CN106075944B - A kind of distilling apparatus for determining volatile materials - Google Patents
A kind of distilling apparatus for determining volatile materials Download PDFInfo
- Publication number
- CN106075944B CN106075944B CN201610374179.6A CN201610374179A CN106075944B CN 106075944 B CN106075944 B CN 106075944B CN 201610374179 A CN201610374179 A CN 201610374179A CN 106075944 B CN106075944 B CN 106075944B
- Authority
- CN
- China
- Prior art keywords
- cylinder body
- piston
- interface
- vertical
- limited block
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of distilling apparatus for determining volatile materials, it is desirable to provide a kind of condensation liquefaction effect is good, and can improve the distilling apparatus of the measure volatile materials of condensation liquefaction efficiency.It includes shuttle, heater, volatile materials collection device, condensing unit and adaptive switching device, volatile materials collection device includes the vertical collecting cylinder body of upper and lower ends closing, the first limited block being successively set on from bottom to top on vertical collecting cylinder body medial surface, second limited block and the 3rd limited block, the lower piston being arranged between the first limited block and the second limited block, the upper piston being arranged between the second limited block and the 3rd limited block, it is arranged on interface on the first lower interface and first on vertical collecting cylinder body, adaptive switching device includes vertical switching cylinder body, the switching piston being arranged in vertical switching cylinder body, the second lower interface being arranged on vertical switching cylinder body lateral surface, interface on intake interface and second.
Description
Technical field
The present invention relates to a kind of distilling apparatus, and in particular to a kind of distilling apparatus for determining volatile materials.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it is different using each component boiling point in mixing liquid or liquid-solid system,
Low boiling component is evaporated, then is condensed to separate the unit process of whole component, is two kinds of unit operations of evaporation and condensation
Joint.The distilling apparatus of current volatile materials is equally different using each component boiling point, makes lower boiling volatility thing
Matter evaporation separation, the volatile materials then isolated using cooling water to evaporation are condensed to obtain volatile materials.At present
By the way of this single volatile materials isolated using cooling water to evaporation of volatile materials distilling apparatus is condensed
Not only condensation liquefaction efficiency is low, and condensation liquefaction is ineffective, comes especially for the relatively low volatile materials of condensation temperature
Say, it is single worse using the liquefied effect of cooling water condensation.
The content of the invention
The invention aims to overcome the deficiencies in the prior art, there is provided and a kind of condensation liquefaction effect is good, and
The distilling apparatus of the measure volatile materials of condensation liquefaction efficiency can be improved.
The technical scheme is that：
A kind of distilling apparatus for determining volatile materials includes the shuttle with sealed internal chamber, held for heating sample
The heater of device, volatile materials collection device, the condensing unit for cooling down volatile materials collection device and adaptive
Switching device, the top of the shuttle are provided with exhaust port, and the volatile materials collection device seals including upper and lower ends
It is the vertical collecting cylinder body that closes, the first limited block being successively set on from bottom to top on vertical collecting cylinder body medial surface, second spacing
Block and the 3rd limited block, the lower piston being arranged between the first limited block and the second limited block, it is arranged on the second limited block and
Upper piston between three limited blocks, interface on the first lower interface and first being arranged on vertical collecting cylinder body, the first lower interface
Between vertical collecting cylinder body bottom surface and the first limited block, on first interface be located at the first limited block and the second limited block it
Between, bar through hole is provided with the middle part of the upper surface of the vertical collecting cylinder body, the upper end of upper piston is provided with First piston bar, and first
Piston rod passes through bar through hole, and the adaptive switching device includes vertical switching cylinder body, is arranged in vertical switching cylinder body
Switching piston, the second piston bar being arranged on switching piston, it is successively set on from bottom to top on vertical switching cylinder body lateral surface
The second lower interface, interface on intake interface and second, the switching piston is located on the second lower interface and second between interface,
The upper end of the second piston bar up extends through the top surface of vertical switching cylinder body and is located at the top of vertical switching cylinder body, the
It is connected between two piston rods and First piston bar by connecting rod, passes through air inlet pipe between the exhaust port and intake interface
Road is connected, and is connected between the first lower interface and the second lower interface by lower pipeline, on first on interface and second interface it
Between be connected by upper pipeline.
Preferably, when upper piston is resisted against on the second limited block, the intake interface is located at interface on second to be cut
Change the same side of piston；When upper piston is resisted against on the 3rd limited block, the intake interface and the second lower interface are positioned at switching
The same side of piston.
Preferably, extension spring is provided between the bottom surface of lower piston and vertical collecting cylinder body.
Preferably, back-moving spring is provided between the top surface of upper piston and vertical collecting cylinder body.
Preferably, the bottom surface of vertical collecting cylinder body is provided with blast pipe, and blast pipe is provided with first switch valve.
Preferably, lower piston is provided with the lower material through hole through lower piston upper and lower surface, in the vertical collecting cylinder body
Provided with vertical blanking pipe, the lower end of vertical collecting cylinder body is provided with guide through hole, the upper end of vertical blanking pipe and lower material through hole
Lower port be tightly connected, the lower end of vertical blanking pipe is through guide through hole and positioned at the lower section of vertical collecting cylinder body, vertically
Sealing ring is provided between blanking pipe and guide through hole medial surface, on vertical blanking pipe and positioned at the lower section of vertical collecting cylinder body
Provided with second switch valve.
Preferably, condensing unit includes the cooling bucket being set on vertical collecting cylinder body, and the bottom surface for cooling down bucket is located at
Between first limited block and the second limited block.
The beneficial effects of the invention are as follows：
First, condensation liquefaction effect is good, and condensation liquefaction efficiency can be improved.
Second, volatile materials can be avoided to be spilt into separation process is evaporated in outside air, building ring around is influenceed
Border.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the present invention.
In figure：Shuttle 1, exhaust port 11, heater 2, admission line 3, the 3rd controlled valve 31, volatility thing
Matter collection device 4, second switch valve 41, vertical blanking pipe 42, extension spring 43, the first limited block 44, lower material through hole 45, lower work
Interface 47, the second limited block 48, upper piston 49, the 3rd limited block 410, back-moving spring 411, First piston bar on plug 46, first
412nd, vertical collecting cylinder body 413, the first lower interface 414, blast pipe 415, first switch valve 416, adaptive switching device 5,
Vertical switching cylinder body 51, switching piston 52, intake interface 53, the second lower interface 54, interface 56 in second piston bar 55, second,
Connecting rod 6, condensing unit 7, connecting tube 8, check valve 81.
Embodiment
The present invention is described in further detail with embodiment below in conjunction with the accompanying drawings：
As shown in figure 1, a kind of distilling apparatus for determining volatile materials includes the shuttle 1 with sealed internal chamber, used
In the heater 2 of heating shuttle, volatile materials collection device 4, for cooling down the cold of volatile materials collection device
Solidifying device 7 and adaptive switching device 5.The top of shuttle is provided with exhaust port 11.Heater is electric heater or water
Heater is bathed, the heater of the present embodiment is water-bath heater, and water-bath heater includes heating container and is arranged on heating appearance
Heating tube in device.Shuttle is in heating container.
Volatile materials collection device includes the vertical collecting cylinder body 413 of upper and lower ends closing, set gradually from bottom to top
The first limited block 44, the second limited block 48 and the 3rd limited block 410 on vertical collecting cylinder body medial surface, it is arranged on the first limit
Position block and the second limited block between lower piston 46, be arranged between the second limited block and the 3rd limited block upper piston 49, set
Put interface 47 on the first lower interface 414 and first on vertical collecting cylinder body.First lower interface is located at vertical collecting cylinder body bottom
Between face and the first limited block, and when lower piston is resisted against on the first limited block, interface is located at the upper of lower piston on first
Side.Interface is between the first limited block and the second limited block on first.Bar is provided with the middle part of the upper surface of vertical collecting cylinder body
Through hole.The upper end of upper piston is provided with First piston bar 412, and First piston bar passes through bar through hole.Lower piston and vertical collecting
Extension spring 43 is provided between the bottom surface of cylinder body, one end of extension spring is connected with lower piston, the bottom surface of the other end and vertical collecting cylinder body
It is connected.Back-moving spring 411 is provided between the top surface of upper piston and vertical collecting cylinder body.
The bottom surface of vertical collecting cylinder body is provided with blast pipe 415, and blast pipe is provided with first switch valve 416.Lower work
The lower material through hole 45 through lower piston upper and lower surface is provided with beyond the Great Wall.Lower material through hole and lower piston are coaxial.Set in vertical collecting cylinder body
There is vertical blanking pipe 42.Vertical blanking pipe and vertical collecting cylinder body are coaxial.The lower end of vertical collecting cylinder body, which is provided with to be oriented to, to be led to
Hole.The upper end of vertical blanking pipe is tightly connected with the lower port of lower material through hole, and the lower end of vertical blanking pipe is logical through being oriented to
Hole and the lower section for being located at vertical collecting cylinder body.Sealing ring is provided between blanking pipe and guide through hole medial surface vertically.Under vertical
Second switch valve 41 is provided with pipe material and positioned at the lower section of vertical collecting cylinder body.
Condensing unit includes the cooling bucket being set on vertical collecting cylinder body, and the bottom surface for cooling down bucket is located at the first limited block
Between the second limited block.Interface is provided with connecting tube 8 on first, the connecting tube through cooling bucket side wall, and connecting tube with
It is tightly connected between the side wall of cooling bucket.Check valve 81 is provided with connecting tube and on the outside of cooling bucket.
Adaptive switching device includes vertical switching cylinder body 51, the switching piston 52 being arranged in vertical switching cylinder body, set
Put the second piston bar 55 on switching piston, be successively set on from bottom to top on vertical switching cylinder body lateral surface second under connect
Interface 56 on mouth 54, intake interface 53 and second.The diameter of upper piston is more than twice of the diameter of switching piston.Intake interface
Bore is more than the spacing between switching piston both ends of the surface.Switching piston is located on the second lower interface and second between interface.Second
The upper end of piston rod up extends through the top surface of vertical switching cylinder body and positioned at the top of vertical switching cylinder body.Second piston bar
It is connected between First piston bar by connecting rod 6.Connecting rod is located at the top of vertical collecting cylinder body.Exhaust port and air inlet
It is connected between interface by admission line 3.Admission line is provided with the 3rd controlled valve 31.Connect under first lower interface and second
It is connected between mouthful by lower pipeline.It is connected on first between interface and interface on second by upper pipeline, specifically, even
The port of adapter is connected between interface on second by upper pipeline.
When upper piston is resisted against on the second limited block, intake interface is located at the same of switching piston with interface on second
Side.When upper piston is resisted against on the 3rd limited block, intake interface and the second lower interface are located at the same side of switching piston.
The specific work process of the distilling apparatus of the measure volatile materials of the present embodiment is as follows：
First, as shown in figure 1, mixed fluid sample is put into shuttle, it is put into the cooling bucket of condensing unit
Cooling water.
Second, the 3rd controlled valve is opened, shuttle is heated by heater, makes to mix in shuttle
Volatile materials evaporation separation in liquid, volatile materials are entered in vertical switching cylinder body by admission line；Then, pass through
Interface on second, interface enters in the vertical collecting cylinder body between lower piston and upper piston on upper pipeline and first, in this mistake
Upper piston gradually up moves through First piston bar, connecting rod and second piston bar drive switching piston one and is same as above in journey
Move, untill upper piston is resisted against on the 3rd limited block.When upper piston is resisted against on the 3rd limited block, intake interface and
Two lower interfaces are located at the same side of switching piston, and the gas hereafter evaporated in shuttle will pass through the second lower interface, down tube
Road and the first lower interface enter in the vertical collecting cylinder body below lower piston, so that lower piston gradually up moves, at this
During pressure in vertical collecting cylinder body between lower piston and upper piston gradually toward increase, so as to promote lower piston and upper piston
Between volatile materials in the presence of cooling water condensation liquefaction, its condensation liquefaction effect is good, and can improve condensation liquefaction effect
Rate.
On the other hand, the volatile materials evaporation separation process of the distilling apparatus of the present embodiment is in closed environment
OK, volatile materials can be avoided to be spilt into separation process is evaporated in outside air, influence surrounding working environment.
3rd, close the 3rd controlled valve, heater stop heating.
4th, opening second switch valve makes the volatile materials of the liquid between lower piston and upper piston lead to by blanking
Hole and the outflow of vertical blanking pipe, so as to the volatile materials of liquid isolated.Meanwhile upper piston is in back-moving spring
Move down reset under effect.
5th, first switch valve makes lower piston be moved down in the presence of extension spring reset.
Claims (6)
1. it is a kind of determine volatile materials distilling apparatus, it is characterized in that, including the shuttle with sealed internal chamber, for adding
Heater, volatile materials collection device, the condensing unit for cooling down volatile materials collection device of hot shuttle
And adaptive switching device, the top of the shuttle are provided with exhaust port, the volatile materials collection device includes upper
Under vertical collecting cylinder body closed at both ends, be successively set on from bottom to top on vertical collecting cylinder body medial surface the first limited block,
Second limited block and the 3rd limited block, the lower piston being arranged between the first limited block and the second limited block, it is arranged on the second limit
Interface on upper piston, the first lower interface and first for being arranged on vertical collecting cylinder body between position block and the 3rd limited block, the
One lower interface is between vertical collecting cylinder body bottom surface and the first limited block, and interface is located at the first limited block and the second limit on first
Between the block of position, bar through hole is provided with the middle part of the upper surface of the vertical collecting cylinder body, the upper end of upper piston is provided with First piston bar,
And First piston bar passes through bar through hole,
The adaptive switching device includes vertical switching cylinder body, the switching piston being arranged in vertical switching cylinder body, is arranged on
Second piston bar on switching piston, the second lower interface being successively set on from bottom to top on vertical switching cylinder body lateral surface, enter
Interface on gas interface and second, the switching piston are located on the second lower interface and second between interface, the second piston bar
Upper end up extend through the top surface of vertical switching cylinder body and positioned at the top of vertical switching cylinder body, second piston bar and first
It is connected between piston rod by connecting rod, is connected between the exhaust port and intake interface by admission line, first
It is connected between lower interface and the second lower interface by lower pipeline, passes through upper pipeline phase on first between interface and interface on second
Connection；
When upper piston is resisted against on the second limited block, the intake interface is located at the same of switching piston with interface on second
Side；When upper piston is resisted against on the 3rd limited block, the intake interface and the second lower interface are located at the same side of switching piston.
2. a kind of distilling apparatus for determining volatile materials according to claim 1, it is characterized in that, the lower piston is with erecting
Extension spring is provided between the straight bottom surface for collecting cylinder body.
3. a kind of distilling apparatus for determining volatile materials according to claim 1 or 2, it is characterized in that, the upper piston
Back-moving spring is provided between the top surface of vertical collecting cylinder body.
4. a kind of distilling apparatus for determining volatile materials according to claim 1 or 2, it is characterized in that, the vertical receipts
The bottom surface of collection cylinder body is provided with blast pipe, and blast pipe is provided with first switch valve.
5. a kind of distilling apparatus for determining volatile materials according to claim 1 or 2, it is characterized in that, the lower piston
The lower material through hole through lower piston upper and lower surface is provided with, vertical blanking pipe is provided with the vertical collecting cylinder body, it is vertical to receive
The lower end of collection cylinder body is provided with guide through hole, and the upper end of vertical blanking pipe and the lower port of lower material through hole are tightly connected, under vertical
The lower end of pipe material is through guide through hole and positioned at the lower section of vertical collecting cylinder body, vertical blanking pipe and guide through hole medial surface
Between be provided with sealing ring, be provided with second switch valve on vertical blanking pipe and positioned at the lower section of vertical collecting cylinder body.
6. a kind of distilling apparatus for determining volatile materials according to claim 1 or 2, it is characterized in that, the condensation dress
Put the cooling bucket including being set on vertical collecting cylinder body, and the bottom surface for cooling down bucket be located at the first limited block and the second limited block it
Between.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610374179.6A CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610374179.6A CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106075944A CN106075944A (en) | 2016-11-09 |
| CN106075944B true CN106075944B (en) | 2017-11-28 |
Family
ID=57230959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610374179.6A Active CN106075944B (en) | 2016-05-30 | 2016-05-30 | A kind of distilling apparatus for determining volatile materials |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106075944B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2785675Y (en) * | 2005-03-21 | 2006-06-07 | 韦建永 | Efficient energy-saving distilled-water machine |
| CN202460159U (en) * | 2012-03-13 | 2012-10-03 | 成都建中香料香精有限公司 | Collecting device for condensed liquid material in distillation system of easily solidified material |
| CN203768306U (en) * | 2014-01-15 | 2014-08-13 | 佛山市和挚承环保科技有限公司 | Distillation tower with heating device |
| CN204182148U (en) * | 2014-09-24 | 2015-03-04 | 宋志国 | A kind of Distallation systm |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008200583A (en) * | 2007-02-19 | 2008-09-04 | Yoshio Yoshimura | Distillation apparatus |
-
2016
- 2016-05-30 CN CN201610374179.6A patent/CN106075944B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2785675Y (en) * | 2005-03-21 | 2006-06-07 | 韦建永 | Efficient energy-saving distilled-water machine |
| CN202460159U (en) * | 2012-03-13 | 2012-10-03 | 成都建中香料香精有限公司 | Collecting device for condensed liquid material in distillation system of easily solidified material |
| CN203768306U (en) * | 2014-01-15 | 2014-08-13 | 佛山市和挚承环保科技有限公司 | Distillation tower with heating device |
| CN204182148U (en) * | 2014-09-24 | 2015-03-04 | 宋志国 | A kind of Distallation systm |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106075944A (en) | 2016-11-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104459016B (en) | A kind of element test instrument | |
| IES20150261A2 (en) | Boiler for concentrates preparation device | |
| IE20150229A1 (en) | Method of production of a boiler for a concentrates preparation device | |
| CN106075944B (en) | A kind of distilling apparatus for determining volatile materials | |
| CN207816756U (en) | A kind of experimental provision of high temperature and high pressure steam pyrolytic reaction | |
| CN102455257B (en) | Sampling device and method for low-water level shallow-liquid level high-temperature hot spring gas | |
| CN104353259B (en) | Combined type rectifying column and application thereof | |
| CN207445672U (en) | Adjustable solid-phase extraction column attachment device | |
| CN206671046U (en) | Acid closure is caught up with counteracting tank decompression | |
| CN209129604U (en) | A kind of production wellhead sampler | |
| CN109138963A (en) | Oil well gas fractionation unit | |
| CN208751915U (en) | A kind of double-U-shaped scale siphon pipe | |
| CN106932227B (en) | A kind of liquefaction of hex divides sampling device | |
| CN208494796U (en) | It is a kind of to use the perfusion rubber head for preventing scalding for manual | |
| CN208292952U (en) | A kind of oil field gas degreasing unit | |
| CN209696346U (en) | Nitrogen assist type positive pressure extraction element | |
| CN209043085U (en) | Extract the heat-exchanger rig of oil field extracted water heat | |
| CN208731271U (en) | A kind of lotion automatic packer | |
| CN207913260U (en) | A kind of rotary distilling apparatus for obtaining different fractions | |
| AU2015100480A4 (en) | Design method for accumulator unit for concentrates preparation device | |
| CN109946118A (en) | A kind of Portable oil-gas water-sampling device | |
| CN205938063U (en) | Oil pipe sample valve and oil pipe | |
| CN205216282U (en) | Device of extract oil in follow oil water mixture | |
| RU2172835C2 (en) | Sampler for research of gas-condensate wells | |
| CN209656386U (en) | A kind of field geothermal fluid gas sample sampling equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP02 | Change in the address of a patent holder | ||
| CP02 | Change in the address of a patent holder |
Address after: 315000 Block A, Qingyi Road, Ningbo High-tech Zone, Zhejiang Province Patentee after: Ningbo Entry-exit Inspection and Quarantine Bureau Technical Center of the People's Republic of China Address before: 315012 Ma Yuan Road, Haishu District, Ningbo, Zhejiang Province, No. 9 Patentee before: Ningbo Entry-exit Inspection and Quarantine Bureau Technical Center of the People's Republic of China |