CN106083200A - Dragon's fountain Song dynasty brother's kiln celadon glaze and the method making dragon's fountain Song dynasty brother's kiln celadon product with this glaze - Google Patents
Dragon's fountain Song dynasty brother's kiln celadon glaze and the method making dragon's fountain Song dynasty brother's kiln celadon product with this glaze Download PDFInfo
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- CN106083200A CN106083200A CN201610396776.9A CN201610396776A CN106083200A CN 106083200 A CN106083200 A CN 106083200A CN 201610396776 A CN201610396776 A CN 201610396776A CN 106083200 A CN106083200 A CN 106083200A
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- glaze
- kiln
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- dragon
- glazing
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Furnace Details (AREA)
- Muffle Furnaces And Rotary Kilns (AREA)
Abstract
The invention belongs to porcelain field, particularly to a kind of dragon's fountain Song dynasty brother's kiln celadon glaze and with this glaze make dragon's fountain Song dynasty brother's kiln celadon product method.A kind of dragon's fountain Song dynasty brother's kiln celadon glaze, including tire material and glaze, wherein: described tire material is mainly made up of the raw material of following weight portion: 80 90 parts of Zijin soil, western source china clay 10 20 parts, yellow altar china clay 10 20 parts；Described glaze is mainly made up of the raw material of following weight portion: 32 35 parts of ridge root glaze soil, quick lime 25 30 parts, 35 parts of quartz, 35 parts of troilite, 11 13 parts of Dayao Zijin soil.The product that the present invention prepares can realize the glaze of cream colour glaze.
Description
Technical field
The invention belongs to porcelain field, particularly to a kind of dragon's fountain Song dynasty brother's kiln celadon glaze and make the dragon's fountain Song dynasty with this glaze
The method of brother's kiln celadon product.
Background technology
The tire color of dragon's fountain brother's kiln porcelain has the multiple color and lusters such as dark-grey, light gray, grey black and the colour of loess, glaze colours more have pale blue, bluish white,
Putty, the difference of bluish yellow, and based on putty.It is mainly characterized by glaze and is covered with the stricture of vagina sheet of be full of cracks, normally referred to as " hacking ".
This sheet stricture of vagina formed by fine cracks, size is different, the depth of crackle color also differs.
Song dynasty brother's kiln crack glaze has stronger vitality as the decoration of a kind of art pottery.Due to of the remote past, brother
Kiln porcelain formula and manufacturing process are the most lost, for meeting the consumer demand day by day increased, have tried in recent years recover
Song dynasty brother's kiln porcelain formula and manufacturing process, but effect is not fully up to expectations.
Summary of the invention
The present invention provides a kind of dragon's fountain Song dynasty brother's kiln celadon glaze, and prepared dragon's fountain Song dynasty brother's kiln celadon product can realize cream colour
The glaze of glaze.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze, including tire material and glaze, wherein: described tire material is mainly by following weight portion
Raw material is made: Zijin soil 80-90 part, western source china clay 10-20 part, yellow altar china clay 10-20 part；Described glaze is mainly by following weight
The raw material of part is made: ridge root glaze soil 32-35 part, quick lime 25-30 part, quartz 3-5 part, troilite 3-5 part and Dayao Zijin soil
11-13 part.
This project, under high temperature reducing atmospheres, utilizes ferrum oxide to present cyan under high temperature reducing atmospheres for feature, with many
Planting china clay mineral is raw material, and prepared dragon's fountain Song dynasty brother's kiln celadon product outward appearance is with the Southern Song Dynasty's black tire brother's kiln celadon pole seemingly.
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze makes the method for dragon's fountain Song dynasty brother's kiln celadon product, comprises the following steps:
A, fire biscuit: add water mix homogeneously by all raw materials of described tire material, makes base mud, by described base mud molding
After drying, kiln-firing, make biscuit；
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, adds water for ball milling, sieve
After i.e. obtain ceramic glaze；
C, glazing: described ceramic glaze is imposed on described biscuit, dried formation glaze layer in uniform thickness, obtain base
Body, carries out second time glazing after base substrate cooling；
D, fire: after the glaze layer on base substrate parches naturally, kiln-firing, fire rear kiln discharge and get product；Wherein fire
Process sequentially passes through following several stage: the stage that is rapidly heated, slow temperature rise period and natural cooling.
As preferably, firing middle start-stop temperature and be room temperature, the programming rate in the stage that is rapidly heated is 2-3 DEG C/min, slow
The programming rate of slow temperature rise period is 0.3-0.5 DEG C/min.
As preferably, before glazing, first base substrate is put into biscuiting in kiln and, to 800 DEG C, carries out after its cooling and dedusting for the first time
Leaching glaze, the leaching glaze time is between 10s-15s；Afterwards, put into roasting in kilns to 500 DEG C, after its cooling and dedusting, carry out second time
Glazing.
As preferably, glazing for the second time uses spray glazing, is positioned on rotating disk by biscuit and slowly rotates, and uses compression pump pair
It carries out glazing, stops glazing when glazed thickness is 1.3:1 with carcass thickness ratio.
The invention has the beneficial effects as follows: the present invention uses rational raw ore raw material to test out tire, glaze formula, and at high temperature also
Burning out the thick glaze celadon glaze that glaze layer is abundant, show the cream-coloured glaze whitened in Huang in Primordial Qi atmosphere, such glaze colours can be by ferrum tire
Black quality be covered with comprehensively, it is beautiful that glaze color and luster presents exquisite in texture, gentle class under the setting off of black tire.
Accompanying drawing explanation
Fig. 1 is the process chart of the present invention；
Fig. 2 be the present invention burn till heating curve.
Detailed description of the invention
Below by specific embodiment, technical scheme is described in further detail.Should be appreciated that this
Bright enforcement is not limited to the following examples, and any pro forma accommodation and/or the change of being made the present invention all will fall
Enter scope.
In the present invention, if not refering in particular to, all of part, percentage ratio are unit of weight, the equipment used and raw material etc.
All it is commercially available or commonly used in the art.Method in following embodiment, if no special instructions, is the normal of this area
Rule method.
Embodiment 1:
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze, including tire material and glaze, wherein: described tire material is mainly by following weight portion
Raw material is made: 80 parts of Zijin soil, western source china clay 18 parts, yellow altar china clay 15 parts；Described glaze is mainly by the raw material of following weight portion
Make: 32 parts of ridge root glaze soil, quick lime 25 parts, 5 parts of quartz, 5 parts of troilite, 13 parts of Dayao Zijin soil.
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze make dragon's fountain Song dynasty brother's kiln celadon product method, flow process as it is shown in figure 1,
Comprise the following steps:
A, fire biscuit: add water mix homogeneously by all raw materials of described tire material, makes base mud, by described base mud molding
After drying, kiln-firing, make biscuit；
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, adds water for ball milling, sieve
After i.e. obtain ceramic glaze；
C, glazing: described ceramic glaze is imposed on described biscuit, dried formation glaze layer in uniform thickness, obtain base
Body, carries out second time glazing after base substrate cooling；
D, fire: after the glaze layer on base substrate parches naturally, kiln-firing, fire rear kiln discharge and get product；Wherein fire
Process sequentially passes through following several stage: the stage that is rapidly heated, slow temperature rise period and natural cooling.
Wherein, glazing process: the Southern Song Dynasty's black tire brother's kiln hacks celadon, and it is mainly characterized in that thin tire thickness glaze, and glaze is thicker than tire, therefore,
Glazing process is particularly critical.The present embodiment mainly uses repeatedly glazing method, and this glazing method is divided into leaching glaze and glaze spraying two parts.Glazing
Before, first base substrate to be put in kiln biscuiting to about 800 DEG C, after its cooling and dedusting, carry out soaking for the first time glaze, the leaching glaze time is
Between 10s 15s.Afterwards, put into roasting in kilns to 500 DEG C, after its cooling and dedusting, carry out second time glazing.Glazing for the second time
Use spray glazing, biscuit is positioned on rotating disk and slowly rotates, use compression pump that it is carried out glazing, treat glazed thickness and carcass
Glazing is stopped when thickness ratio is about 1.3:1.
Firing process: in order to ensure products appearance effect and improve yield rate, the present embodiment uses shuttle kiln slowly to burn till,
Enter the strong reductive firing stages in 1080 DEG C, and transfer in 1200 DEG C and weak be reduced to 1320 DEG C of only fire, total time-consuming nearly 18h.It burns
Become curve as shown in Figure 2.Firing middle start-stop temperature and be room temperature, the programming rate in the stage that is rapidly heated is 2-3 DEG C/min, slowly
The programming rate of temperature rise period is 0.3-0.5 DEG C/min.
Embodiment 2:
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze, including tire material and glaze, wherein: described tire material is mainly by following weight portion
Raw material is made: 90 parts of Zijin soil, western source china clay 15 parts, yellow altar china clay 20 parts；Described glaze is mainly by the raw material of following weight portion
Make: 35 parts of ridge root glaze soil, quick lime 25 parts, 3 parts of quartz, 3 parts of troilite, 11 parts of Dayao Zijin soil.Brother's kiln hacks celadon system
Make technique with embodiment 1.
Embodiment 3:
A kind of dragon's fountain Song dynasty brother's kiln celadon glaze, including tire material and glaze, wherein: described tire material is mainly by following weight portion
Raw material is made: 85 parts of Zijin soil, western source china clay 16 parts, yellow altar china clay 18 parts；Described glaze is mainly by the raw material of following weight portion
Make: ridge root glaze soil 32-35 part, quick lime 25-30 part, 3 parts of quartz, 5 parts of troilite, 12 parts of Dayao Zijin soil.Brother's kiln hacks
Celadon manufacturing process is with embodiment 1.
The present invention has made black tire brother's kiln by many experiments and has hacked celadon tire material, and such tire material has preferable mouldability
Can, present black when burning till for 1300 DEG C 1320 DEG C.Celadon glaze outward appearance effect is hacked for burning out tire brother's kiln black with the Southern Song Dynasty
Celadon as fruit, by many experiments, obtains rational formula, finally burns out glaze exquisite in texture, gentle class is beautiful, victory is beautiful refined
Causing, glaze colours is simple and elegant, the cream-coloured glaze of whiting in Huang.
Embodiment described above is the one preferably scheme of the present invention, not makees the present invention any pro forma
Limit, on the premise of without departing from the technical scheme described in claim, also have other variant and remodeling.
Claims (5)
1. dragon's fountain Song dynasty brother's kiln celadon glaze, it is characterised in that: include tire material and glaze, wherein: described tire material mainly by with
The raw material of lower weight portion is made: Zijin soil 80-90 part, western source china clay 10-20 part, yellow altar china clay 10-20 part；Described glaze is main
Be made up of the raw material of following weight portion: ridge root glaze soil 32-35 part, quick lime 25-30 part, quartz 3-5 part, troilite 3-5 part and
Dayao Zijin soil 11-13 part.
2. the method that dragon's fountain Song dynasty brother's kiln celadon glaze makes dragon's fountain Song dynasty brother's kiln celadon product according to claim 1,
It is characterized in that, comprise the following steps:
A, fire biscuit: add water mix homogeneously by all raw materials of described tire material, makes base mud, by described base mud shaping and drying
After, kiln-firing, make biscuit；
B, preparation ceramic glaze: the raw material in described glaze is mixed according to proportioning, after pulverizing, adds water for ball milling, after sieving i.e.
Obtain ceramic glaze；
C, glazing: described ceramic glaze is imposed on described biscuit, dried formation glaze layer in uniform thickness, obtain base substrate, base
Second time glazing is carried out after body cooling；
D, fire: after the glaze layer on base substrate parches naturally, kiln-firing, fire rear kiln discharge and get product；Wherein sintering procedure
Sequentially pass through following several stage: the stage that is rapidly heated, slow temperature rise period and natural cooling.
Method the most according to claim 2, it is characterised in that: fire middle start-stop temperature and be room temperature, be rapidly heated the stage
Programming rate be 2-3 DEG C/min, the programming rate of slow temperature rise period is 0.3-0.5 DEG C/min.
Method the most according to claim 2, it is characterised in that: before glazing, first base substrate is put in kiln biscuiting to 800 DEG C,
Carrying out soaking for the first time glaze after its cooling and dedusting, the leaching glaze time is between 10s-15s；Afterwards, put into roasting in kilns to 500 DEG C,
Second time glazing is carried out after its cooling and dedusting.
Manufacturing process the most according to claim 2, it is characterised in that: glazing for the second time uses spray glazing, is placed by biscuit
Slowly rotate on rotating disk, use compression pump that it is carried out glazing, stop when glazed thickness is 1.3:1 with carcass thickness ratio
Glazing.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610396776.9A CN106083200B (en) | 2016-06-06 | 2016-06-06 | Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze |
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| CN201610396776.9A CN106083200B (en) | 2016-06-06 | 2016-06-06 | Dragon's fountain Song Dynasty brother's kiln celadon glaze and the method for making dragon's fountain Song Dynasty brother's kiln celadon product with the glaze |
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| CN106083200A true CN106083200A (en) | 2016-11-09 |
| CN106083200B CN106083200B (en) | 2019-01-04 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108373265A (en) * | 2018-02-06 | 2018-08-07 | 平顶山学院 | A kind of shrinkproof glaze handicraft of celadon and method |
| CN108751708A (en) * | 2018-06-04 | 2018-11-06 | 浙江上木木陶瓷文化有限公司 | The pure matting glaze of high temperature more kiln, using the matting glaze kiln secret colour ware and its method for cooking |
| CN110183248A (en) * | 2019-05-22 | 2019-08-30 | 李茂林 | Material, dragon's fountain porcelain and preparation method thereof is presented in Vermilion for dragon's fountain porcelain |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
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2016
- 2016-06-06 CN CN201610396776.9A patent/CN106083200B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101734948A (en) * | 2008-11-04 | 2010-06-16 | 李邦强 | Longquan official ware celadon glaze of the Ming Dynasty and method for manufacturing Longquan official ware celadon product of the Ming Dynasty by using glaze |
Non-Patent Citations (2)
| Title |
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| 吴艳芳等: ""黑胎哥窑青瓷的仿制"", 《丽水学院学报》 * |
| 毛伟杰: ""南宋龙泉黑胎哥窑开片青瓷的复烧工艺研究"", 《大众文艺》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108373265A (en) * | 2018-02-06 | 2018-08-07 | 平顶山学院 | A kind of shrinkproof glaze handicraft of celadon and method |
| CN108751708A (en) * | 2018-06-04 | 2018-11-06 | 浙江上木木陶瓷文化有限公司 | The pure matting glaze of high temperature more kiln, using the matting glaze kiln secret colour ware and its method for cooking |
| CN110183248A (en) * | 2019-05-22 | 2019-08-30 | 李茂林 | Material, dragon's fountain porcelain and preparation method thereof is presented in Vermilion for dragon's fountain porcelain |
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