CN106040118A - A preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco - Google Patents
A preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco Download PDFInfo
- Publication number
- CN106040118A CN106040118A CN201610306679.6A CN201610306679A CN106040118A CN 106040118 A CN106040118 A CN 106040118A CN 201610306679 A CN201610306679 A CN 201610306679A CN 106040118 A CN106040118 A CN 106040118A
- Authority
- CN
- China
- Prior art keywords
- microcapsule
- mass
- cigarette
- flos micheliae
- micheliae albae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
- B01J13/043—Drying and spraying
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Botany (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Agronomy & Crop Science (AREA)
- Dispersion Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The invention discloses a preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco, and belongs to the technical field of cigarette processing. The method is characterized in that the microcapsule is prepared by adding sodium alginate and gelatin in a mass ratio of 2:1 into water the mass of which is 10-15% of the sum of the mass of the sodium alginate and the mass of the gelatin, fully mixing, preparing into a wall material solution at 70-80 DEG C, cooling to 40-50 DEG C, adding white michelia essence oil the mass of which is 20-30% of the mass of the added wall material and an emulsifier the mass of which is 2-3% of the mass of the added wall material, performing high-pressure homogenization to form white michelia essence oil emulsion, and spray-drying to obtain the microcapsule. The microcapsule prepared by the method has good fluidity and dissolution dispersibility, is adopted as an additive into cigarette filters and then rolled into cigarettes. The microcapsule is capable of improving cigarette quality, reducing irritation, increasing aroma and improving moral cavity wettability.
Description
Technical field
The invention belongs to technical field of cigarette processing, be specifically related to a kind of Flos micheliae Albae essential oil microcapsules preparation method and
Application in Nicotiana tabacum L..
Background technology
Essence spice for cigarette is to specialize in each tobacco articles perfuming taste masking to use, in production of cigarettes, and essence spice for cigarette
Abundant in content, various in style.Its Type of aroma and aromatic style decide class and the grade of tobacco to a certain extent.Generally
Nicotiana tabacum L. can produce the Organic substance of some pungent tastes when burning, if adding some essence in medicated cigarette, it is possible to use fragrance
The acid produced during covering result of combustion of tobacco, is allowed to when burning and sucking produce good flue gas effect.But essence or quintessence oil are added
Enter cigarette shreds can increase the complexity of tobacco shred combustion process and generate the uncertainty of product harm, and the present invention is by essence
Add in cigarette filter and then can avoid this problem.
Flos micheliae Albae is the flower of Magnoliacea plant white orchid.It is warm in nature, bitter in the mouth is pungent, has cough-relieving and changes turbid effect.Its volatilization
Oil component reaches 81.9% to the effective percentage of chronic bronchitis.Flos micheliae Albae quintessence oil has strong fragrance, its complex chemical composition, main
Esters to be, alkenes, acids, ketone and ethers composition, and with linalool as bulk composition, Type of aroma be QINGXIANG, the Radix Aucklandiae and
The fragrance of a flower.
The present invention passes through microcapsule technology, solves volatile, oxidizable the asking during storing of Flos micheliae Albae essential oil product
Topic.The Flos micheliae Albae essential oil microcapsules of preparation is applied in cigarette filter, it is possible to decrease the harm of Medicated cigarette, improves Medicated cigarette igniting and sucking quality.
By literature search, identical with present invention open source literature report is had no.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of Flos micheliae Albae essential oil microcapsules and the application in Nicotiana tabacum L. thereof.
The present invention adopts the following technical scheme that
Sodium alginate that mass ratio is 2:1 and gelatin are added the water mix homogeneously of these two kinds of material masses 70 ~ 80%, in 70 ~ 80
Make wall material solution at DEG C, be cooled to 40 ~ 50 DEG C, the Flos micheliae Albae quintessence oil of the 20 ~ 30% of addition wall material amount and the emulsifying of 2 ~ 3%
Agent, is passed through high pressure homogenizer after 8000 ~ 10000r/min high-speed stirred 15min, under 70 ~ 80 DEG C and pressure 20 ~ 30MPa all
Matter three times, each 5min, form the emulsion of uniform particle diameter, be 150 ~ 180 DEG C in inlet temperature, outlet temperature is 70 ~ 100 DEG C,
Atomizing pressure is spray drying under conditions of 0.2 ~ 0.5MPa, obtains Flos micheliae Albae essential oil microcapsules.
Emulsifying agent of the present invention is tween 20.
Flos micheliae Albae essential oil microcapsules distilled water diluting of the present invention 800 ~ 1000 times, dilute solution is with filter tip weight
3% join in cigarette filter, filter tip cigarette is become cigarette.
The beneficial effects of the present invention is: Flos micheliae Albae essential oil microcapsules has good mobility and dissolution dispersity, will
It can improve cigarette quality in cigarette filter, reduces and stimulates, and increases fragrance, improves oral cavity wettability.
Further illustrate the present invention below in conjunction with detailed description of the invention, but the scope of protection of present invention is not limited to
In following embodiments.
Detailed description of the invention:
Embodiment 1:
Sodium alginate that mass ratio is 2:1 and gelatin are added the water mix homogeneously of these two kinds of material masses 70%, makes at 70 DEG C
Become wall material solution, be cooled to 40 DEG C, the Flos micheliae Albae quintessence oil of the 20% of addition wall material amount and emulsifier tween-20 of 2%, in
It is passed through high pressure homogenizer after 8000r/min high-speed stirred 15min, homogenizing three times under 70 DEG C and pressure 20MPa, each 5min,
Forming the emulsion of uniform particle diameter, be 150 DEG C in inlet temperature, outlet temperature is 70 DEG C, under conditions of atomizing pressure is 0.2MPa
It is spray-dried, obtains Flos micheliae Albae essential oil microcapsules.The Flos micheliae Albae essential oil microcapsules of gained distilled water diluting 1000 times, dilutes molten
Liquid joins in cigarette filter with the 3% of filter tip weight, and filter tip cigarette is become cigarette, carries out sensory evaluating smoking's qualification through perfumer, its
Note in fragrance increases, and with light Flos micheliae Albae feature note, fragrance is plentiful, abundant, harmony, and zest has dropped
Low, and the sensation of slightly Hui Tian on pleasant impression.
Embodiment 2:
Sodium alginate that mass ratio is 2:1 and gelatin are added the water mix homogeneously of these two kinds of material masses 80%, makes at 75 DEG C
Become wall material solution, be cooled to 45 DEG C, the Flos micheliae Albae quintessence oil of the 25% of addition wall material amount and emulsifier tween-20 of 3%, in
It is passed through high pressure homogenizer after 10000r/min high-speed stirred 15min, homogenizing three times under 75 DEG C and pressure 25MPa, each 5min,
Forming the emulsion of uniform particle diameter, be 160 DEG C in inlet temperature, outlet temperature is 80 DEG C, under conditions of atomizing pressure is 0.5MPa
It is spray-dried, obtains Flos micheliae Albae essential oil microcapsules.The Flos micheliae Albae essential oil microcapsules of gained distilled water diluting 800 times, dilutes molten
Liquid joins in cigarette filter with the 2.5% of filter tip weight, and filter tip cigarette is become cigarette, carries out sensory evaluating smoking's qualification through perfumer,
Note in its fragrance increases, and with light Flos micheliae Albae feature note, fragrance is plentiful, abundant, harmony, and zest has dropped
Low, and on pleasant impression, have the sensation of obvious Hui Tian.
Embodiment 3:
Sodium alginate that mass ratio is 2:1 and gelatin are added the water mix homogeneously of these two kinds of material masses 75%, makes at 80 DEG C
Become wall material solution, be cooled to 50 DEG C, the Flos micheliae Albae quintessence oil of the 30% of addition wall material amount and emulsifier tween-20 of 2.5%, in
It is passed through high pressure homogenizer after 10000r/min high-speed stirred 15min, homogenizing three times under 80 DEG C and pressure 30MPa, each 5min,
Forming the emulsion of uniform particle diameter, be 180 DEG C in inlet temperature, outlet temperature is 100 DEG C, under conditions of atomizing pressure is 0.3MPa
It is spray-dried, obtains Flos micheliae Albae essential oil microcapsules.The Flos micheliae Albae essential oil microcapsules of gained distilled water diluting 800 times, dilutes molten
Liquid joins in cigarette filter with the 3% of filter tip weight, and filter tip cigarette is become cigarette, carries out sensory evaluating smoking's qualification through perfumer, its
Note in fragrance increases, and with light Flos micheliae Albae feature note, fragrance is plentiful, abundant, harmony, and zest has dropped
Low, along with the increase of addition, the Nicotiana tabacum L. Radix Aucklandiae can slightly be suppressed, pleasant impression also can slightly bring residual.
Claims (3)
1. the preparation method of a Flos micheliae Albae essential oil microcapsules, it is characterised in that comprise the steps: that by mass ratio be 2:1's
Sodium alginate and gelatin add the water mix homogeneously of these two kinds of material masses 70 ~ 80%, make wall material solution at 70 ~ 80 DEG C, cold
But to 40 ~ 50 DEG C, the Flos micheliae Albae quintessence oil of the 20 ~ 30% of addition wall material amount and the emulsifying agent of 2 ~ 3%, in 8000 ~ 10000r/min
High pressure homogenizer it is passed through after high-speed stirred 15min, homogenizing three times under 70 ~ 80 DEG C and pressure 20 ~ 30MPa, each 5min, formed
The emulsion of uniform particle diameter, is 150 ~ 180 DEG C in inlet temperature, and outlet temperature is 70 ~ 100 DEG C, and atomizing pressure is 0.2 ~ 0.5MPa
Under conditions of be spray-dried, obtain Flos micheliae Albae essential oil microcapsules.
The preparation method of a kind of Flos micheliae Albae essential oil microcapsules the most according to claim 1, it is characterised in that described emulsifying
Agent is tween 20.
Flos micheliae Albae essential oil microcapsules prepared by method the most according to claim 1 or claim 2 application in Nicotiana tabacum L., its feature exists
In, Flos micheliae Albae essential oil microcapsules distilled water diluting 800 ~ 1000 times, dilute solution with the 2 ~ 3% of filter tip weight join volume
In cigarette filter tip, filter tip cigarette is become cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610306679.6A CN106040118A (en) | 2016-05-11 | 2016-05-11 | A preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610306679.6A CN106040118A (en) | 2016-05-11 | 2016-05-11 | A preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco |
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| Publication Number | Publication Date |
|---|---|
| CN106040118A true CN106040118A (en) | 2016-10-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610306679.6A Pending CN106040118A (en) | 2016-05-11 | 2016-05-11 | A preparing method of a white michelia essence oil microcapsule and applications of the microcapsule in tobacco |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107969730A (en) * | 2017-11-23 | 2018-05-01 | 北京亚美方舟科贸有限公司 | A kind of preparation method of tobacco aromaticss microcapsules |
| CN108244693A (en) * | 2016-12-29 | 2018-07-06 | 广州华芳烟用香精有限公司 | A kind of preparation method of cloud and mist extract powder fragrance and its application in cigarette |
| CN114081204A (en) * | 2021-11-26 | 2022-02-25 | 福建中烟工业有限责任公司 | Cinnamyl alcohol microcapsule and preparation method thereof, tobacco granules and preparation method thereof, filter stick or filter tip, tobacco product and application |
| CN114989889A (en) * | 2022-05-18 | 2022-09-02 | 广东本研新材料科技有限公司 | Preparation method of plant essential oil microspheres |
| CN116622445A (en) * | 2023-07-24 | 2023-08-22 | 内蒙古昆明卷烟有限责任公司 | Preparation method, composition and application of oncidium essential oil |
-
2016
- 2016-05-11 CN CN201610306679.6A patent/CN106040118A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108244693A (en) * | 2016-12-29 | 2018-07-06 | 广州华芳烟用香精有限公司 | A kind of preparation method of cloud and mist extract powder fragrance and its application in cigarette |
| CN107969730A (en) * | 2017-11-23 | 2018-05-01 | 北京亚美方舟科贸有限公司 | A kind of preparation method of tobacco aromaticss microcapsules |
| CN107969730B (en) * | 2017-11-23 | 2020-04-14 | 北京亚美方舟科贸有限公司 | Preparation method of tobacco flavor microcapsule |
| CN114081204A (en) * | 2021-11-26 | 2022-02-25 | 福建中烟工业有限责任公司 | Cinnamyl alcohol microcapsule and preparation method thereof, tobacco granules and preparation method thereof, filter stick or filter tip, tobacco product and application |
| CN114989889A (en) * | 2022-05-18 | 2022-09-02 | 广东本研新材料科技有限公司 | Preparation method of plant essential oil microspheres |
| CN116622445A (en) * | 2023-07-24 | 2023-08-22 | 内蒙古昆明卷烟有限责任公司 | Preparation method, composition and application of oncidium essential oil |
| CN116622445B (en) * | 2023-07-24 | 2023-10-27 | 内蒙古昆明卷烟有限责任公司 | Preparation method, composition and application of oncidium essential oil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161026 |