CN207429707U - A kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device - Google Patents

Abstract

The utility model discloses a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation devices, including preheating can, evaporator body, cyclone separator and fluid reservoir A, the preheating can includes tank body and electrical heating elements A, steam pipe is welded at the upper side of the evaporator body, the steam pipe is communicated with the heating chamber inside evaporator body, the evaporator body upper end is welded with steam outlet pipe, outlet tube is welded in the cyclone separator lowermost position, it is tightly connected between outlet tube and fluid reservoir A below the cyclone separator by conduit, gas-guide tube is welded on the top position of the fluid reservoir A.The utility model is by setting preheating can, evaporator body and fluid reservoir A, it solves due to extracting sample repeatedly, adds unnecessary process, while also avoid extracting sample repeatedly, the problem of affecting the quality of solution, while solve the problems, such as that processing efficiency is low.

Description

A kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device

Technical field

The utility model is related to technical field of chemical, are specially a kind of processing loop coil decenol chiral intermediate ratio Concentration and evaporation device.

Background technology

Loop coil decenol is a kind of chemical substance, is a kind of colourless to weak yellow liquid, is naturally occurring in cilantro, can It is allocated for daily chemical essence formula, it is necessary to carry out concentration and evaporation in proportion to it during being processed to it, to ensure its hair Wave the effect of it should have.

Shortcoming deficiency possessed by the prior art：

1. in evaporation process, since evaporator and solution self-temperature are too low, cause evaporation efficiency low, heat conduction rate Slowly；

2. it is inconvenient for the sampling of substance after evaporation, sample is extracted repeatedly, adds unnecessary process, simultaneously Also avoid extracting sample repeatedly, affect the quality of solution；

3. existing vaporising device work efficiency is low, inconvenient for the recycling of waste material.

The content of the invention

（One）The technical issues of solution

In view of the deficiencies of the prior art, it is dense to provide a kind of processing loop coil decenol chiral intermediate ratio for the utility model Contracting vaporising device solves due to extracting sample repeatedly, adds unnecessary process, while also avoid extracting sample repeatedly Product, the problem of affecting the quality of solution, while solve the problems, such as that processing efficiency is low.

（Two）Technical solution

To achieve the above object, the utility model provides following technical solution：Among a kind of processing loop coil decenol is chiral Body ratio concentration and evaporation device, including preheating can, evaporator body, cyclone separator and fluid reservoir A, the preheating can includes tank Body and electrical heating elements A, the inside of the tank body are equipped with electrical heating elements A, feed pipe are welded at the upper side of the tank body, Discharge nozzle is welded on the lower position of the tank body opposite side, below the discharge nozzle and evaporator body below the tank body It is tightly connected between inlet tube by conduit, the inside of the evaporator body is equipped with electrical heating elements B, the evaporator sheet Steam pipe is welded at the upper side of body, the steam pipe is communicated with the heating chamber inside evaporator body, the evaporator body Upper end is welded with steam outlet pipe, is tightly connected between the steam outlet pipe and the air inlet of cyclone separator by conduit, the eddy flow Outlet tube is welded in separator lowermost position, by leading between the outlet tube and fluid reservoir A below the cyclone separator The seal of tube connects, and is welded with gas-guide tube on the top position of the fluid reservoir A, is equipped between the gas-guide tube and fluid reservoir A Solenoid valve is tightly connected between the gas-guide tube and barostat, the gas-guide tube between the barostat and vacuum machine On be provided with branched pipe, solenoid valve is provided on the branched pipe, is installed on the gas-guide tube between the branched pipe and vacuum machine There is a solenoid valve, be provided with seal nipple on the material taking mouth below the fluid reservoir A, seal nipple and sample on the fluid reservoir A It is tightly connected between product tank by conduit.

Preferably, sealed between the venthole above the cyclone separator and the air intake of tubular heat exchanger by conduit It connects, is tightly connected between the liquid outlet and fluid reservoir B below the tubular heat exchanger by conduit.

Preferably, direct-acting electromagnetic valve is installed on the conduit between the fluid reservoir A seal nipples and sample jar.

Preferably, pressure gauge is installed on the fluid reservoir A.

Preferably, temperature sensor is all installed inside the preheating can and evaporator body.

（Three）Advantageous effect

The utility model provides a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device, possesses following Advantageous effect：

（1）The utility model will be treated by setting preheating can, evaporator body, electrical heating elements A and electrical heating elements B Processing substance is passed through inside preheating can, and electrical heating elements A preheats the in vivo solution of tank, adds quality and the steaming of evaporation The rate of hair, simultaneously electrical heating elements B carries out the pre-heat treatment to evaporator body inside evaporator body, ensure that steam Thermal conductivity, avoid because evaporator body case temperature is too low that thermal conductivity is caused to decline.

（2）The utility model adds inert gas by setting fluid reservoir A and sample jar into anti-fluid reservoir A, at this point, Air pressure increase in fluid reservoir A, according to the value of material to be taken, fills suitable inert gas thereto, all after inflation Solenoid valve is all closed, and opens direct-acting electromagnetic valve, due to air pressure, the material in fluid reservoir A is transported to liquid storage along conduit In tank A, pressure gauge shows the pressure in current fluid reservoir A, and when pressure returns to initial value, direct-acting electromagnetic valve is closed, this sets Meter avoids extracting sample repeatedly, adds unnecessary process, while also avoids extracting sample repeatedly, affects the matter of solution Amount.

（3）The utility model is by setting fluid reservoir B, and for exhaust gas after tubular heat exchanger condenses, waste liquid is flowed into liquid storage Case B, convenient for the collection to waste liquid.

Description of the drawings

Fig. 1 is the utility model overall structure diagram；

Fig. 2 is preheating can structure diagram in the utility model Fig. 1；

Fig. 3 is evaporator body structure diagram in the utility model Fig. 1；

Fig. 4 is fluid reservoir A structure diagrams in the utility model Fig. 1；

Fig. 5 is the assembling structure schematic diagram of fluid reservoir A in the utility model Fig. 1.

In figure：1 preheating can, 2 evaporator bodies, 3 cyclone separators, 4 tubular heat exchangers, 5 fluid reservoir A, 6 fluid reservoir B, 7 Electrical heating elements A, 8 tank bodies, 9 steam outlet pipes, 10 electrical heating elements B, 11 steam pipes, 12 inlet tubes, 13 gas-guide tubes, 14 direct drive type electros Magnet valve, 15 sample jars, 16 solenoid valves, 17 barostats, 18 branched pipes.

Specific embodiment

The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out It clearly and completely describes, it is clear that the described embodiments are only a part of the embodiments of the utility model rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work All other embodiments obtained shall fall within the protection scope of the present invention.

As shown in Figs. 1-5, the utility model provides a kind of technical solution：A kind of processing loop coil decenol chiral intermediate ratio Example concentration and evaporation device, including preheating can 1, evaporator body 2, cyclone separator 3 and fluid reservoir A5, preheating can 1 includes tank body 8 With electrical heating elements A7, the inside of tank body 8 is equipped with electrical heating elements A7, and 8 upper side of tank body is welded with feed pipe, tank body 8 Be welded with discharge nozzle on the lower position of opposite side, the discharge nozzle of 8 lower section of tank body and the inlet tube 12 of 2 lower section of evaporator body it Between be tightly connected by conduit, the inside of evaporator body 2 is equipped with electrical heating elements B10 preheating cans 1 and evaporator body 2 Inside is all equipped with temperature sensor, is electrically connected between the temperature sensor and electrical heating elements A7 in preheating can 1, evaporator It is electrically connected between temperature sensor and electrical heating elements B10 inside body 2, substance to be processed is passed through inside preheating can 1, Electrical heating elements A7 preheats the solution in tank body 8, adds the quality of evaporation and the rate of evaporation, simultaneously evaporates 2 inside electrical heating elements B10 of device body to evaporator body 2 carry out the pre-heat treatment, ensure that the thermal conductivity of steam, avoid because For 2 case temperature of evaporator body is too low thermal conductivity is caused to decline, when being preheating to certain temperature, electrical heating elements A7 and electricity Heating element B10 is all stopped, and the solution in preheating can 1 is transported to from inlet tube 12 in evaporator body 2, evaporator sheet 2 upper side of body is welded with steam pipe 11, and steam pipe 11 is communicated with the heating chamber inside evaporator body 2, into steam pipe 11 Logical to put steam, steam heats solution, solution fast vaporizing under the action of steam, and 2 upper end of evaporator body is welded with It is tightly connected between the air inlet of steam outlet pipe 9, steam outlet pipe 9 and cyclone separator 3 by conduit, 3 top of cyclone separator goes out It is tightly connected between the air intake of steam ports and tubular heat exchanger 4 by conduit, the liquid outlet and fluid reservoir of 4 lower section of tubular heat exchanger It is tightly connected between B6 by conduit, outlet tube is welded in 3 lowermost position of cyclone separator, 3 lower section of cyclone separator It is tightly connected between outlet tube and fluid reservoir A5 by conduit, gas-guide tube 13, gas-guide tube is welded on the top position of fluid reservoir A Solenoid valve 16 between 13 and fluid reservoir A5 is installed, is tightly connected between gas-guide tube 13 and barostat 17, barostat Branched pipe 18 is provided on gas-guide tube 13 between 17 and vacuum machine, is provided with solenoid valve 16 on branched pipe 18, branched pipe 18 with Solenoid valve 16 on the gas-guide tube 13 between vacuum machine is installed, pressure gauge is installed on fluid reservoir A5, taking below fluid reservoir A5 It is provided with seal nipple in material mouth, is tightly connected between the seal nipple and sample jar 15 on fluid reservoir A5 by conduit, liquid storage Direct-acting electromagnetic valve 14 is installed, the solution after vaporization is transported to eddy flow on the conduit between tank A5 seal nipples and sample jar 15 In separator 3, cyclone separator 3 carries out gas-liquid separation to it, ensures its machining accuracy, and the liquid after separation is conveyed along outlet tube Into fluid reservoir A5, the gas isolated is transported in tubular heat exchanger 4, and gas conveys after being condensed in tubular heat exchanger 4 It is stored into fluid reservoir B6, when needing to be sampled the solution in fluid reservoir A5, the solenoid valve 16 of vacuum machine junction is opened It opens, vacuum machine extracts the air in gas-guide tube 13 and branched pipe 18 out, and after extraction, which closes, branched pipe Solenoid valve 16 at 18 is opened, and the solenoid valve 16 between gas-guide tube 13 and fluid reservoir A5 opens simultaneously, by branched pipe 18 to anti- Inert gas is added in fluid reservoir A5, at this point, the air pressure increase in fluid reservoir A5, according to the value of material to be taken, fills suitable thereto The inert gas of amount, after inflation, all solenoid valves 16 are all closed, and direct-acting electromagnetic valve 14 are opened, due to the original of air pressure Cause, the material in fluid reservoir A5 are transported to along conduit in fluid reservoir A5, and pressure gauge shows the pressure in current fluid reservoir A5, works as pressure When power returns to initial value, direct-acting electromagnetic valve 14 is closed, this design avoids extracting sample repeatedly, adds unnecessary process, It also avoids extracting sample repeatedly simultaneously, affects the quality of solution.

In use, substance to be processed is passed through inside preheating can 1, electrical heating elements A7 carries out the solution in tank body 8 pre- Heat adds the quality of evaporation and the rate of evaporation, and simultaneously 2 inside electrical heating elements B10 of evaporator body is to evaporator Body 2 carries out the pre-heat treatment, ensure that the thermal conductivity of steam, and avoiding causes because 2 case temperature of evaporator body is too low Heating rate declines, and when being preheating to certain temperature, electrical heating elements A7 and electrical heating elements B10 are all stopped, by preheating can 1 Interior solution is transported to from inlet tube 12 in evaporator body 2, is led into steam pipe 11 and is put steam, steam adds solution Heat, solution fast vaporizing under the action of steam, the solution after vaporization are transported in cyclone separator 3, and cyclone separator 3 is to it Gas-liquid separation is carried out, ensures its machining accuracy, the liquid after separation is transported to along outlet tube in fluid reservoir A5, the gas isolated It is transported in tubular heat exchanger 4, gas is transported in fluid reservoir B6 after being condensed in tubular heat exchanger 4 and stores, when needs pair When solution in fluid reservoir A5 is sampled, the solenoid valve 16 of vacuum machine junction is opened, and vacuum machine is by gas-guide tube 13 and divides Air extraction in branch pipe 18, after extraction, which closes, and the solenoid valve 16 at branched pipe 18 is opened, gas-guide tube Solenoid valve 16 between 13 and fluid reservoir A5 opens simultaneously, and inert gas is added into anti-fluid reservoir A5 by branched pipe 18, this When, the air pressure increase in fluid reservoir A5 according to the value of material to be taken, fills suitable inert gas thereto, after inflation, institute Some solenoid valves 16 are all closed, and open direct-acting electromagnetic valve 14, due to air pressure, the material in fluid reservoir A5 is defeated along conduit It is sent in fluid reservoir A5, pressure gauge shows the pressure in current fluid reservoir A5, when pressure returns to initial value, direct-acting electromagnetic valve 14 close.

It can to sum up obtain, the utility model is solved by setting preheating can 1, evaporator body 2 and fluid reservoir A5 due to anti- Sample is extracted again, adds unnecessary process, while also avoiding extracting sample repeatedly, the quality for affecting solution is asked Topic, while solve the problems, such as that processing efficiency is low.

It should be noted that herein, relational terms such as first and second and the like are used merely to a reality Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to Non-exclusive inclusion, so that process, method, article or equipment including a series of elements not only will including those Element, but also including other elements that are not explicitly listed or further include as this process, method, article or equipment Intrinsic element.

While there has been shown and described that the embodiment of the utility model, for the ordinary skill in the art, It is appreciated that in the case where not departing from the principle of the utility model and spirit can these embodiments be carried out with a variety of variations, repaiied Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.

Claims (5)

1. a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device, including preheating can（1）, evaporator body （2）, cyclone separator（3）With fluid reservoir A（5）, it is characterised in that：The preheating can（1）Including tank body（8）And electrical heating elements A（7）, the tank body（8）Inside electrical heating elements A is installed（7）, the tank body（8）Upper side is welded with feed pipe, institute State tank body（8）Discharge nozzle, the tank body are welded on the lower position of opposite side（8）The discharge nozzle and evaporator body of lower section （2）The inlet tube of lower section（12）Between be tightly connected by conduit, the evaporator body（2）Inside be equipped with electrical heating member Part B（10）, the evaporator body（2）Upper side is welded with steam pipe（11）, the steam pipe（11）With evaporator body （2）Internal heating chamber communicates, the evaporator body（2）Upper end is welded with steam outlet pipe（9）, the steam outlet pipe（9）With eddy flow Separator（3）Air inlet between be tightly connected by conduit, the cyclone separator（3）Liquid is welded with out in lowermost position Pipe, the cyclone separator（3）The outlet tube of lower section and fluid reservoir A（5）Between be tightly connected by conduit, the fluid reservoir A （5）Top position on be welded with gas-guide tube（13）, the gas-guide tube（13）With fluid reservoir A（5）Between solenoid valve is installed （16）, the gas-guide tube（13）With barostat（17）Between be tightly connected, the barostat（17）With vacuum machine it Between gas-guide tube（13）On be provided with branched pipe（18）, the branched pipe（18）On be provided with solenoid valve（16）, the branched pipe （18）Gas-guide tube between vacuum machine（13）On solenoid valve is installed（16）, the fluid reservoir A（5）It is set on the material taking mouth of lower section It is equipped with seal nipple, the fluid reservoir A（5）On seal nipple and sample jar（15）Between be tightly connected by conduit.

2. a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device according to claim 1, feature It is：The cyclone separator（3）The venthole and tubular heat exchanger of top（4）Air intake between pass through conduit sealing connect It connects, the tubular heat exchanger（4）The liquid outlet of lower section and fluid reservoir B（6）Between be tightly connected by conduit.

3. a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device according to claim 1, feature It is：The fluid reservoir A（5）Seal nipple and sample jar（15）Between conduit on direct-acting electromagnetic valve is installed（14）.

4. a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device according to claim 1, feature It is：The fluid reservoir A（5）On pressure gauge is installed.

5. a kind of processing loop coil decenol chiral intermediate ratio concentration and evaporation device according to claim 1, feature It is：The preheating can（1）And evaporator body（2）Inside is all equipped with temperature sensor.