion:Para hydroxybenzene first Sour methyl esters 1.2-1.5 part, ethyl-para-hydroxybenzoate 0.5-0.9 part, propylparaben 0.2-0.5 part, para hydroxybenzene Butyl formate 1-1.5 part, p-Hydroxybenzoic acid isobutyl ester 0.6-0.8 part, Phenoxyethanol 2-3 part, tea extract 2-6 part.
2. a kind of special compounding liquid preservative of food according to claim 1 is it is characterised in that by following weight portion Group is grouped into:1.3 parts of methyl p-hydroxybenzoate, 0.7 part of ethyl-para-hydroxybenzoate, 0.4 part of propylparaben, right 1.3 parts of butoben, 0.7 part of p-Hydroxybenzoic acid isobutyl ester, 2.5 parts of Phenoxyethanol, 4 parts of tea extract.
3. a kind of special compounding liquid preservative of food according to claim 1 and 2 is it is characterised in that described tealeaves carries Liquid is taken to be obtained by following methods:80 mesh sieves pulverized by tealeaves, and the tea weight part ratio by 1: 20 adds distilled water, at 40-60 DEG C At a temperature of stirring extract 60min, centrifugation, filter, obtain tea extract.
4. the special compounding liquid preservative of a kind of food according to claim 3 is it is characterised in that described tealeaves is green At least one in tea, black tea.
5. application in food fresh keeping for a kind of compounding liquid preservative.
CN201610769569.3A 2016-08-30 2016-08-30 Special compound liquid preservative for foods Pending CN106387605A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610769569.3A CN106387605A (en) 2016-08-30 2016-08-30 Special compound liquid preservative for foods

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Application Number Priority Date Filing Date Title
CN201610769569.3A CN106387605A (en) 2016-08-30 2016-08-30 Special compound liquid preservative for foods

Publications (1)

Publication Number Publication Date
CN106387605A true CN106387605A (en) 2017-02-15

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102599613A (en) * 2011-12-03 2012-07-25 天津北洋百川生物技术有限公司 Selection and application of compound antiseptic
CN103385241A (en) * 2013-08-19 2013-11-13 广州博嘉生物科技有限公司 Compound preservative and application thereof
CN104800134A (en) * 2015-05-19 2015-07-29 胡红慧 Preservative for skin care product
CN105520041A (en) * 2014-09-29 2016-04-27 李元生 Preparation method of wild garlic preservative

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102599613A (en) * 2011-12-03 2012-07-25 天津北洋百川生物技术有限公司 Selection and application of compound antiseptic
CN103385241A (en) * 2013-08-19 2013-11-13 广州博嘉生物科技有限公司 Compound preservative and application thereof
CN105520041A (en) * 2014-09-29 2016-04-27 李元生 Preparation method of wild garlic preservative
CN104800134A (en) * 2015-05-19 2015-07-29 胡红慧 Preservative for skin care product

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