CN105919899A - Hair re-growing nourishing dew and preparation method thereof - Google Patents
Hair re-growing nourishing dew and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention relates to hair re-growing nourishing dew. Effective components are extracted from a mixed material consisting of flos humuli lupuli, mulberry, radix polygoni multiflora, coleus forskohlii briq, saffron and cortex moutan according to reasonable ratios, and glycerol, butanediol, bis-hydroxymethyl imidazolidinyl urea and essence components are added; the prepared hair re-growing nourishing dew contains a herbaceous plant extracting solution and multiple nutrient substances essential for the growth of hairs and medicinal effect components for moistening hairs, thereby repairing damaged hair follicles, supplementing specific nutrition for the hairs, nourishing the hairs, improving the scalp environment, preventing and treating hair loss, and relieving the conditions of withering and yellowing of the hairs, no glossiness, easiness in folding and hair breaking, and the like; in addition, the hair re-growing nourishing dew has the advantages of easily-obtained raw materials, low cost and remarkable treatment effect; furthermore, according to a method disclosed by the invention, the los humuli lupuli, the mulberry, the radix polygoni multiflora, the coleus forskohlii briq, the saffron and the cortex moutan are mixed according to the reasonable ratios to obtain the mixed material, and the effective components are extracted from the mixed material according to a specific method. The method has the advantages that the steps are simple and easily-operated and the effective components of the raw materials are low in loss.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to one and set out again nourishing dew and preparation method thereof.
Background technology
" hair is glossy, without dandruff " is classified as important in man's new concept of health one by World Health Organization (WHO),
And dense hair is a glamour man indispensability.But the problems such as alopecia, dandruff, the whitest, root of hair is fragile
It it is the most common hair problem of male.
Alopecia is the phenomenon of alopecia, have physiological and pathologic point.Physiologic alopecia refers to that hair is just
Normal comes off；Pathologic alopecia refers to hair exception or excessive coming off, and its reason is a lot.According to an investigation
Display, the youngster of 60% is perplexed by alopecia, particularly male personage.This swashs mainly due to competition
Immense pressure in the too fast rhythm of life of strong living environment, frequency, working and learning, easily makes human psychological
Anxiety, anxious state of mind, mental distress, additionally, such as smoke, drink, the bad life such as online all night is practised
Used, cause the sickness rate of alopecia in males more and more higher.
Alopecia not only looks and is old for one's age, and also can reduce the confidence that male participates in social activity.But, current city
Although having a lot for the treatment of or the product of prevention alopecia on field, but its effect inconspicuous.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides one can the effective impaired hair of maintenance
The nourishing dew and preparation method thereof that sets out again of capsule, prevention and hair growth.Nourishing of setting out again of the present invention
Dew, includes herbaceous plant extracting solution and multiple hair growth desired nutritional material and composition and effectiveness, repairing
Impaired hair follicle, supplements specific nutrition for hair, improves scalp environment.
The technical solution adopted in the present invention is:
One is set out and is nourished dew, and raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 0.5～3 weight portions；
Fructus Mori, 0.5～3 weight portions；
Radix Polygoni Multiflori, 0.5～3 weight portions；
Coleus forskohlii Briq., 0.5～3 weight portions；
Stigma Croci, 0.5～3 weight portions；
Cortex Moutan, 0.5～3 weight portions.
The raw material components that nourishing of setting out again described in Jin Yibuyouxuan is revealed includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 2 weight portions；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 1 weight portion；
Cortex Moutan, 1 weight portion.
The described raw material components setting out nourishing dew more also includes glycerol 1～5 weight portion, butanediol 1～5 weight
Part, double hydroxy methylimidazole ureine 0.1～0.8 weight portion and essence 0.01～0.1 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to described weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution；
(5) ethanol adding 1～4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate；
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, i.e.
Set out described in get nourishing dew again.
Set out again described in Jin Yibuyouxuan and nourish the preparation method of dew, comprise the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to described weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution；
(5) ethanol adding 1～4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate；
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine mixed liquor；Glycerol, butanediol, double hydroxy methylimidazole alkane it is sequentially added in described Chinese medicine mixed liquor
Base urea, essence, obtain described in again set out nourishing dew.
In step (2), the mass ratio of described compound and described deionized water is 1:6～1:9, described in boil and carry
Carrying out for normal pressure, temperature is 95～100 DEG C, and extraction time is 0.5～3h.
In step (3), the mass ratio of described first medicinal residues and described deionized water is 1:6～1:9, described in boil
Carrying and carrying out for normal pressure, temperature is 95～100 DEG C, and extraction time is 0.5～3h.
Step (4) is carried out described first time heating concentrating under reduced pressure temperature be 63～68 DEG C, pressure be-0.04～
-0.07MPa, described concentrated solution is 1:2～1:4 with the mass ratio of described stock solution.
Described in step (5), the volumetric concentration of ethanol is 60～80%, carry out time of described sedimentation be 12～
36h。
Step (6) is carried out described second time heating concentrating under reduced pressure temperature be 40～50 DEG C, pressure be-0.04～
-0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2～5h.
For the ease of understanding the present invention, below the raw material in the present invention and drug effect are further elaborated.
Flos lupuli (Flos Humuli Lupuli): perennial herb trailing plant, antibacterial and sedation, it is used for treating leprosy, treatment
Pulmonary tuberculosis, treatment pneumosilicosis, treatment tuberculous lymphadenitis, treatment dysentery.Invigorating the stomach and promoting digestion, diuresis is calmed the nerves.Control and disappear
Change bad, abdominal distention, edema, cystitis, pulmonary tuberculosis, insomnia.
Fructus Mori, sweet in the mouth, acid, cold in nature.Enrich blood YIN nourishing, effect moisturized of promoting the production of body fluid.For treating dizziness ear
Ring, palpitation and insomnia, early whitening of beard and hair, Tianjin wound is thirsty, and interior-heat is quenched one's thirst, blood deficiency and constipation.
Radix Polygoni Multiflori: bitter in the mouth, sweet, puckery, warm in nature.There are tonifying liver, kidney tonifying, nourish blood, the effect dispeled the wind.For
Treatment hepatic and renal YIN deficiency, sending out must be the whitest, and blood deficiency is dizzy, and waist knee joint is weak, and muscles and bones is ached, seminal emission, metrorrhagia and leukorrhagia, for a long time
Malaria, chronic dysentery, chronic hepatitis, carbuncle, scrofula, hemorrhoidal hamorrhage, haemorrhoids.
Coleus forskohlii Briq., Labiatae, herbaceos perennial.It is grown in all over the world as ornamental plant.
The extract of Coleus forskohlii Briq. is not this Kelin, and its effect can reduce blood pressure, and suppresses anaphylactic reaction,
And thyroxinic secretion can be promoted.Not other effects of this Kelin are notable equally, including suppression as by
Inflammation that platelet activating factor (PAF) 6 causes and the diffusion of anticancer.
Stigma Croci, sweet in the mouth, property is put down.There is blood circulation promoting and blood stasis dispelling, effect of dispersing stagnation and relieving accumulation of pathogens.For treating troubled thoughts pent-up,
Chest and diaphragm painful abdominal mass is vexed, spits blood, and typhoid fever is gone mad, frightened fear in a trance, women's amenorrhea, and postnatal blood stasis is suffered from abdominal pain, tumbling and swelling.
Cortex Moutan, bitter, pungent, it is slightly cold.There is clearing away heat and cooling blood, effect of blood circulation promoting and blood stasis dispelling.Send out for treating temperature poison
Speckle, hematemesis and epistaxis, night fever abating at dawn, lossless hectic fever due to YIN-deficiency, amenorrhea dysmenorrhea, carbuncle sore tumefacting virus, falls and flutters the pain of injury.
The invention have the benefit that
1, the nourishing dew that sets out again of the present invention, by from Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, hair larynx sheath stamen
Extracting active component in the compound that flower, Stigma Croci, Cortex Moutan form according to rational proportion, prepared goes out again
Send out nourishing dew and include herbaceous plant extracting solution and multiple hair growth desired nutritional material and hair care drug effect group
Point, the impaired hair follicle of repairing, supplements specific nutrition for hair, nourishes hair, improve scalp environment, it is possible to
Prevention and hair growth, improve withered and yellowish hairs, tarnish, the problem such as easy to break, easily broken；And raw material is easy
, low cost, therapeutic effect is obvious.
2, the nourishing dew that sets out again of the present invention, by by Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, hair larynx sheath stamen
Flower, Stigma Croci, Cortex Moutan carry out being mixed to prepare compound according to rational proportion, then according to spy from compound
Fixed method extracts active component, is finally also added with glycerol, butanediol, double hydroxy methylimidazole ureine, perfume (or spice)
Essence, the prepared nourishing dew that sets out again includes herbaceous plant extracting solution and multiple hair growth desired nutritional material
With hair care composition and effectiveness, and can use as conventional shampoo, the impaired hair follicle of repairing, supplementary for hair
Specific nutrition, nourish hair, improve scalp environment, it is possible to prevention and hair growth, improve withered and yellowish hairs,
The problem such as matt, easy to break, easily broken.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further elaborated.
Following example represent 1g with 1 weight portion.
Embodiment 1
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 0.5 weight portion；
Fructus Mori, 3 weight portions；
Radix Polygoni Multiflori, 0.5 weight portion；
Coleus forskohlii Briq., 3 weight portions；
Stigma Croci, 0.5 weight portion；
Cortex Moutan, 3 weight portions.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3h, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3h, obtain the second medicinal liquid and the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution exists
63-68 DEG C ,-0.04～-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is
The 1/2 of described stock solution quality；
(5) in step (4) described concentrated solution, add 1 times of volume ethanol (volumetric concentration is 60%) to enter
Row sedimentation 12h, carries out after having settled filtering and collecting filtrate；
(6) at 40-50 DEG C ,-0.04～-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 5h, is evaporated off whole ethanol, obtain described in again set out nourishing dew.
Embodiment 2
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 0.5 weight portion；
Fructus Mori, 3 weight portions；
Radix Polygoni Multiflori, 0.5 weight portion；
Coleus forskohlii Briq., 3 weight portions；
Stigma Croci, 0.5 weight portion；
Cortex Moutan, 3 weight portions；
Glycerol, 5 weight portions；
Butanediol, 1 weight portion；
Double hydroxy methylimidazole ureines, 0.8 weight portion；
Essence, 0.01 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution exists
63-68 DEG C ,-0.04～-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is
The 1/4 of described stock solution quality；
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 80%) of 4 times of volumes
Carry out settling 36h, carry out after having settled filtering and collecting filtrate；
(6) at 40-50 DEG C ,-0.04～-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 2h, is evaporated off whole ethanol, obtains Chinese medicine mixed liquor；It is sequentially added in described Chinese medicine mixed liquor
Glycerol, butanediol, double hydroxy methylimidazole ureine, essence, mix homogeneously, obtain the nourishing dew that sets out again.
Embodiment 3
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 2 weight portions；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 1 weight portion；
Cortex Moutan, 1 weight portion；
Glycerol, 1 weight portion；
Butanediol, 5 weight portions；
Double hydroxy methylimidazole ureines, 0.1 weight portion；
Essence, 0.1 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution exists
63-68 DEG C ,-0.04～-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is
The 1/3 of described stock solution quality；
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate；
(6) at 40-50 DEG C ,-0.04～-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine mixed liquor；In described Chinese medicine mixed liquor under agitation
It is sequentially added into glycerol, butanediol, double hydroxy methylimidazole ureine, essence, mix homogeneously, obtains and set out again
Nourish dew.
Embodiment 4
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 1 weight portion；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 2 weight portions；
Cortex Moutan, 1 weight portion；
Glycerol, 2 weight portions；
Butanediol, 3 weight portions；
Double hydroxy methylimidazole ureines, 0.5 weight portion；
Essence, 0.05 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3 hours, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution exists
63-68 DEG C ,-0.04～-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is
The 1/2 of described stock solution quality；
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes
Carry out settling 36h, carry out after having settled filtering and collecting filtrate；
(6) at 40-50 DEG C ,-0.04～-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine mixed liquor；In described Chinese medicine mixed liquor under agitation
It is sequentially added into glycerol, butanediol, double hydroxy methylimidazole ureine, essence, mix homogeneously, obtains and set out again
Nourish dew.
Embodiment 5
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 2 weight portions；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 1 weight portion；
Cortex Moutan, 1 weight portion；
Glycerol, 3 weight portions；
Butanediol, 3 weight portions；
Double hydroxy methylimidazole ureines, 0.4 weight portion；
Essence, 0.04 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 2h and obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 2h, obtain the second medicinal liquid and the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution exists
63-68 DEG C ,-0.04～-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is
The 1/2 of described stock solution quality；
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 65%) of 2 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate；
(6) at 40-50 DEG C ,-0.04～-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine mixed liquor；In described Chinese medicine mixed liquor under agitation
It is sequentially added into glycerol, butanediol, double hydroxy methylimidazole ureine, essence, mix homogeneously, obtains and set out again
Nourish dew.
Embodiment 6
The present embodiment provides one to set out again and nourishes dew, and its raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 2 weight portions；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 1 weight portion；
Cortex Moutan, 1 weight portion；
Glycerol, 4 weight portions；
Butanediol, 4 weight portions；
Double hydroxy methylimidazole ureines, 0.6 weight portion；
Essence, 0.06 weight portion.
A kind of method preparing the described nourishing dew that sets out again, comprises the steps:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to above-mentioned weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95～100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues；
(4) stock solution, described stock solution warp are obtained after described first medicinal liquid and the second medicinal liquid being sufficiently mixed
63-68 DEG C ,-0.04～-0.07MPa heating are concentrated under reduced pressure to give concentrated solution, and described concentrated solution is described stock solution matter
The 1/2 of amount；
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 75%) of 2.5 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate；
(6) step (5) described filtrate is carried out heating decompression at 40-50 DEG C ,-0.04～-0.07MPa dense
Contracting 3h, is evaporated off whole ethanol, obtains described Chinese medicine mixed liquor；Under agitation depend in described Chinese medicine mixed liquor
Secondary addition glycerol, butanediol, double hydroxy methylimidazole ureine, essence, mix homogeneously, obtain taste of setting out again
Support dew.
Experimental example
By of the present invention again set out nourishing dew be applied to 100 examples exist alopecia, withered and yellowish hairs, tarnish,
The patient of the symptom such as easy to break, easily broken, the maleest 53 examples, female 47 example, minimum 28 years old of age, maximum
65 years old.
Using method: smear scalp especially alopecia relatively many places, each 8ml every day for twice.
Efficacy assessment standard:
Cure: alopecia, withered and yellowish hairs, tarnish, the symptom such as easy to break, easily broken are wholly absent, 72 examples.
Effective: alopecia, withered and yellowish hairs, tarnish, the symptom such as easy to break, easily broken are obviously improved, 24 examples.
Invalid: alopecia, withered and yellowish hairs, tarnish, the symptom such as easy to break, easily broken are all not improved 4 examples.
Total effective rate 96%.
Typical clinical case:
Zhang, female, 32 years old, hair was sparse withered and yellow, and alopecia when washing hair of combing one's hair is a lot of, uses the present invention to implement
After nourishing of setting out again described in example 3 is revealed 40, alopecia phenomenon is obviously improved, after adhering to using 80,
The most no longer alopecia, color development blackening, glossy.
Wang, female, 39 years old, withered and yellowish hairs, tarnish, alopecia was more, uses the embodiment of the present invention 4 institute
After the nourishing of setting out again stated is revealed 40, color development blackening, depilation phenomenon is obviously improved, after adhering to using 70,
The most no longer alopecia, color development and glossiness all have clear improvement.
Liu, female, 28 years old, hair was matt, easy to break, easily broken, used described in the embodiment of the present invention 5
Set out again nourishing dew 50 days after, hair is pitch-black shinny.
The present invention is not limited to above-mentioned preferred forms, and anyone can draw it under the enlightenment of the present invention
His various forms of products, no matter but in its shape or structure, make any change, every have and the application
Technical scheme as same or like, within all falling within protection scope of the present invention.
Claims (10)
1. the nourishing dew that sets out again, it is characterised in that raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 0.5～3 weight portions；
Fructus Mori, 0.5～3 weight portions；
Radix Polygoni Multiflori, 0.5～3 weight portions；
Coleus forskohlii Briq., 0.5～3 weight portions；
Stigma Croci, 0.5～3 weight portions；
Cortex Moutan, 0.5～3 weight portions.
The nourishing dew that sets out again the most according to claim 1, it is characterised in that raw material components includes:
Flos lupuli (Flos Humuli Lupuli), 1 weight portion；
Fructus Mori, 2 weight portions；
Radix Polygoni Multiflori, 2 weight portions；
Coleus forskohlii Briq., 2 weight portions；
Stigma Croci, 1 weight portion；
Cortex Moutan, 1 weight portion.
The nourishing dew that sets out again the most according to claim 1 and 2, it is characterised in that raw material components also wraps
Include glycerol 1～5 weight portion, butanediol 1～5 weight portion, double hydroxy methylimidazole ureine 0.1～0.8 weight
Part and essence 0.01～0.1 weight portion.
4. one kind prepare described in claim 1 set out again nourish dew method, it is characterised in that include as
Lower step:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to described weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution；
(5) ethanol adding 1～4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate；
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, i.e.
Set out described in get nourishing dew again.
5. one kind prepare described in claim 3 set out again nourish dew method, it is characterised in that include as
Lower step:
(1) Flos lupuli (Flos Humuli Lupuli), Fructus Mori, Radix Polygoni Multiflori, Coleus forskohlii Briq., safranine are weighed successively according to described weight portion
Flower, Cortex Moutan are also sufficiently mixed, and obtain compound；
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues；
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues；
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution；
(5) ethanol adding 1～4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate；
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine mixed liquor；Glycerol, butanediol, double hydroxy methylimidazole alkane it is sequentially added in described Chinese medicine mixed liquor
Base urea, essence, obtain described in again set out nourishing dew.
6. according to the method nourishing dew of setting out again described in claim 4 or 5, it is characterised in that step (2)
In, the mass ratio of described compound and described deionized water is 1:6～1:9, described in boil to carry and carry out for normal pressure,
Temperature is 95～100 DEG C, and extraction time is 0.5～3h.
7. according to the method nourishing dew of setting out again described in claim 4 or 5, it is characterised in that step (3)
In, the mass ratio of described first medicinal residues and described deionized water is 1:6～1:9, described in boil to carry and carry out for normal pressure,
Temperature is 95～100 DEG C, and extraction time is 0.5～3h.
8. according to the method nourishing dew of setting out again described in claim 4 or 5, it is characterised in that step (4)
In carry out described first time heating concentrating under reduced pressure temperature be 63～68 DEG C, pressure is-0.04～-0.07MPa,
Described concentrated solution is 1:2～1:4 with the mass ratio of described stock solution.
9. according to the method nourishing dew of setting out again described in claim 4 or 5, it is characterised in that step (5)
Described in the volumetric concentration of ethanol be 60～80%, the time carrying out described sedimentation is 12～36h.
10. according to the method nourishing dew of setting out again described in claim 4 or 5, it is characterised in that step
(6) carry out in described second time heating concentrating under reduced pressure temperature be 40～50 DEG C, pressure be-0.04～
-0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2～5h.
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| CN201610482648.6A CN105919899A (en) | 2016-06-27 | 2016-06-27 | Hair re-growing nourishing dew and preparation method thereof |
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| CN106333916A (en) * | 2016-09-09 | 2017-01-18 | 拉芳家化股份有限公司 | Scalp nourishing liquid for treating alopecia and promoting hair growth |
| CN107334894A (en) * | 2016-12-14 | 2017-11-10 | 北京福纳康生物技术有限公司 | A kind of composition for treating alopecia seborrheica |
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Application publication date: 20160907 |