CN105623335A - Medical bactericidal paint and preparation method thereof - Google Patents
Medical bactericidal paint and preparation method thereof Download PDFInfo
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- CN105623335A CN105623335A CN201610106293.0A CN201610106293A CN105623335A CN 105623335 A CN105623335 A CN 105623335A CN 201610106293 A CN201610106293 A CN 201610106293A CN 105623335 A CN105623335 A CN 105623335A
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- titanium dioxide
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- fergusonite
- polystyrene
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
Abstract
The invention discloses medical bactericidal paint and a preparation method thereof.The medical bactericidal paint is prepared from epoxy resin, fergusonite powder, ethyl acrylate, polystyrene, calcium carbonate, polypropylene, barium sulfate, titanium dioxide and talcum powder.The paint is excellent in bactericidal performance and suitable for coating protection of medical materials; the viscosity is 15-35 s, the adhesive force is level 1-3, and the flexibility is 1-2 mm; the paint is free of toxicity and good in thixotropic performance, the surface drying time is 2-6 h, the hard drying time is 20-24 h, and the 45-degree luster rate is 85%-95%; the water resistance does not change within 2-6 days, the Shore hardness is 30-50, the tensile strength is 15-35 MPa, and the elastic elongation ratio is 500%-600%.The preparation method is simple, and the raw materials are simple and easy to obtain.
Description
Technical field
The present invention relates to medical material tech field, particularly relate to a kind of Medical sterilization coating and preparation method thereof.
Background technology
Fungicidal Latex Coatings is possible to prevent the coating of fungus growth. It is based on emulsion paint, lacquer, ethenoid resin paint, oil paint., in the room temperature dry property coating of urea formaldehyde coating, phthalic resin coating etc., add a small amount of biocide and maybe can suppress the anti-of fungus growth--the coating that agent coordinates. After paint solidification film forming; antifungus agent can slowly be exuded to film and prevent mycete generation for a long time; thus protecting coated article once not used oleic acid phenyl not etc. by mould erosion, antifungus agent made by organic mercury salt, and the nontoxic or hypotoxicity antifungus agent adopted before having disabled mouth because of the harmful drought of Liu Renti mainly has; The organo-tin compounds such as double; two two J mono-base stannum oxide, two fourth bun tin dilaurate stannum, tributyl-tin fumarate, tributyltin chlorides, the organocopper compounds such as copper naphthenate, pentachlorophenol copper .H-base beautiful jade copper. tetrachloro isophthalonitrile, to organochlorine compounds such as chlorine Resorcinos, two, two, four, pentachlorophenol, adjacent benzene China phenol, the phenolic compounds such as penta sodium pentachlorophenate, the inorganic salts such as based compound barium metaborate, zinc oxide, copper sulfate, sodium fluoride, Plumbum preparatium. This type of coating is mainly used in the building wall of fermentation plant, food factory, hospital, humid area, or for communication device, computer, electric equipment products etc.
Coating, is called paint in Chinese tradition name. So-called coating is to be coated in protected or decorated body surface; and the continuous film of firm attachment can be formed with coated article, it is common that based on resin or oil or emulsion, add or without pigment, filler; add corresponding additive, with the formulated thick liquid of organic solvent or water. China's more authoritative " coating process " book of coating circle is defined such that " coating is a kind of material, and this material can be coated in object surface by different construction technologies, is formed and adheres to firmly, has some strength, continuous print solid film. The film common name film so formed, also known as paint film or coating. "
Coating (paint), our usually described paint is one therein. Refer to coat body surface to form thin film under certain conditions and play protection, the class I liquid I of decoration or other specific functions (insulation, antirust, mildew-resistant, heat-resisting etc.) or solid material. Because the coating of early stage is mostly with vegetable oil for primary raw material, therefore also referred to as paint. Present synthetic resin instead of vegetable oil, therefore is called coating. Coating non-liquid, powdery paints is the big class of coating variety one.
Coating belongs to organic chemical industry's macromolecular material, and the film formed belongs to macromolecular compound type. According to the classification of the chemical products that the modern times pass through, coating belongs to fine chemical product. Modern coating is progressively becoming a polyfunctional engineering material of class, is an important industry in chemical industry.
Effect mainly has 4 points: protection, decoration, covers up defect and other special roles of product, the value of improving product. Founding of New is over 60 years, along with the development of national economy every profession and trade, progressively develops into the requisite important industry of all fields of national economy as its supporting coatings industry from an extremely unobtrusive little industry. Through the struggling hard of several generations, pioneering and keeping forging ahead, China has become second-biggest-in-the-world coating material production state and country of consumption, enters into the main flow of world's coating industry development.
Summary of the invention
The present invention provides a kind of nontoxic, Medical sterilization coating that bactericidal property is good, vapour permeability is good and preparation method thereof, solves existing medical material and covers with paint, lacquer, colour wash, etc. the technical problem such as protective coating bactericidal properties and thixotropy difference.
The present invention is by the following technical solutions: a kind of Medical sterilization coating, it is as follows that mass fraction proportioning pressed by its raw material: epoxy resin 100 parts, fergusonite powder 15-35 part, ethyl acrylate 5-25 part, polystyrene 55-75 part, calcium carbonate 40-60 part, polypropylene 50-70 part, barium sulfate 20-40 part, titanium dioxide 10-30 part, titanium dioxide 5-25 part, Pulvis Talci 1-5 part.
As a preferred technical solution of the present invention: it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, fergusonite powder 20-30 part, ethyl acrylate 10-20 part, polystyrene 60-70 part, calcium carbonate 45-55 part, polypropylene 55-65 part, barium sulfate 25-35 part, titanium dioxide 15-25 part, titanium dioxide 10-20 part, Pulvis Talci 2-4 part.
As a preferred technical solution of the present invention: it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, 20 parts of fergusonite powder, ethyl acrylate 10 parts, polystyrene 60 parts, carbonic acid Ca45 part, polypropylene 55 parts, 25 parts of barium sulfate, titanium dioxide 15 parts, titanium dioxide 10 parts, Pulvis Talci 2 parts.
As a preferred technical solution of the present invention: it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, 30 parts of fergusonite powder, ethyl acrylate 20 parts, polystyrene 70 parts, calcium carbonate 55 parts, polypropylene 65 parts, 35 parts of barium sulfate, titanium dioxide 25 parts, titanium dioxide 20 parts, Pulvis Talci 4 parts.
As a preferred technical solution of the present invention: it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, 25 parts of fergusonite powder, ethyl acrylate 15 parts, polystyrene 65 parts, calcium carbonate 50 parts, polypropylene 60 parts, 30 parts of barium sulfate, titanium dioxide 20 parts, titanium dioxide 15 parts, Pulvis Talci 3 parts.
A kind of method preparing described Medical sterilization coating, step is:
The first step: weigh epoxy resin, fergusonite powder, ethyl acrylate, polystyrene, calcium carbonate, polypropylene, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci according to mass fraction proportioning;
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 20-40min with 300-500r/min speed;
3rd step: the liquid after stirring is stood 24-28h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 30-50min, pack after filtration after mix homogeneously.
Beneficial effect
A kind of Medical sterilization coating of the present invention and preparation method thereof adopts above technical scheme compared with prior art, have following technical effect that 1, product bactericidal property excellent, it is adaptable to the covering with paint protection of medical material, viscosity 15-35s, adhesive force 1-3 level, pliability 1-2mm; 2, product is nontoxic, and thixotropic property is good, and surface drying time 2-6h does solid work 20-24h, 45 �� of gloss 85-95%; 3, resistance to water 2-6d is unchanged, Shore hardness 30-50, tensile strength 15-35MPa, elastic extension 500-600%, and preparation method is simple, and raw material is simple and easy to get, it is possible to current material is replaced in the widespread production not division of history into periods.
Detailed description of the invention
Below in conjunction with example, the invention will be further described, and embodiment only for the present invention will be described, is not intended that the restriction to right, and other alternative means that it may occur to persons skilled in the art that, all within the scope of the claims in the present invention.
Embodiment 1:
The first step: weigh epoxy resin 100 parts, 15 parts of fergusonite powder, ethyl acrylate 5 parts, polystyrene 55 parts, calcium carbonate 40 parts, polypropylene 50 parts, 20 parts of barium sulfate, titanium dioxide 10 parts, titanium dioxide 5 parts, Pulvis Talci 1 part according to mass fraction proportioning.
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 20min with 300r/min speed.
3rd step: the liquid after stirring is stood 24h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 30min, pack after filtration after mix homogeneously.
Product bactericidal property is excellent, it is adaptable to the covering with paint protection of medical material, viscosity 15s, adhesive force 3 grades, pliability 1mm; Product is nontoxic, and thixotropic property is good, and surface drying time 6h does solid work 24h, 45 �� of gloss 85%; Resistance to water 2d is unchanged, Shore hardness 30, tensile strength 15MPa, elastic extension 500%, and preparation method is simple, and raw material is simple and easy to get.
Embodiment 2:
The first step: weigh epoxy resin 100 parts, 35 parts of fergusonite powder, ethyl acrylate 25 parts, polystyrene 75 parts, calcium carbonate 60 parts, polypropylene 70 parts, 40 parts of barium sulfate, titanium dioxide 30 parts, titanium dioxide 25 parts, Pulvis Talci 5 parts according to mass fraction proportioning.
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 40min with 500r/min speed.
3rd step: the liquid after stirring is stood 28h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 50min, pack after filtration after mix homogeneously.
Product bactericidal property is excellent, it is adaptable to the covering with paint protection of medical material, viscosity 20s, adhesive force 3 grades, pliability 2mm; Product is nontoxic, and thixotropic property is good, and surface drying time 5h does solid work 23h, 45 �� of gloss 88%; Resistance to water 3d is unchanged, Shore hardness 35, tensile strength 20MPa, elastic extension 520%, and preparation method is simple, and raw material is simple and easy to get.
Embodiment 3:
The first step: weigh epoxy resin 100 parts, 20 parts of fergusonite powder, ethyl acrylate 10 parts, polystyrene 60 parts, carbonic acid Ca45 part, polypropylene 55 parts, 25 parts of barium sulfate, titanium dioxide 15 parts, titanium dioxide 10 parts, Pulvis Talci 2 parts according to mass fraction proportioning.
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 20min with 300r/min speed.
3rd step: the liquid after stirring is stood 24h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 30min, pack after filtration after mix homogeneously.
Product bactericidal property is excellent, it is adaptable to the covering with paint protection of medical material, viscosity 25s, adhesive force 2 grades, pliability 1mm; Product is nontoxic, and thixotropic property is good, and surface drying time 4h does solid work 22h, 45 �� of gloss 90%; Resistance to water 4d is unchanged, Shore hardness 40, tensile strength 25MPa, elastic extension 550%, and preparation method is simple, and raw material is simple and easy to get.
Embodiment 4:
The first step: weigh epoxy resin 100 parts, 30 parts of fergusonite powder, ethyl acrylate 20 parts, polystyrene 70 parts, calcium carbonate 55 parts, polypropylene 65 parts, 35 parts of barium sulfate, titanium dioxide 25 parts, titanium dioxide 20 parts, Pulvis Talci 4 parts according to mass fraction proportioning.
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 40min with 500r/min speed.
3rd step: the liquid after stirring is stood 28h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 50min, pack after filtration after mix homogeneously.
Product bactericidal property is excellent, it is adaptable to the covering with paint protection of medical material, viscosity 30s, adhesion 1 grade, pliability 1mm; Product is nontoxic, and thixotropic property is good, and surface drying time 3h does solid work 21h, 45 �� of gloss 93%; Resistance to water 5d is unchanged, Shore hardness 45, tensile strength 30MPa, elastic extension 580%, and preparation method is simple, and raw material is simple and easy to get.
Embodiment 5:
The first step: weigh epoxy resin 100 parts, 25 parts of fergusonite powder, ethyl acrylate 15 parts, polystyrene 65 parts, calcium carbonate 50 parts, polypropylene 60 parts, 30 parts of barium sulfate, titanium dioxide 20 parts, titanium dioxide 15 parts, Pulvis Talci 3 parts according to mass fraction proportioning.
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 30min with 400r/min speed.
3rd step: the liquid after stirring is stood 26h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 40min, pack after filtration after mix homogeneously.
Product bactericidal property is excellent, it is adaptable to the covering with paint protection of medical material, viscosity 35s, adhesion 1 grade, pliability 2mm; Product is nontoxic, and thixotropic property is good, and surface drying time 2h does solid work 20h, 45 �� of gloss 95%; Resistance to water 6d is unchanged, Shore hardness 50, tensile strength 35MPa, elastic extension 600%, and preparation method is simple, and raw material is simple and easy to get.
Claims (6)
1. a Medical sterilization coating, it is characterized in that, it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, fergusonite powder 15-35 part, ethyl acrylate 5-25 part, polystyrene 55-75 part, calcium carbonate 40-60 part, polypropylene 50-70 part, barium sulfate 20-40 part, titanium dioxide 10-30 part, titanium dioxide 5-25 part, Pulvis Talci 1-5 part.
2. a kind of Medical sterilization coating according to claim 1, it is characterized in that, it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, fergusonite powder 20-30 part, ethyl acrylate 10-20 part, polystyrene 60-70 part, calcium carbonate 45-55 part, polypropylene 55-65 part, barium sulfate 25-35 part, titanium dioxide 15-25 part, titanium dioxide 10-20 part, Pulvis Talci 2-4 part.
3. a kind of Medical sterilization coating according to claim 1, it is characterized in that, it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, 20 parts of fergusonite powder, ethyl acrylate 10 parts, polystyrene 60 parts, carbonic acid Ca45 part, polypropylene 55 parts, 25 parts of barium sulfate, titanium dioxide 15 parts, titanium dioxide 10 parts, Pulvis Talci 2 parts.
4. a kind of Medical sterilization coating according to claim 1, it is characterized in that, it is as follows that mass fraction proportioning pressed by the raw material of described Medical sterilization coating: epoxy resin 100 parts, 30 parts of fergusonite powder, ethyl acrylate 20 parts, polystyrene 70 parts, calcium carbonate 55 parts, polypropylene 65 parts, 35 parts of barium sulfate, titanium dioxide 25 parts, titanium dioxide 20 parts, Pulvis Talci 4 parts.
5. a kind of Medical sterilization coating according to claim 1, it is characterized in that: the raw material of described Medical sterilization coating is as follows by mass fraction proportioning: epoxy resin 100 parts, 25 parts of fergusonite powder, ethyl acrylate 15 parts, polystyrene 65 parts, calcium carbonate 50 parts, polypropylene 60 parts, 30 parts of barium sulfate, titanium dioxide 20 parts, titanium dioxide 15 parts, Pulvis Talci 3 parts.
6. the method for the Medical sterilization coating that one kind makes described in claim 1, it is characterised in that comprise the steps:
The first step: weigh epoxy resin, fergusonite powder, ethyl acrylate, polystyrene, calcium carbonate, polypropylene, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci according to mass fraction proportioning;
Second step: fergusonite powder, epoxy resin, ethyl acrylate, polystyrene and polypropylene are put in the reactor with agitator and thermometer, stir 20-40min with 300-500r/min speed;
3rd step: the liquid after stirring is stood 24-28h, adds calcium carbonate, barium sulfate, titanium dioxide, titanium dioxide and Pulvis Talci, puts into grinder and grinds 30-50min, pack after filtration after mix homogeneously.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610106293.0A CN105623335A (en) | 2016-02-26 | 2016-02-26 | Medical bactericidal paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610106293.0A CN105623335A (en) | 2016-02-26 | 2016-02-26 | Medical bactericidal paint and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105623335A true CN105623335A (en) | 2016-06-01 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610106293.0A Withdrawn CN105623335A (en) | 2016-02-26 | 2016-02-26 | Medical bactericidal paint and preparation method thereof |
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| CN (1) | CN105623335A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107334282A (en) * | 2017-05-27 | 2017-11-10 | 太仓市康乐沙发家具厂 | Sterilizing shoe cabinet |
| CN114085591A (en) * | 2021-11-16 | 2022-02-25 | 湖南华菱线缆股份有限公司 | High-adhesion mildew-resistant coating for cables |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1693393A (en) * | 2005-05-18 | 2005-11-09 | 孟鋆辉 | Sterilizing type corrosion-proof epoxy powder coating |
| CN103143067A (en) * | 2013-02-21 | 2013-06-12 | 宁波保税区安杰脉德医疗器械有限公司 | Antimicrobial coat on surface of water system, and its preparation method |
| CN103159437A (en) * | 2011-12-15 | 2013-06-19 | 张国庆 | Temperature adjusting humidity adjusting coating and preparation method thereof |
-
2016
- 2016-02-26 CN CN201610106293.0A patent/CN105623335A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1693393A (en) * | 2005-05-18 | 2005-11-09 | 孟鋆辉 | Sterilizing type corrosion-proof epoxy powder coating |
| CN103159437A (en) * | 2011-12-15 | 2013-06-19 | 张国庆 | Temperature adjusting humidity adjusting coating and preparation method thereof |
| CN103143067A (en) * | 2013-02-21 | 2013-06-12 | 宁波保税区安杰脉德医疗器械有限公司 | Antimicrobial coat on surface of water system, and its preparation method |
Non-Patent Citations (1)
| Title |
|---|
| 宋小平: "《化工小商品生产法》", 30 September 1993, 湖南科学技术出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107334282A (en) * | 2017-05-27 | 2017-11-10 | 太仓市康乐沙发家具厂 | Sterilizing shoe cabinet |
| CN114085591A (en) * | 2021-11-16 | 2022-02-25 | 湖南华菱线缆股份有限公司 | High-adhesion mildew-resistant coating for cables |
| CN114085591B (en) * | 2021-11-16 | 2022-05-27 | 湖南华菱线缆股份有限公司 | High-adhesion mildew-resistant coating for cables |
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Application publication date: 20160601 |
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