CN105482135A - 一种纳米微晶纤维素改性土豆淀粉醋酸酯食品保鲜膜的制备方法 - Google Patents
一种纳米微晶纤维素改性土豆淀粉醋酸酯食品保鲜膜的制备方法 Download PDFInfo
- Publication number
- CN105482135A CN105482135A CN201510877335.6A CN201510877335A CN105482135A CN 105482135 A CN105482135 A CN 105482135A CN 201510877335 A CN201510877335 A CN 201510877335A CN 105482135 A CN105482135 A CN 105482135A
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- Prior art keywords
- potato starch
- bath
- stirring
- mentioned
- microcrystalline cellulose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920001592 potato starch Polymers 0.000 title claims abstract description 28
- MKRNVBXERAPZOP-UHFFFAOYSA-N Starch acetate Chemical compound O1C(CO)C(OC)C(O)C(O)C1OCC1C(OC2C(C(O)C(OC)C(CO)O2)OC(C)=O)C(O)C(O)C(OC2C(OC(C)C(O)C2O)CO)O1 MKRNVBXERAPZOP-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 229920000168 Microcrystalline cellulose Polymers 0.000 title claims abstract description 11
- 235000019813 microcrystalline cellulose Nutrition 0.000 title claims abstract description 11
- 239000008108 microcrystalline cellulose Substances 0.000 title claims abstract description 11
- 229940016286 microcrystalline cellulose Drugs 0.000 title claims abstract description 11
- 239000005452 food preservative Substances 0.000 title abstract description 7
- 235000019249 food preservative Nutrition 0.000 title abstract description 6
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000001035 drying Methods 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 8
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 54
- 238000003756 stirring Methods 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
- 235000010980 cellulose Nutrition 0.000 claims description 27
- 239000001913 cellulose Substances 0.000 claims description 27
- 229920002678 cellulose Polymers 0.000 claims description 27
- 239000013081 microcrystal Substances 0.000 claims description 27
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 24
- 235000013305 food Nutrition 0.000 claims description 23
- 239000012528 membrane Substances 0.000 claims description 22
- 239000011521 glass Substances 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 18
- 230000004048 modification Effects 0.000 claims description 15
- 238000012986 modification Methods 0.000 claims description 15
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- 229960000583 acetic acid Drugs 0.000 claims description 12
- 239000012530 fluid Substances 0.000 claims description 12
- 239000012362 glacial acetic acid Substances 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 230000010355 oscillation Effects 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000001117 sulphuric acid Substances 0.000 claims description 12
- 235000011149 sulphuric acid Nutrition 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 7
- 230000001186 cumulative effect Effects 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 238000003760 magnetic stirring Methods 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 229920002472 Starch Polymers 0.000 abstract description 17
- 239000008107 starch Substances 0.000 abstract description 17
- 235000019698 starch Nutrition 0.000 abstract description 17
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract description 12
- 239000000463 material Substances 0.000 abstract description 4
- 230000015556 catabolic process Effects 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000010345 tape casting Methods 0.000 abstract 1
- 241000220225 Malus Species 0.000 description 16
- 239000003755 preservative agent Substances 0.000 description 13
- 230000002335 preservative effect Effects 0.000 description 13
- 230000006378 damage Effects 0.000 description 6
- 235000021016 apples Nutrition 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 238000005520 cutting process Methods 0.000 description 4
- 231100000252 nontoxic Toxicity 0.000 description 4
- 230000003000 nontoxic effect Effects 0.000 description 4
- -1 polyethylene Polymers 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 238000003754 machining Methods 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 239000006057 Non-nutritive feed additive Substances 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000019439 ethyl acetate Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 235000021404 traditional food Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/18—Manufacture of films or sheets
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/04—Starch derivatives, e.g. crosslinked derivatives
- C08L3/06—Esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2303/00—Characterised by the use of starch, amylose or amylopectin or of their derivatives or degradation products
- C08J2303/04—Starch derivatives
- C08J2303/06—Esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2401/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2401/02—Cellulose; Modified cellulose
- C08J2401/04—Oxycellulose; Hydrocellulose
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/16—Applications used for films
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510877335.6A CN105482135B (zh) | 2015-12-03 | 2015-12-03 | 一种纳米微晶纤维素改性土豆淀粉醋酸酯食品保鲜膜的制备方法 |
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CN201510877335.6A CN105482135B (zh) | 2015-12-03 | 2015-12-03 | 一种纳米微晶纤维素改性土豆淀粉醋酸酯食品保鲜膜的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN105482135A true CN105482135A (zh) | 2016-04-13 |
CN105482135B CN105482135B (zh) | 2018-05-04 |
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CN201510877335.6A Active CN105482135B (zh) | 2015-12-03 | 2015-12-03 | 一种纳米微晶纤维素改性土豆淀粉醋酸酯食品保鲜膜的制备方法 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107691638A (zh) * | 2017-10-31 | 2018-02-16 | 广西浙缘农业科技有限公司 | 一种青枣的保存方法 |
CN111320774A (zh) * | 2020-04-17 | 2020-06-23 | 武汉轻工大学 | 一种淀粉复合膜的制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103421215A (zh) * | 2013-08-20 | 2013-12-04 | 华东理工大学 | 淀粉组合物、淀粉基薄膜及其制备方法 |
CN103965519A (zh) * | 2014-05-16 | 2014-08-06 | 齐鲁工业大学 | 一种再生纤维素增强淀粉薄膜的制备方法 |
CN104130431A (zh) * | 2014-07-06 | 2014-11-05 | 东北林业大学 | 一种壳聚糖-糠醛渣纳米纤维素复合膜的制备方法 |
-
2015
- 2015-12-03 CN CN201510877335.6A patent/CN105482135B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103421215A (zh) * | 2013-08-20 | 2013-12-04 | 华东理工大学 | 淀粉组合物、淀粉基薄膜及其制备方法 |
CN103965519A (zh) * | 2014-05-16 | 2014-08-06 | 齐鲁工业大学 | 一种再生纤维素增强淀粉薄膜的制备方法 |
CN104130431A (zh) * | 2014-07-06 | 2014-11-05 | 东北林业大学 | 一种壳聚糖-糠醛渣纳米纤维素复合膜的制备方法 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107691638A (zh) * | 2017-10-31 | 2018-02-16 | 广西浙缘农业科技有限公司 | 一种青枣的保存方法 |
CN111320774A (zh) * | 2020-04-17 | 2020-06-23 | 武汉轻工大学 | 一种淀粉复合膜的制备方法 |
Also Published As
Publication number | Publication date |
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CN105482135B (zh) | 2018-05-04 |
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C06 | Publication | ||
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SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Sun Shihai Inventor before: Gao Dayuan Inventor before: Lin Dawei Inventor before: Zhang Fan |
|
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20180328 Address after: Guo Meng Zhen Jiangsu province 224014 Yancheng City District double new road No. 13 Applicant after: JIANGSU HONGGUIFANG INDUSTRIAL CO., LTD. Address before: 213164 Jiangsu province Changzhou New District Xinli Garden Building 5 room 1202, unit B Applicant before: Gao Dayuan |
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