CN106281680A - A kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application - Google Patents
A kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application Download PDFInfo
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- CN106281680A CN106281680A CN201610736752.3A CN201610736752A CN106281680A CN 106281680 A CN106281680 A CN 106281680A CN 201610736752 A CN201610736752 A CN 201610736752A CN 106281680 A CN106281680 A CN 106281680A
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- quick
- cigarette
- herba menthae
- fried pearl
- cool taste
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application.Cool taste Mint Essence formula of the present invention is by forming according to the component of mass percentage as follows: Mentholum 1 8%, menthyl lactate 1 10%, and menthyl acetate 1 5%, coolant agent 0.2 0.5%, surplus are fat solvent.The present invention can make the mint flavored and cool feeling that imparting Medicated cigarette is natural when quick-fried pearl pinches brokenly, and without the medicinal herbs breath of Mentholum and zest, can well merge with cigarette flavor, be effectively improved the comfort of cigarette smoking, promote cigarette smoking quality.
Description
Technical field
The present invention relates to a kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method and application, belong to flavouring essence for tobacco
Spice technical field.
Background technology
Pursue " newly ", " very ", " special ", be the main flow psychological peculiarity in cigarette consumption market forever.To answer after essence capsule
For Field of Tobacco, it is possible not only to bring " newly ", " very ", the bright spot of " special " to Medicated cigarette, it is also possible to solve tradition essence applying side
The difficult problems such as the essence holdup time that formula exists is short, and essence release is uneven.
Herba Menthae quick-fried pearl Medicated cigarette is as a market segmentation most important in quick-fried pearl cigarette market, always deeply by the heat of consumer
Hold in both hands, and market share is continuing to increase.From pure this perfume of Nicotiana tabacum L., to pinching brokenly cool peppermint taste after quick-fried pearl, the quick-fried pearl of Herba Menthae
Medicated cigarette is that consumer provides two kinds and different sucks mode.But, current cigarette market is sold Herba Menthae quick-fried pearl Medicated cigarette, is made
Essence main component be Mentholum, when suction, consumer can feel that one refrigerant breath enters throat, bring subsequently
Be bad breath and the oral stimulation of medicinal herbs specific to Mentholum, and and Nicotiana tabacum L. this perfume degrees of fusion bad, Herba Menthae cool feeling is held
The continuous time is short.
Therefore, using quick-fried pearl for Herba Menthae quick-fried pearl Medicated cigarette, the research carrying out the removal bad breath of medicinal herbs has highly important
Meaning.
Summary of the invention
It is an object of the invention to provide a kind of quick-fried pearl of Herba Menthae cigarette cool taste Mint Essence and preparation method thereof.The present invention's is thin
The quick-fried pearl of lotus cigarette can make the natural mint flavored and cool feeling of imparting Medicated cigarette with cool taste Mint Essence when quick-fried pearl pinches brokenly, and without thin
The medicinal herbs breath of lotus brain and zest, well can merge with cigarette flavor, is effectively improved the comfort of cigarette smoking, promotes volume
Cigarette suction quality.
It is a further object of the present invention to provide above-mentioned cool taste Mint Essence purposes in preparation Herba Menthae quick-fried pearl Medicated cigarette.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of quick-fried pearl of Herba Menthae cigarette with cool taste Mint Essence, is made up of the raw material of following mass percent:
Mentholum 1-8%, menthyl lactate 1-10%, menthyl acetate 1-5%, coolant agent 0.2-0.5%, surplus is oil
Fatsolvent；
Preferably, this quick-fried pearl of Herba Menthae cigarette with cool taste Mint Essence, is made up of the raw material of following mass percent:
Mentholum 2-4%, menthyl lactate 1-2%, menthyl acetate 1-2%, coolant agent 0.2-0.4%, surplus is oil
Fatsolvent.
One or more in Semen Maydis oil, olive oil or neodecanoic acid glyceride of described fat solvent.
Described coolant agent is selected from carbonic acid MENTHOL glycol ester (FEMA:3805), L-menthone glycerol ketal
(FEMA:3807), N-ethyl-menthyl Methanamide (FEMA:3455), L-TK-10 (FEMA:3784) or cool taste
One or more in agent WS-3.
This quick-fried pearl of Herba Menthae cigarette preparation method of cool taste Mint Essence, comprises the following steps:
(1) coolant agent is dissolved in propylene glycol, makes the solution that mass fraction is 8-12%；
(2) in the solution of step (1), add Mentholum, menthyl lactate and menthyl acetate, add fat solvent,
Mix homogeneously, to obtain final product.
Preferably, in step (1), coolant agent is dissolved in propylene glycol, makes the solution that mass fraction is 10%.
The above-mentioned quick-fried pearl of Herba Menthae cigarette with cool taste Mint Essence preparation the quick-fried pearl of Herba Menthae cigarette or Herba Menthae quick-fried pearl Medicated cigarette in purposes also
It it is protection scope of the present invention.
The present invention also provides for a kind of quick-fried pearl of Herba Menthae cigarette, containing the above-mentioned cool taste Mint Essence of effective dose.
The preparation method of this quick-fried pearl of Herba Menthae cigarette, step is as follows:
Olive oil and decanoyl/octanoyl glycerides 1:2 by volume are mixed, then presses olive oil and decanoyl/octanoyl glycerides gross weight
0.2-0.5% add emulsifying agent, then stir, whipping process add the cool taste minty note of the above-mentioned quick-fried pearl of Herba Menthae cigarette
Essence, addition is olive oil and the 1-2% of decanoyl/octanoyl glycerides gross weight, is further continued for stirring 0.5h, completes process for preparation, finally
Make the quick-fried pearl of Herba Menthae cigarette.
Preferably, described emulsifying agent is sorbester p17.
The present invention also provides for a kind of Herba Menthae quick-fried pearl Medicated cigarette, containing the above-mentioned quick-fried pearl of Herba Menthae cigarette.
The beneficial effects of the present invention is:
(1) for removing the medicinal herbs breath of Mentholum, the quick-fried pearl of Herba Menthae cigarette of the present invention decreases Herba Menthae with cool taste Mint Essence
The consumption of brain, is simultaneously introduced menthyl lactate and menthyl acetate, and wherein, menthyl lactate has slight Herba Menthae fragrance, but accompanies
There is lasting, pleasant cooling effect；Menthyl acetate has soft Herba Menthae and Flos Rosae Rugosae fragrance, passes through menthyl lactate
With the addition of menthyl acetate, mask the medicinal herbs breath of Mentholum further, and it is clear to overcome single use Mentholum
The shortcoming that cool effect is strong and very brief.Additionally, for preventing from causing the reduction of cooling effect because of the minimizing of Mentholum addition, this
Invention has been also added with coolant agent on the quick-fried pearl of Herba Menthae cigarette with in cool taste Mint Essence, and coolant agent is optimized investigation, through sense
Official's evaluation comparison, the coolant agent that the present invention is added can increase the harmonious feeling of cool taste, stay taste the longest, and cool taste is pure and fresh, long-acting, without bitter
Taste.
(2) the quick-fried pearl of Herba Menthae cigarette of the present invention cool taste Mint Essence, the solvent that this essence and quick-fried pearl are wrapped up can dissolve each other,
Quick-fried pearl wall material can be covered completely and bad breath that solvent brings.
(3) through quick-fried pearl pilot production, quick-fried pearl stability is preferable, and otch is little, and producing quick-fried pearl does not has any impact.
(4) by adding the above-mentioned quick-fried pearl containing cool taste Mint Essence in mouth rod, quick-fried pearl is pinched brokenly by aspiration procedure, energy
Well merging with cigarette flavor, be effectively improved the comfort of cigarette smoking, natural mint flavored and cool feeling is lasting.
(5) the quick-fried pearl of Herba Menthae cigarette of the present invention is easy, with low cost by cool taste Mint Essence preparation method, can be used for extensive
Industrialized production, has the strongest practicality.
(6) the quick-fried pearl of Herba Menthae cigarette of the present invention is with in cool taste Mint Essence, and each raw material components is an organic whole, lacks one
Can not.Inventor finds in R&D process, reduces any one of above-mentioned cool taste Mint Essence raw material components, or to have
The raw material components of the raw material of similar performance taste cool to present invention Mint Essence is replaced (as replaced this by isovaleric acid menthyl ester
Menthyl acetate in bright), the action effect of the coolest taste Mint Essence entirety significantly reduces；Cool taste Mint Essence in the present invention
On the basis of be further added by other raw material components, the whole structure of cool taste Mint Essence does not improve significantly, and even has cool
The situation that the whole structure of taste Mint Essence reduces occurs.
Detailed description of the invention
The present invention is further illustrated in conjunction with the embodiments, it should explanation, and following embodiment is merely to explain
The present invention, is not defined its content.
Embodiment 1: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
Raw material forms:
By mass percentage, it is prepared from the following materials:
Mentholum 2%, menthyl lactate 1%, menthyl acetate 1%, coolant agent 0.2%, surplus is olive oil.
Mentholum, menthyl acetate and menthyl lactate used in the present embodiment is fragrantly rich purchased from Jinan, Shandong Province nine divisions of China in remote antiquity
Material Co., Ltd；Coolant agent used is purchased from Jishui, Jiangxi Lian Xing perfumery oil company limited, trade name WS-3.
The physicochemical property of each raw material and odor characteristic such as table 1:
Table 1:
The preparation method of this cool taste Mint Essence is:
(1) coolant agent is dissolved in propylene glycol, makes the solution that mass fraction is 10%；
(2) in the solution of step (1), add Mentholum, menthyl lactate and menthyl acetate, add fat solvent
(olive oil), mix homogeneously, to obtain final product.
Embodiment 2: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
Raw material forms:
By mass percentage, it is prepared from the following materials:
Mentholum 4%, menthyl lactate 1%, menthyl acetate 2%, coolant agent 0.4%, surplus is neodecanoic acid glyceride.
The source of Mentholum, menthyl lactate, menthyl acetate and coolant agent is with embodiment 1.
The preparation method of this cool taste Mint Essence is with embodiment 1.
Embodiment 3: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
Raw material forms:
By mass percentage, it is prepared from the following materials:
Mentholum 1%, menthyl lactate 10%, menthyl acetate 1%, coolant agent 0.5%, surplus is olive oil.
Mentholum, menthyl lactate, menthyl acetate source with embodiment 1.
Coolant agent is L-menthone glycerol ketal (FEMA:3807).
The preparation method of this cool taste Mint Essence is with embodiment 1.
Embodiment 4: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
Raw material forms:
By mass percentage, it is prepared from the following materials:
Mentholum 8%, menthyl lactate 1%, menthyl acetate 5%, coolant agent 0.2%, surplus is olive oil.
Mentholum, menthyl lactate, menthyl acetate source with embodiment 1.
Coolant agent is N-ethyl-menthyl Methanamide (FEMA:3455).
The preparation method of this cool taste Mint Essence is with embodiment 1.
Application examples 1: the preparation of the quick-fried pearl of Herba Menthae cigarette
Preparation method is as follows:
Olive oil and decanoyl/octanoyl glycerides 1:2 by volume are mixed, then presses olive oil and decanoyl/octanoyl glycerides gross weight
0.3% addition emulsifying agent (sorbester p17), then stir, in whipping process add above-described embodiment 1 preparation Herba Menthae
The quick-fried pearl of cigarette is olive oil and the 1.5% of decanoyl/octanoyl glycerides gross weight with cool taste Mint Essence, addition, is further continued for stirring
0.5h, completes process for preparation, is eventually fabricated the quick-fried pearl of Herba Menthae cigarette.
Application examples 2: the preparation of the quick-fried pearl of Herba Menthae cigarette
Preparation method is as follows:
Olive oil and decanoyl/octanoyl glycerides 1:2 by volume are mixed, then presses olive oil and decanoyl/octanoyl glycerides gross weight
0.3% addition emulsifying agent (sorbester p17), then stir, in whipping process add above-described embodiment 2 preparation Herba Menthae
The quick-fried pearl of cigarette is olive oil and the 2% of decanoyl/octanoyl glycerides gross weight with cool taste Mint Essence, addition, is further continued for stirring 0.5h,
Complete process for preparation, be eventually fabricated the quick-fried pearl of Herba Menthae cigarette.
Sensory quality assessment is tested:
The cool quick-fried pearl of taste Herba Menthae in application examples 1-2 is added in cigarette filter rod, carries out with reference to GB sensory evaluation way
Evaluate, aspiration procedure is pinched brokenly quick-fried pearl.Group of smokeing panel test is made up of 9 Medicated cigarette sensory evaluation experts, uses and secretly comments mode to carry out
Sensory quality assessment, sensory quality assessment table is as shown in table 2:
Table 2:
From table 2 it can be seen that the present invention can make the mint flavored and cool feeling that imparting Medicated cigarette is natural when quick-fried pearl pinches brokenly, and
Without medicinal herbs breath and the zest of Mentholum, can well merge with cigarette flavor, be effectively improved the comfort of cigarette smoking,
Promote cigarette smoking quality.
Comparative example 1: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
The plurality of raw materials with similar performance is investigated and has been studied in R&D process by the present inventor, and result is sent out
Existing, even if the performance between certain several raw material is similar, but after the material combination different from other uses, the effect that its entirety is realized
Really significant difference.Such as, the investigation of the menthyl ester for using with Mentholum compatibility, the present invention is by the raw material prescription of embodiment 1
In menthyl lactate replace with menthyl carbonates, menthyl acetate is replaced with isovaleric acid menthyl ester, the consumption of each raw material and
Preparation method, with embodiment 1, prepares cool taste Mint Essence.
The cool taste Mint Essence of preparation is made the quick-fried pearl of Herba Menthae cigarette by the method for application examples 1, and the cool quick-fried pearl of taste Herba Menthae is added
It is added in cigarette filter rod, is evaluated with reference to GB sensory evaluation way, aspiration procedure is pinched brokenly quick-fried pearl, carries out aesthetic quality
Evaluate, it was found that the quick-fried pearl cigarette prepared by the cool taste Mint Essence of comparative example 1 is still with the medicinal herbs breath of Mentholum, Herba Menthae
The cool feeling persistent period is shorter, and nose larynx is had stimulation.
Comparative example 2: the Herba Menthae cigarette quick-fried pearl preparation of cool taste Mint Essence
In cool taste Mint Essence, the consumption of each raw material can produce crucial effect to the overall performance of cool taste Mint Essence, this
Person of good sense's content to each raw material in cool taste Mint Essence in R&D process has carried out the research of investigation and action effect, knot
Fruit finds, inappropriate proportioning raw materials relation, its action effect significant difference.Such as: by the use of menthyl lactate in embodiment 1
Amount is adjusted to 15%, and the consumption of menthyl acetate is adjusted to 0.5%, and the consumption of coolant agent is adjusted to 1.0%, the use of other raw materials
Amount is with embodiment 1, and prepares as described in Example 1.
The cool taste Mint Essence of preparation is made the quick-fried pearl of Herba Menthae cigarette by the method for application examples 1, and the cool quick-fried pearl of taste Herba Menthae is added
It is added in cigarette filter rod, is evaluated with reference to GB sensory evaluation way, aspiration procedure is pinched brokenly quick-fried pearl, carries out aesthetic quality
Evaluate, it was found that the quick-fried pearl cigarette prepared by the cool taste Mint Essence of comparative example 2 is still with the medicinal herbs breath of Mentholum, flue gas
Thin, the Herba Menthae cool feeling persistent period is shorter, and nose larynx is had stimulation.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-described embodiment
Limiting, one of ordinary skill in the art should be understood that, on the basis of technical scheme, those skilled in the art need not
Pay various amendments or deformation that creative work can make still within protection scope of the present invention.
Claims (10)
1. the quick-fried pearl of Herba Menthae cigarette is with cool taste Mint Essence, it is characterised in that be made up of the raw material of following mass percent:
Mentholum 1-8%, menthyl lactate 1-10%, menthyl acetate 1-5%, coolant agent 0.2-0.5%, surplus is that oils and fats is molten
Agent.
2. the quick-fried pearl of Herba Menthae cigarette as claimed in claim 1 is with cool taste Mint Essence, it is characterised in that by following mass percent
Raw material is made:
Mentholum 2-4%, menthyl lactate 1-2%, menthyl acetate 1-2%, coolant agent 0.2-0.4%, surplus is that oils and fats is molten
Agent.
3. the quick-fried pearl of Herba Menthae cigarette as claimed in claim 1 or 2 is with cool taste Mint Essence, it is characterised in that the choosing of described fat solvent
One or more in Semen Maydis oil, olive oil or neodecanoic acid glyceride.
4. the quick-fried pearl of Herba Menthae cigarette as claimed in claim 1 or 2 is with cool taste Mint Essence, it is characterised in that described coolant agent is selected from
Carbonic acid MENTHOL glycol ester, L-menthone glycerol ketal, N-ethyl-menthyl Methanamide, L-TK-10
Or one or more in coolant agent WS-3.
5. the Herba Menthae cigarette quick-fried pearl preparation method of cool taste Mint Essence described in any one of claim 1-4, comprises the following steps:
(1) coolant agent is dissolved in propylene glycol, makes the solution that mass fraction is 8-12%；
(2) in the solution of step (1), add Mentholum, menthyl lactate and menthyl acetate, add fat solvent, mixing
Uniformly, to obtain final product.
6. preparation method as claimed in claim 5, it is characterised in that in step (1), coolant agent is dissolved in propylene glycol,
Make the solution that mass fraction is 10%.
7. the quick-fried pearl of Herba Menthae cigarette described in any one of claim 1-4 is quick-fried on the preparation quick-fried pearl of Herba Menthae cigarette or Herba Menthae with cool taste Mint Essence
Purposes in pearl Medicated cigarette.
8. the quick-fried pearl of Herba Menthae cigarette, it is characterised in that the cool taste minty note described in any one of claim 1-4 containing effective dose
Essence.
9. the preparation method of the quick-fried pearl of Herba Menthae cigarette described in claim 8, it is characterised in that step is as follows:
Olive oil and decanoyl/octanoyl glycerides 1:2 by volume are mixed, then presses olive oil and decanoyl/octanoyl glycerides gross weight
0.2-0.5% adds emulsifying agent, then stirs, and adds the Herba Menthae described in any one of claim 1-4 in whipping process
The quick-fried pearl of cigarette is olive oil and the 1-2% of decanoyl/octanoyl glycerides gross weight with cool taste Mint Essence, addition, is further continued for stirring
0.5h, completes process for preparation, is eventually fabricated the quick-fried pearl of Herba Menthae cigarette.
10. a Herba Menthae quick-fried pearl Medicated cigarette, it is characterised in that containing the quick-fried pearl of Herba Menthae cigarette described in claim 8.
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| CN201610736752.3A CN106281680B (en) | 2016-08-27 | 2016-08-27 | A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof |
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| CN201610736752.3A CN106281680B (en) | 2016-08-27 | 2016-08-27 | A kind of quick-fried pearl of peppermint cigarette cool taste Mint Essence and the preparation method and application thereof |
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| CN106942781A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of chrysanthemum and its application in cigarette |
| CN107034017A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette |
| CN107142153A (en) * | 2017-04-27 | 2017-09-08 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl matrimony vine essence and its application in cigarette |
| CN107641557A (en) * | 2017-10-31 | 2018-01-30 | 鹰潭中投科技有限公司 | MoonlIght on the Lotus Pond artistic conception flavouring essence for tobacco and its preparation method and application |
| CN107802031A (en) * | 2017-10-18 | 2018-03-16 | 汉寿亿达新材料科技有限公司 | A kind of quick-fried pearl of cigarette |
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| CN115252446A (en) * | 2022-08-09 | 2022-11-01 | 广州途富香料科技有限公司 | Composite cooling agent and application thereof in preparation of oral cleaning products |
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