CN106075944A - A kind of distilling apparatus measuring volatile material - Google Patents
A kind of distilling apparatus measuring volatile material Download PDFInfo
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- CN106075944A CN106075944A CN201610374179.6A CN201610374179A CN106075944A CN 106075944 A CN106075944 A CN 106075944A CN 201610374179 A CN201610374179 A CN 201610374179A CN 106075944 A CN106075944 A CN 106075944A
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- cylinder body
- interface
- piston
- limited block
- collecting cylinder
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of distilling apparatus measuring volatile material, it is desirable to provide a kind of condensation liquefaction is effective, and the distilling apparatus measuring volatile material of condensation liquefaction efficiency can be improved.It includes shuttle, heater, volatile material collection device, condensing unit and self adaptation switching device, volatile material collection device includes the vertical collecting cylinder body of upper and lower closed at both ends, it is successively set on the first limited block on vertical collecting cylinder body medial surface from bottom to top, second limited block and the 3rd limited block, it is arranged on the lower piston between the first limited block and the second limited block, it is arranged on the upper piston between the second limited block and the 3rd limited block, it is arranged on interface on the first lower interface and first on vertical collecting cylinder body, self adaptation switching device includes vertically switching cylinder body, it is arranged on and vertically switches the switching piston in cylinder body, it is arranged on and vertically switches the second lower interface on cylinder body lateral surface, interface on intake interface and second.
Description
Technical field
The present invention relates to a kind of distilling apparatus, be specifically related to a kind of distilling apparatus measuring volatile material.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it utilizes each component boiling point in mixing liquid or liquid-solid system different,
Make low boiling component evaporate, then condense to separate the unit process of whole component, be evaporation and two kinds of unit operations of condensation
Associating.The distilling apparatus of current volatile material is to utilize each component boiling point different equally, makes lower boiling volatility thing
Matter evaporation separates, and then uses cooling water that the isolated volatile material of evaporation is carried out condensation and obtains volatile material.At present
This single employing cooling water of volatile material distilling apparatus is to evaporating the mode that isolated volatile material condenses
Not only condensation liquefaction efficiency is low, and condensation liquefaction poor effect, the volatile material relatively low especially for condensation temperature comes
Saying, the effect of single employing cooling water condensation liquefaction is worse.
Summary of the invention
The invention aims to overcome the deficiencies in the prior art, it is provided that a kind of condensation liquefaction is effective, and
The distilling apparatus measuring volatile material of condensation liquefaction efficiency can be improved.
The technical scheme is that
A kind of distilling apparatus measuring volatile material includes having the shuttle of sealed internal chamber, for heating shuttle
Heater, volatile material collection device, for cooling down the condensing unit of volatile material collection device and self adaptation switching
Device, the top of described shuttle is provided with exhaust port, and described volatile material collection device includes upper and lower closed at both ends
Vertical collecting cylinder body, the first limited block being successively set on vertical collecting cylinder body medial surface from bottom to top, the second limited block and
3rd limited block, the lower piston being arranged between the first limited block and the second limited block, it is arranged on the second limited block and the 3rd limit
Interface on upper piston between the block of position, the first lower interface and first of being arranged on vertical collecting cylinder body, the first lower interface is positioned at
Between vertical collecting cylinder body bottom surface and the first limited block, on first, interface is between the first limited block and the second limited block, institute
Stating and be provided with bar through hole in the middle part of the upper surface of vertical collecting cylinder body, the upper end of upper piston is provided with first piston bar, and first piston
Bar passes bar through hole, and described self adaptation switching device includes the switching vertically switching cylinder body, being arranged in vertical switching cylinder body
Piston, the second piston rod being arranged on switching piston, be successively set on vertical switching cylinder body lateral surface from bottom to top the
Interface on two lower interfaces, intake interface and second, described switching piston is on the second lower interface and second between interface, described
The upper end of the second piston rod up extends through the end face of vertically switching cylinder body and is positioned at the top vertically switching cylinder body, and second lives
It is connected by connecting rod between stopper rod with first piston bar, by admission line phase between described exhaust port and intake interface
Connect, be connected by lower pipeline between the first lower interface and the second lower interface, logical between interface on interface and second on first
Cross pipeline to be connected.
As preferably, when upper piston is resisted against on the second limited block, on described intake interface and second, interface is positioned at and cuts
Change the same side of piston；When upper piston is resisted against on the 3rd limited block, described intake interface and the second lower interface are positioned at switching
The same side of piston.
As preferably, between the bottom surface of lower piston and vertical collecting cylinder body, it is provided with extension spring.
As preferably, between the end face of upper piston and vertical collecting cylinder body, it is provided with back-moving spring.
As preferably, the bottom surface of vertical collecting cylinder body is provided with exhaustor, and exhaustor is provided with the first controlled valve.
As preferably, lower piston is provided with the lower material through hole running through lower piston upper and lower surface, in described vertical collecting cylinder body
Being provided with vertical blanking pipe, the lower end of vertical collecting cylinder body is provided with guide through hole, the upper end of vertical blanking pipe and lower material through hole
Lower port be tightly connected, the lower end of vertical blanking pipe is through guide through hole and is positioned at the lower section of vertical collecting cylinder body, vertically
Sealing ring it is provided with, on vertical blanking pipe and be positioned at the lower section of vertical collecting cylinder body between blanking pipe and guide through hole medial surface
It is provided with second switch valve.
As preferably, condensing unit includes the cooling bucket being set on vertical collecting cylinder body, and the bottom surface of cooling bucket is positioned at
Between first limited block and the second limited block.
The invention has the beneficial effects as follows:
One, condensation liquefaction is effective, and can improve condensation liquefaction efficiency.
Its two, volatile material can be avoided to spill in outside air in evaporation separation process, impact building ring around
Border.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation of the present invention.
In figure: shuttle 1, exhaust port 11, heater 2, admission line the 3, the 3rd controlled valve 31, volatility thing
Matter collection device 4, second switch valve 41, vertical blanking pipe 42, extension spring the 43, first limited block 44, lower material through hole 45, lower work
Interface the 47, second limited block 48, upper piston the 49, the 3rd limited block 410, back-moving spring 411, first piston bar on plug 46, first
412, vertical collecting cylinder body the 413, first lower interface 414, exhaustor the 415, first controlled valve 416, self adaptation switching device 5,
Vertically interface 56 on switching cylinder body 51, switching piston 52, intake interface the 53, second lower interface the 54, second piston rod 55, second,
Connecting rod 6, condensing unit 7, connecting tube 8, check valve 81.
Detailed description of the invention
With detailed description of the invention, the present invention is described in further detail below in conjunction with the accompanying drawings:
As it is shown in figure 1, a kind of distilling apparatus measuring volatile material includes having the shuttle 1 of sealed internal chamber, for adding
The heater 2 of hot shuttle, volatile material collection device 4, for cool down volatile material collection device condensation dress
Put 7 and self adaptation switching device 5.The top of shuttle is provided with exhaust port 11.Heater is electric heater or water-bath adds
Hot device, the heater of the present embodiment is water-bath heater, and water-bath heater includes adding heat container and being arranged on and adds in heat container
Add heat pipe.Shuttle is positioned at and adds heat container.
Volatile material collection device includes the vertical collecting cylinder body 413 of upper and lower closed at both ends, sets gradually from bottom to top
First limited block the 44, second limited block 48 and the 3rd limited block 410 on vertical collecting cylinder body medial surface, it is arranged on the first limit
Position block and the second limited block between lower piston 46, the upper piston 49 being arranged between the second limited block and the 3rd limited block, set
Put interface 47 on the first lower interface 414 and first on vertical collecting cylinder body.First lower interface is positioned at the bottom of vertical collecting cylinder body
Between face and the first limited block, and when lower piston is resisted against on the first limited block, on first, interface is positioned at the upper of lower piston
Side.On first, interface is between the first limited block and the second limited block.It is provided with bar in the middle part of the upper surface of vertical collecting cylinder body
Through hole.The upper end of upper piston is provided with first piston bar 412, and first piston bar is through bar through hole.Lower piston and vertical collecting
Being provided with extension spring 43 between the bottom surface of cylinder body, one end of extension spring is connected with lower piston, the other end and the bottom surface of vertical collecting cylinder body
It is connected.Back-moving spring 411 it is provided with between the end face of upper piston and vertical collecting cylinder body.
The bottom surface of vertical collecting cylinder body is provided with exhaustor 415, and exhaustor is provided with the first controlled valve 416.Lower work
It is provided with the lower material through hole 45 running through lower piston upper and lower surface beyond the Great Wall.Lower material through hole is coaxial with lower piston.Set in vertical collecting cylinder body
There is vertical blanking pipe 42.Vertically blanking pipe is coaxial with vertical collecting cylinder body.It is logical that the lower end of vertical collecting cylinder body is provided with guiding
Hole.Vertically the upper end of blanking pipe is tightly connected with the lower port of lower material through hole, and the lower end of vertical blanking pipe is logical through guiding
Hole is also positioned at the lower section of vertical collecting cylinder body.Vertically it is provided with sealing ring between blanking pipe and guide through hole medial surface.Under Shu Zhi
On pipe material and be positioned at the lower section of vertical collecting cylinder body and be provided with second switch valve 41.
Condensing unit includes the cooling bucket being set on vertical collecting cylinder body, and the bottom surface of cooling bucket is positioned at the first limited block
And between the second limited block.On first, seam is provided with connecting tube 8, this connecting tube through cooling bucket sidewall, and connecting tube with
It is tightly connected between the sidewall of cooling bucket.In connecting tube and be positioned at cooling bucket outside be provided with check valve 81.
Self adaptation switching device includes vertically switching cylinder body 51, the switching piston 52 being arranged in vertical switching cylinder body, setting
Put the second piston rod 55 on switching piston, be successively set on connecing for second time on vertical switching cylinder body lateral surface from bottom to top
Interface 56 on mouth 54, intake interface 53 and second.The diameter of upper piston is more than the twice of the diameter of switching piston.Intake interface
Bore is more than the spacing between switching piston both ends of the surface.Switching piston is on the second lower interface and second between interface.Second
The upper end of piston rod up extends through the end face of vertically switching cylinder body and is positioned at the top vertically switching cylinder body.Second piston rod
It is connected by connecting rod 6 with between first piston bar.Connecting rod is positioned at the top of vertical collecting cylinder body.Exhaust port and air inlet
It is connected by admission line 3 between interface.Admission line is provided with the 3rd controlled valve 31.First lower interface and connecing for second time
It is connected by lower pipeline between Kou.It is connected by upper pipeline between interface on interface and second on first, specifically, even
The port of adapter is connected by upper pipeline with between interface on second.
When upper piston is resisted against on the second limited block, on intake interface and second, interface is positioned at the same of switching piston
Side.When upper piston is resisted against on the 3rd limited block, intake interface and the second lower interface are positioned at the same side of switching piston.
The specific works process of the distilling apparatus measuring volatile material of the present embodiment is as follows:
First, as it is shown in figure 1, mixed fluid sample is put into shuttle, in the cooling bucket of condensing unit, put into cooling
Water.
Second, open the 3rd controlled valve, by heater, shuttle is heated, make mixing in shuttle
Volatile material evaporation in liquid separates, and volatile material is entered in vertical switching cylinder body by admission line；Then, pass through
In on second, on interface, upper pipeline and first, interface enters the vertical collecting cylinder body between lower piston and upper piston, in this mistake
In journey, upper piston the most up moves through first piston bar, connecting rod and the second piston rod and drives switching piston one ibid
Move, till upper piston is resisted against on the 3rd limited block.When upper piston is resisted against on the 3rd limited block, intake interface and
Two lower interfaces are positioned at the same side of switching piston, and the gas hereafter evaporated in shuttle will be by the second lower interface, down tube
Road and the first lower interface enter in the vertical collecting cylinder body below lower piston, so that lower piston the most up moves, at this
During pressure in vertical collecting cylinder body between lower piston and upper piston gradually toward increasing, thus promote lower piston and upper piston
Between volatile material cooling water effect under condensation liquefaction, its condensation liquefaction is effective, and can improve condensation liquefaction effect
Rate.
On the other hand, the volatile material evaporation separation process of the distilling apparatus of the present embodiment is entered in being in airtight environment
OK, volatile material can be avoided to spill in outside air in evaporation separation process, affect surrounding working environment.
3rd, close the 3rd controlled valve, heater stop heats.
4th, open second switch valve and make the volatile material of the liquid between lower piston and upper piston be led to by blanking
Hole and vertically blanking pipe flow out, thus obtain the volatile material of isolated liquid.Meanwhile, upper piston is at back-moving spring
Move down under effect reset.
5th, the first controlled valve makes lower piston move down under the effect of extension spring reset.
Claims (7)
1. measure a distilling apparatus for volatile material, it is characterized in that, including there is the shuttle of sealed internal chamber, for adding
The heater of hot shuttle, volatile material collection device, for cooling down the condensing unit of volatile material collection device
And self adaptation switching device, the top of described shuttle is provided with exhaust port, and described volatile material collection device includes
The vertical collecting cylinder body of lower closed at both ends, the first limited block being successively set on vertical collecting cylinder body medial surface from bottom to top,
Second limited block and the 3rd limited block, the lower piston being arranged between the first limited block and the second limited block, it is arranged on the second limit
Interface on upper piston between position block and the 3rd limited block, the first lower interface and first of being arranged on vertical collecting cylinder body, the
One lower interface is between vertical collecting cylinder body bottom surface and the first limited block, and on first, interface is positioned at the first limited block and the second limit
Between the block of position, being provided with bar through hole in the middle part of the upper surface of described vertical collecting cylinder body, the upper end of upper piston is provided with first piston bar,
And first piston bar is through bar through hole,
Described self adaptation switching device includes vertically switching cylinder body, the switching piston being arranged in vertical switching cylinder body, being arranged on
The second piston rod on switching piston, the second lower interface being successively set on vertical switching cylinder body lateral surface from bottom to top, enter
Interface on gas interface and second, described switching piston on the second lower interface and second between interface, described second piston rod
Upper end up extend through the end face of vertically switching cylinder body and be positioned at the top vertically switching cylinder body, the second piston rod and first
It is connected by connecting rod between piston rod, is connected by admission line between described exhaust port and intake interface, first
Be connected by lower pipeline between lower interface and the second lower interface, on first on interface and second between interface by upper pipeline phase
Connect.
A kind of distilling apparatus measuring volatile material the most according to claim 1, is characterized in that, when upper piston is resisted against
Time on second limited block, on described intake interface and second, interface is positioned at the same side of switching piston；When upper piston is resisted against
Time on three limited blocks, described intake interface and the second lower interface are positioned at the same side of switching piston.
A kind of distilling apparatus measuring volatile material the most according to claim 1, is characterized in that, described lower piston is with perpendicular
It is provided with extension spring between the straight bottom surface collecting cylinder body.
4., according to a kind of distilling apparatus measuring volatile material described in claim 1 or 2 or 3, it is characterized in that, described upper work
It is provided with back-moving spring between plug and the end face of vertical collecting cylinder body.
5., according to a kind of distilling apparatus measuring volatile material described in claim 1 or 2 or 3, it is characterized in that, described vertically
The bottom surface collecting cylinder body is provided with exhaustor, and exhaustor is provided with the first controlled valve.
6., according to a kind of distilling apparatus measuring volatile material described in claim 1 or 2 or 3, it is characterized in that, described lower work
It is provided with the lower material through hole running through lower piston upper and lower surface beyond the Great Wall, is provided with vertical blanking pipe in described vertical collecting cylinder body, vertically
The lower end collecting cylinder body is provided with guide through hole, and the upper end of vertical blanking pipe is tightly connected, vertically with the lower port of lower material through hole
The lower end of blanking pipe passes guide through hole and is positioned at inside the lower section of vertical collecting cylinder body, vertical blanking pipe and guide through hole
Sealing ring it is provided with, on vertical blanking pipe and be positioned at the lower section of vertical collecting cylinder body and be provided with the first controlled valve between face.
7., according to a kind of distilling apparatus measuring volatile material described in claim 1 or 2 or 3, it is characterized in that, described condensation
Device includes the cooling bucket being set on vertical collecting cylinder body, and the bottom surface of cooling bucket is positioned at the first limited block and the second limited block
Between.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610374179.6A CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610374179.6A CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106075944A true CN106075944A (en) | 2016-11-09 |
| CN106075944B CN106075944B (en) | 2017-11-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610374179.6A Active CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
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| Country | Link |
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| CN (1) | CN106075944B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2785675Y (en) * | 2005-03-21 | 2006-06-07 | 韦建永 | Efficient energy-saving distilled-water machine |
| JP2008200583A (en) * | 2007-02-19 | 2008-09-04 | Yoshio Yoshimura | Distillation apparatus |
| CN202460159U (en) * | 2012-03-13 | 2012-10-03 | 成都建中香料香精有限公司 | Collecting device for condensed liquid material in distillation system of easily solidified material |
| CN203768306U (en) * | 2014-01-15 | 2014-08-13 | 佛山市和挚承环保科技有限公司 | Distillation tower with heating device |
| CN204182148U (en) * | 2014-09-24 | 2015-03-04 | 宋志国 | A kind of Distallation systm |
-
2016
- 2016-05-30 CN CN201610374179.6A patent/CN106075944B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2785675Y (en) * | 2005-03-21 | 2006-06-07 | 韦建永 | Efficient energy-saving distilled-water machine |
| JP2008200583A (en) * | 2007-02-19 | 2008-09-04 | Yoshio Yoshimura | Distillation apparatus |
| CN202460159U (en) * | 2012-03-13 | 2012-10-03 | 成都建中香料香精有限公司 | Collecting device for condensed liquid material in distillation system of easily solidified material |
| CN203768306U (en) * | 2014-01-15 | 2014-08-13 | 佛山市和挚承环保科技有限公司 | Distillation tower with heating device |
| CN204182148U (en) * | 2014-09-24 | 2015-03-04 | 宋志国 | A kind of Distallation systm |
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| Publication number | Publication date |
|---|---|
| CN106075944B (en) | 2017-11-28 |
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Address after: 315000 Block A, Qingyi Road, Ningbo High-tech Zone, Zhejiang Province Patentee after: Ningbo Entry-exit Inspection and Quarantine Bureau Technical Center of the People's Republic of China Address before: 315012 Ma Yuan Road, Haishu District, Ningbo, Zhejiang Province, No. 9 Patentee before: Ningbo Entry-exit Inspection and Quarantine Bureau Technical Center of the People's Republic of China |