CN1062745C - Shuangshi Zaishengjing oral liquor and preparation method thereof - Google Patents
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Abstract
The present invention relates to a Shuangshizaishengjing oral liquid which belongs to a Chinese medicine preparation for mainly treating impotence and a preparation method thereof. The oral liquid is prepared by mixing the alcohol extracting solution of hairy deer-horn, ant and tokay gecko with the distilled spirit soaking solution of male silkworm moth and the decoction of epimedium herb, desertliving cistanche, tuber onion seed, giant knotweed rhizome and milkvetch root. The oral liquid is used for treating impotence, prospermia, etc., and has the advantages of high therapeutic effect, short course, no side effect, convenient and simple preparation, and low cost; the oral liquid not only is easy to preserve and carry, but also is convenient to take; clinical trial proves that the oral liquid has the functions of warming the kidney to invigorate yang, tonifying the kidney, replenishing essence, strengthening erection and increasing the sexual feeling of men and women each other, and the oral liquid belongs to a good Chinese medicine preparation for treating impotence.
Description
The present invention relates to a kind of Shuangshi Zhaishengjin oral liquid and its preparation ,method, particularly a kind of Chinese medicine oral liquid that is mainly used in treatment impotence disease and preparation method thereof.
Because improving constantly of living standards of the people, seeking needs especially to the new drug of the health care of healthy and helpful and taking convenience, impotence deficiency is one of andrology's commonly encountered diseases, the sickness rate of impotence deficiency is in rising trend in recent years, account for about 10% of adult male according to statistics, especially the middle-aged and elderly people patient is in the majority, brings very big worries for I and family, even influences the harmony of work and family.Since the eighties, along with the development of spermology, improved the theoretic knowledge to sexual impotence, and obtained clinical treatment experience, utilization traditional Chinese medical herbal treatment sexual impotence obtains better effects.In the present used Chinese medicine, contain valuable ingredient of Chinese medicine more, the cost height, the Chinese medicine poor effect that has, the course of treatment is long, takes effect slowly; Many Chinese medicine toxic side effects, and take inconvenience.Chinese invention patent " preparation method of a kind of strengthen ' Yang ' nourishing Chinese patent medicine and preparation thereof " (applying date 1993.09.01, application number 93100150,1 publication number CN1075639A) Chinese medicine of Jie Shaoing, being made up of 18 flavor Chinese medicines such as Radix Ginseng's piece of antler, is that earlier Radix Ginseng to be waited the Six-element Chinese medicine powder be powder, 12 flavor Chinese medicines such as water second extraction Radix Rehmanniae Preparata, be condensed into thick paste after, adding the Radix Ginseng waits powder, water and asparagine nipalgin antiseptic face to make, used Chinese medicine is many, and preparation procedure is loaded down with trivial details, the cost height.
The objective of the invention is: first provide a kind of good effect, short treating period, only with nine flavor Chinese medicines, be convenient to preserve, carry, the Shuangshi Zaishengjing oral liquor that is mainly used in treatment sexual impotence of taking convenience, second provides the preparation method of the Shuangshi Zaishengjing oral liquor that a kind of preparation method is simple, cost is low.
Shuangshi Zaishengjing oral liquor of the present invention, be with nine flavor Chinese medicines, be mixed with its alcohol reflux liquid, soaking in Chinese liquor liquid, water decoction and distilled water respectively, it is characterized in that containing in this Shuangshi Zaishengjing mouth liquid of every 1000ml: the concentration of Cornu Cervi Pantotrichum, Formica fusca, the sufficient Gecko that decaptitates is the ethanol extract 270-330ml of 60-75%, removes soaking in Chinese liquor liquid 270-330ml, Herba Epimedii, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the water decoction 270-330ml of the Radix Astragali and an amount of distilled water of the 50-65 degree of wing male Bombycis mori.Wherein used Chinese medicine and weight thereof are:
Cornu Cervi Pantotrichum 8-12g, Radix Astragali 24-32g, Herba Epimedii 90-110g, Gecko 16-24g, Semen Allii Tuberosi 24-32g, Formica fusca 1-3g, Herba Cistanches 36-42g, male Bombycis mori 46-52g, Rhizoma Polygoni Cuspidati 24-32g.And in this Shuangshi Zaishengjing oral liquor, containing concentration of alcohol is 20-30%.
The preparation method of Shuangshi Zaishengjing oral liquor is to adopt such technical scheme to realize:
1, the pre-treatment of medicine
(1) preparation of medicine ethanol extract:
Get metering Cornu Cervi Pantotrichum, Formica fusca, sufficient Gecko decaptitates, be under 20 ± 2 ℃ the temperature at pressure for the 0.08mpa temperature, with concentration is the alcohol reflux three times of 60-75%: the 9-11 that adds ethanol for the first time and be three flavor Chinese medicine weight doubly, after the reflux, extract, two hours, take out and requiredly in the medicinal liquid of remainder, add ethanol with 1/3 of extracting solution, make ethanol content in the medicinal liquid be three flavor Chinese medicine weight 7-9 doubly, reflux, extract, is taken out required 1/3 of the extracting solution of using after two hours more again; In the medicinal liquid of remainder, add ethanol again, make ethanol in the medicinal liquid be three flavor Chinese medicine weight 5-7 doubly, reflux, extract, one hour is taken out required with 1/3 of extracting solution for the third time.
Merge three times reflux extracting liquid, and fully mix, be the medicine ethanol extract of required usefulness after the mixing, standby.
(2) preparation of medicine soaking in Chinese liquor liquid:
Remove the male Bombycis mori that measures behind the wing, weight with the 50-65 degree is Bombycis mori 9-11 Chinese liquor doubly, under 1-5 ℃ of temperature, soaked 12-15 days, stirred in per 4 hours once, the squeezing back take out add 3/5 of Chinese liquor amount, under 20 ± 2 ℃ temperature, left standstill 24 hours, be the soaking in Chinese liquor liquid of male Bombycis mori, standby.
(3) preparation of medicine water decoction:
Get the Herba Epimedii of metering, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali, water decocts three times: the 14-16 that adds water for the first time and be Chinese medicine of the five flavours weight doubly, decoct after two hours, take out 1/3 of required water decoction liquor, in the medicinal liquid of remainder, add water again, make water in the medicinal liquid be Chinese medicine of the five flavours weight 11-13 doubly, after decocting two hours again, take out for the second time 1/3 of required water decoction liquor, in the medicinal liquid of remainder, add water for the third time afterwards, make water in the medicinal liquid be Chinese medicine of the five flavours weight 9-11 doubly, it is required with 1/3 of decoction liquor decocting to last water, taking-up merges with the water decoction of preceding twice taking-up, and it is fully mixed, and filters with known method, be the medicine water decoction of required usefulness, standby.
2, the preparation of Shuangshi Zaishengjing oral liquor:
(1) gets above-mentioned medicine ethanol extract, medicine soaking in Chinese liquor liquid, medicine water decoction and mix, and stir and make its mix homogeneously.
(2) in above-mentioned three kinds of admixing medical solutions, add distilled water, make that concentration of alcohol is 20-30% in the medicinal liquid, under 20 ± 2 ℃ of temperature, left standstill 24 hours.
(3) leave standstill the liquid fine straining with the known method handle, filling bottle, capping, decals are packed afterwards, have promptly prepared the Shuangshi Zaishengjing oral liquor of every bottle of 10ml.
Shuangshi Zaishengjing oral liquor provided by the invention is used for the treatment of andrology's diseases such as sexual impotence, premature ejaculation, its effective in cure height, instant effect, short treating period, has no side effect, because only with the general Chinese medicine of nine flavors, and its preparation method is simple, so cost is low, is easy to popularization.This oral liquid not only is easy to preserve, carry, and taking convenience, for a kind of andropathy for the treatment of preferably, especially treats Chinese medicine oral liquid of impotence deficiency and preparation method thereof.By pharmacological evaluation and clinic trial, prove this oral liquid, have the kidney warming, tonifying YANG, enriching kidney essence, erection enhancing, increase sexuality, it is satisfied to make men and women reach sexual life.So this medicine of title of image is a Shuangshi Zaishengjing oral liquor, this Shuangshi Zaishengjing oral liquor preparation procedure is easy, is easy to promote.
Further specify this Shuangshi Zhaishengjin oral liquid and its preparation ,method below in conjunction with embodiment:
Embodiment:
One, the composition of Shuangshi Zaishengjing oral liquor: contain in every 1000ml Shuangshi Zaishengjing oral liquor: it is three extracting solution 300ml of ethanol of 70% that the decaptitate concentration of sufficient Gecko of big Black Hills woods ant is produced on the Changbai Mountain that the Cornu Cervi Pantotrichum after the metering, spring, two seasons of autumn capture, going the concentration of the male Bombycis mori that metering behind the wing captures summer is the soaking in Chinese liquor liquid 300ml of 60 degree, three water decoction 300ml of the Herba Epimedii of metering, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali, and an amount of distilled water, wherein used Chinese medicine and weight thereof are:
Cornu Cervi Pantotrichum 10g, Radix Astragali 30g, Herba Epimedii 10g, Gecko 20g, Semen Allii Tuberosi 30g, Formica fusca 2g, Herba Cistanches 40g, male Bombycis mori 50g, Rhizoma Polygoni Cuspidati 30g.
Transfer this Shuangshi Zaishengjing oral liquor to make containing concentration of alcohol with distilled water simultaneously is 25 ± 2%.
The quality of above-mentioned kinds of traditional Chinese medicines all will meet the quality standard that Chinese Pharmacopoeia (nineteen ninety version) is indicated, for ensuring the quality of products, wherein Herba Epimedii adopts Liaoning, Shanxi, Guangxi to produce; Cornu Cervi Pantotrichum adopts Jilin, Heilungkiang, the Inner Mongol to produce; Gecko adopts Guangdong, Yunnan, Guizhou to produce; Herba Cistanches adopts the Inner Mongol, Ningxia, Xinjiang to produce; The Radix Astragali adopts Jilin, Heilungkiang to produce.Animal tcm, the interior contained active ingredient of body is different different because of season, so male Bombycis mori must be in the capture in summer, and Formica fusca captured in spring, two seasons of autumn, and must be the big Black Hills woods ant that produce on the Changbai Mountain.
Two, the preparation method of Shuangshi Zaishengjing oral liquor
Oral liquid with preparation 1000ml is an example, and technical scheme of the present invention is elaborated:
1, medicine pre-treatment:
(1) preparation of medicine ethanol extract: get Cornu Cervi Pantotrichum 10g, capture exsiccant Changbai Mountain in spring, two seasons of autumn and produce big Black Hills woods ant 2g, the Gecko 20g that decaptitates sufficient, behind the phase mix homogeneously, putting into extraction pot, is that 0.08MPa, temperature are under 20 ± 2 ℃ the condition at pressure, with concentration is 70% alcohol reflux three times: add ethanol for the first time and be 10 times of three flavor Chinese medicine weight, be 320ml, reflux, extract, is after two hours, and taking out ethanol extract for the first time is that 1/3 of aequum is 100ml; Add ethanol in the medicinal liquid of remainder again, making ethanol in the medicinal liquid is 8 times of three flavor Chinese medicine weight, i.e. 256ml, and reflux, extract, is after two hours, and taking out ethanol extract for the second time is that 1/3 of aequum is 100ml; Add ethanol again in the medicinal liquid of remainder, making ethanol in the medicinal liquid is 6 times of three flavor Chinese medicine weight, i.e. 192ml, and reflux, extract, is after one hour, and taking out extracting solution for the third time is that 1/3 of aequum is 100ml.The alcohol reflux liquid that merges three taking-ups is 300ml, and it is fully mixed, and has promptly produced medicine alcohol reflux liquid.
(2) preparation of medicine soaking in Chinese liquor liquid:
Get capture summer remove wing male Bombycis mori 50g, with 10 times of drug weight, be the Chinese liquor of 500ml, 60 degree, under 1-5 ℃ temperature, soaked 14 days, and stirred once every 4 hours, get supernatant, filtering the back is under 20 ± 2 ℃ in temperature, leave standstill 24 hours after, getting soaking in Chinese liquor liquid is that 3/5 of Chinese liquor addition is 300ml.
(3) preparation of medicine water decoction:
Get Herba Epimedii 100g, Herba Cistanches 40g, Semen Allii Tuberosi 30g, Rhizoma Polygoni Cuspidati 30g, after Radix Astragali 30g mixes mutually, the water that adds for the first time 15 times of five kinds of Chinese medicine weight is 3450ml, after decocting two hours with fire, taking out decoction liquor is that 1/3 of aequum is 100ml, and adding water again in the medicinal liquid of remainder, to make water in the medicinal liquid be 12 times of Chinese medicine of the five flavours weight, i.e. 2760ml, after decocting two hours again, for the second time taking out water decoction is that 1/3 of aequum is 100ml, adds water again in the medicinal liquid of remainder, makes that water is 10 times that Chinese medicine of the five flavours is reset in the medicinal liquid, be 2300ml, decoct that last water is that 1/3 of aequum is 100ml to the medicinal liquid, take out with the medicinal liquid of preceding secondary taking-up and fully mix, promptly prepared medicine water decoction 300ml.
2, the preparation of oral liquid
(1) with Cornu Cervi Pantotrichum, Formica fusca, the ethanol extract 300ml of Gecko and the soaking in Chinese liquor liquid 300ml of male Bombycis mori of above-mentioned preparation, the water decoction 300ml of Herba Epimedii, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, Huang Shi fully mixes mutually;
(2) to above-mentioned ethanol extract, add distilled water in the mixing material of soaking in Chinese liquor liquid and water decoction, transferring the alcohol concentration of mixed liquor is 25 ± 2%, leaves standstill under 20 ± 2 ℃ temperature 24 hours afterwards;
(3) with known method the above-mentioned liquid fine straining that leaves standstill, filling bottle is a 10ml dress afterwards, capping then, decals, packing are the product of Shuangshi Zaishengjing oral liquor.
By the Shuangshi Zaishengjing oral liquor of this method preparation, PH is 4.5-5.5, and relative density is 1.04-1.10, and other quality meet the standard of 15 pages of Chinese Pharmacopoeia 1990 (an one) version appendix.
The pharmacological experiment result
1, has the kidney invigorating, QI invigorating, yang invigorating functions, can improve the tolerance of the external pessimal stimulation of body, strengthen the animal body physiological function, the yang deficiency mice is had protective effect.
2, increase castration mouse accessory sex organ weight, improve the state of suffering from a deficiency of the kidney.
3, the male Mus serum testosterone of rising immaturity content increases testicular weight.
4, improve the male mouse fertility, rate of rise is about 10-25%.
The toxicity study experiment
1, acute toxicity testing: its minimum lethal dose (rat) is more than the 9.4 gram/kilograms, is equivalent to more than 102 times of people's clinical every day of consumption.
2, the maximum amount of rat is by 4.0 gram/kilograms, successive administration 60 days, rat sign, appearance, diet etc. there is no unusually as a result, and pathological examination is all no abnormal pathological changes of important organ such as the heart, liver, spleen, lung, kidney as a result, prove that this medicine has no side effect, the mankind take safety.
Clinical observation:
Select case by " new Chinese medicine clinical research guideline " that Ministry of Health of the People's Republic of China develops and publishes, all have a deficiency of kidney-YANG syndrome, as symptoms such as sexual impotence, premature ejaculation, spiritlessness and weakness, sexual anesthesias, all can be the object of observation, classify the patient of observation as, obey one of the Shuangshi Zaishengjing oral liquor of 10ml dress at every turn, obey every day 3 times, two weeks were a course of treatment, took during this medicine, prohibited the clothes other medicines.By produce effects, effective, invalid three kinds of situations 120 inpatients of a 94.2-94.4.3 period three day hospital are carried out t check, rank test respectively.
Clinic trial result:
Shuangshi Zaishengjing oral liquor has life lengthening, anti-aging effects, is 95% to the male sexual disorder effective percentage, does not see toxic side effect in clinical practice, statistical result such as following table:
Shuangshi Zaishengjing oral liquor is to the clinical statistics of male sexual disorder treatment
This table statistical data explanation Shuangshi Zaishengjing oral liquor has obvious therapeutic action to male sexual disorder, P＜0.05.
The Shuangshi Zaishengjing oral liquor of the trial-production city medicine inspecting institute check according to the present invention, its quality reaches standard fully, and submits a report asking for Department of Public Health of Shanxi Province, and is granted, grants and produces.
Claims (10)
1, a kind of Chinese medicine preparation Shuangshi Zaishengjing oral liquor of main treatment sexual impotence is formulated by alcohol reflux liquid, soaking in Chinese liquor liquid and the water decoction of nine flavor Chinese medicines respectively, it is characterized in that containing in every 1000ml oral liquid:
The concentration of Cornu Cervi Pantotrichum, Formica fusca, the sufficient Gecko that decaptitates is that the ethanol of 60-75% proposes liquid 270-330ml, the concentration of removing the wing male Bombycis mori is the soaking in Chinese liquor liquid 270-330ml of 50-65 degree, the water decoction 270-330ml of Herba Epimedii, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali and an amount of distilled water, and used Chinese medicine and weight thereof are:
Cornu Cervi Pantotrichum 8-12g, Radix Astragali 24-32g, Herba Epimedii 90-110g, Gecko 16-24g, Semen Allii Tuberosi 24-32g, Formica fusca 1-3g, Herba Cistanches 36-42g, male Bombycis mori 46-52g, Rhizoma Polygoni Cuspidati 24-32g, simultaneously, wherein concentration of ethanol is 20-30%.
2, Shuangshi Zaishengjing oral liquor according to claim 1 is characterized in that the optimum amount of the used Chinese medicine of respectively distinguishing the flavor of is: Cornu Cervi Pantotrichum 10g, Radix Astragali 30g, Herba Epimedii 100g, Gecko 20g, Semen Allii Tuberosi 30g, Formica fusca 2g, Herba Cistanches 40g, male Bombycis mori 50g, Rhizoma Polygoni Cuspidati 30g.
3, Shuangshi Zaishengjing oral liquor according to claim 2, when it is characterized in that three alcohol reflux Cornu Cervi Pantotrichums, Formica fusca, Gecko, get the ethanol extract optimised quantity is 1/3 of aequum at every turn; During with the soaking in Chinese liquor male Bombycis mori, the optimised quantity of getting soaking in Chinese liquor liquid is 3/5 of a Chinese liquor addition; When decocting Herba Epimedii, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali three times, the optimised quantity of the decoction liquor of at every turn fetching water is 1/3 of an aequum.
4, Shuangshi Zaishengjing oral liquor according to claim 1 and 2 is characterized in that male Bombycis mori must capture in summer.
5, Shuangshi Zaishengjing oral liquor according to claim 1 and 2 is characterized in that the big Black Hills woods ant that Formica fusca must produce on the Changbai Mountain that spring, two seasons of autumn capture.
6, Shuangshi Zaishengjing oral liquor according to claim 1 and 2, it is characterized in that containing in this oral liquid alcoholic acid optium concentration is 25 ± 2%.
7, a kind of preparation method of Shuangshi Zaishengjing oral liquor as claimed in claim 1 is characterized in that this method carries out according to following order:
The medicine pre-treatment
(1) preparation of medicine ethanol extract: getting Cornu Cervi Pantotrichum, the Formica fusca of metering, the sufficient Gecko that decaptitates, is 0.08MPa at pressure, and temperature is under 20 ± 2 ℃ the condition, is the alcohol reflux three times of 60-75% with concentration; The 9-11 that adds for the first time ethanol and be three flavor medicine weight doubly, reflux, extract, was taken out 1/3 of required usefulness ethanol extract after two hours; For the second time in the medicinal liquid of remainder, add ethanol again, make ethanol in the medicinal liquid be three flavor medicine weight 7-9 doubly, reflux, extract, is taken out required with 1/3 of ethanol extract after two hours again; In the medicinal liquid of remainder, add ethanol for the third time again, make ethanol in the medicinal liquid be three flavor medicine weight 5-7 doubly, after the reflux, extract, one hour, take out required for the third time with 1/3 of ethanol extract, the alcohol reflux liquid that merges three taking-ups, it is fully mixed, be the medicine alcohol reflux liquid of required usefulness;
(2) preparation of medicine soaking in Chinese liquor liquid: remove the male Bombycis mori that measures behind the wing,, under 1-5 ℃ of temperature, soaked 12-15 days with 50-65 degree, male Bombycis mori weight 9-11 Chinese liquor doubly, after the squeezing, 3/5 of Chinese liquor amount that taking-up adds;
(3) the medicine decocting preparation of boiling: get Herba Epimedii, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali of metering, water decocts three times: the 14-16 that adds water for the first time and be five kinds of Chinese medicine weight doubly decocts after two hours 1/3 of taking-up required water decoction liquor; Again in the medicinal liquid of remainder, add for the second time water make water in the medicinal liquid be five kinds of Chinese medicine weight 11-13 doubly, decocts after two hours, take out 1/3 of required usefulness decoction liquor for the second time; In the medicinal liquid of remainder, add water again, make water in the medicinal liquid be five kinds of Chinese medicine weight 9-11 doubly, decoct to the medicinal liquid water and be and requiredly the medicine water decoction of three taking-ups is fully mixed with 1/3 of decoction liquor, be the medicine water decoction of required usefulness;
The preparation of Shuangshi Zaishengjing oral liquor:
(1) three water decoctions of Cornu Cervi Pantotrichum, Formica fusca, three alcohol reflux liquid of Gecko and male Bombycis mori soaking in Chinese liquor liquid and excessive year leaves of pulse plants, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, the Radix Astragali is fully mixed;
(2) in above-mentioned mixed liquor, add distilled water, make that concentration of alcohol is 20-30% in the mixed liquor, under 20 ± 2 ℃ of temperature, left standstill 24 hours;
(3) be made as bottled oral liquid leaving standstill liquid.
8, the preparation method of Shuangshi Zaishengjing oral liquor according to claim 7, when it is characterized in that three alcohol reflux Cornu Cervi Pantotrichums, Formica fusca, Gecko, used ethanol optimised quantity is, be 10 times of three flavor Chinese medicine weight the first time, getting the extracting solution optimised quantity is 1/3 of aequum, add for the second time ethanol ethanol to the medicinal liquid and be 8 times of three flavor medicine weight, getting the extracting solution optimised quantity is 1/3 of aequum, add ethanol ethanol to the medicinal liquid for the third time and be 6 times of three flavor medicine weight, getting the extracting solution optimised quantity is 1/3 of aequum, and used ethanol optium concentration is 70%.
9, according to the preparation method of claim 7 or 8 described Shuangshi Zaishengjing oral liquors, it is characterized in that soaking the best number of degrees of the used Chinese liquor of male Bombycis mori is 60 degree, optimum amount is 10 times of male Bombycis mori weight, and soaking Best Times is 14 days, and the optimised quantity of getting soaking in Chinese liquor liquid is 3/5 of a Chinese liquor addition.
10, preparation method according to claim or 7 or 8 or 9 described Shuangshi Zaishengjing oral liquors, it is characterized in that three decoctings boil the excessive year leaves of pulse plants, Herba Cistanches, Semen Allii Tuberosi, Rhizoma Polygoni Cuspidati, during the Radix Astragali, add for the first time the water optimised quantity and be 15 times of five kinds of Chinese medicine weight, it is required with 1/3 of decoction liquor getting the decoction liquor optimised quantity, add for the second time water optimised quantity water to the medicinal liquid and be 12 times of five tastes dose, getting the decoction liquor optimised quantity is 1/3 of required decoction liquor, add water optimised quantity water to the medicinal liquid for the third time and be 10 times of five tastes dose, decoct that last water optimised quantity is required with 1/3 of decoction liquor to the medicinal liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94116420 CN1062745C (en) | 1994-09-30 | 1994-09-30 | Shuangshi Zaishengjing oral liquor and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 94116420 CN1062745C (en) | 1994-09-30 | 1994-09-30 | Shuangshi Zaishengjing oral liquor and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
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| CN1110171A CN1110171A (en) | 1995-10-18 |
| CN1062745C true CN1062745C (en) | 2001-03-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 94116420 Expired - Fee Related CN1062745C (en) | 1994-09-30 | 1994-09-30 | Shuangshi Zaishengjing oral liquor and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1071122C (en) * | 1997-08-01 | 2001-09-19 | 李余地 | Chinese medicine preparation for treating prospermia and preventing impotence |
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Assignee: Jilin Shuang Shi Pharmaceutical Co., Ltd. Assignor: An Jicai|Gu Zhiyuan Contract fulfillment period: 2007.1.6 to 2014.9.30 contract change Contract record no.: 2009220000081 Denomination of invention: Shuangshi Zaishengjing oral liquor and preparation method thereof Granted publication date: 20010203 License type: Exclusive license Record date: 20091027 |
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