CN105400345B - Computer color-mixed exterior wall is flat to apply basic shallow foundation paint and preparation method thereof - Google Patents
Computer color-mixed exterior wall is flat to apply basic shallow foundation paint and preparation method thereof Download PDFInfo
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Abstract
It is formulated the present invention relates to the wall finiss described in a kind of economical net mould proof wall finiss of taste by following components：Water, cellulose, pH adjusting agent, dispersant, wetting agent, wetting antifreezing agent, defoamer, titanium dioxide, filler, emulsion, Opacifying polymers, coalescents, sterilization antiseptic, mould inhibitor, thickener, waterproofing agent of organosilicon.The present invention has advantages below：Abrasion resistance, water resistance, alkali resistance, have excellent weather resistance；Compatibility and color developing with the popular mill base of in the market is very excellent, accurate and favorable reproducibility of mixing colours；And smooth smooth, froth breaking is exceedingly fast, anti-splashing is excellent during construction, paint film richness high；The preparation method simple and fast and production process are easy to management and control, manufacturing cost is low and different batches between stability it is good, the color recalled is accurately and reliably；Storage stability is good；The film of the present invention is not in bubbling, come off, the paint marketing such as rainprint, speck.
Description
Technical field
The present invention relates to architectural decoration water paint field, more particularly to a kind of computer color-mixed exterior wall is flat to apply basic shallow foundation
Paint and preparation method thereof.
Background technology
As aesthetic standards are lifted, requirement of the consumer to building coating color also becomes more diverse and personalized, therefore passes
The coating material production of system, artificial toning process can not meet consumer demand.The introducing of tinting system is modernized, factory only needs
Three kinds of base paints of production (being respectively shallow foundation, middle base, deep base), dealer only needs to basic mill base, it becomes possible to rapidly recall into
Million colors on thousand, to meet the personalization and variation selection of different clients, so as to improve the market competitiveness.
Computer color-mixed base paint quality at present on the market is uneven, and main deficiency has：One is, some computer color-mixed bases
Plinth paint does not distinguish inner-outer wall, generally without specific aim, i.e., the different performance demand not according to interior wall paint and exterior wall paint is come
Reasonable design basis paint；Two are, the poor compatibility of base paint and the popular mill base of in the market, color developing is bad, is also easy to produce loose colour, hair
The phenomenons such as flower；Three are, base paint production process is difficult management and control, and the base paint difference of different batches production is larger, causes what is recalled
Color is not accurate enough；Four are, the flat performance (such as abrasion resistance, water resistance, alkali resistance, weatherability) for applying base paint of exterior wall itself
It is not good, it is impossible to meet the performance requirement of high-performance coatings with high weatherability.
The content of the invention
The invention provides basic shallow foundation paint of the flat painting of a kind of computer color-mixed exterior wall and preparation method thereof, the prepared base of the present invention
Abrasion resistance, water resistance, alkali resistance, weatherability of plinth paint etc. are all very prominent, and with the compatibility of the popular mill base of in the market
It is very excellent with color developing；The preparation method simple and fast and production process are easy to management and control, manufacturing cost is low and different batches between
Stability is good, and the color recalled is accurately and reliably.
What the present invention was realized in：
Scheme (one)：
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the paint is matched according to following parts by weight by following components and prepared
Form：
| Water | 9.77-25.2 part |
| Cellulose | 0.2-0.6 parts |
| PH adjusting agent | 0.05-0.25 parts |
| Dispersant | 0.5-1 parts |
| Wetting agent | 0.1-0.4 parts |
| Antifreezing agent | 0.8-1.5 parts |
| Soak antifreezing agent | 0-0.4 parts |
| Defoamer | 0.4-0.8 parts |
| Titanium dioxide | 12-20 parts |
| Filler | 22-35 parts |
| Emulsion | 20-30 parts |
| Opacifying polymers | 3-6 parts |
| Coalescents | 1-2 parts |
| Sterilization antiseptic | 0.1-0.3 parts |
| Mould inhibitor | 0.2-0.4 parts |
| Thickener | 0.1-0.5 parts |
| Waterproofing agent of organosilicon | 0.5-3 parts |
It is preferred that, the pH adjusting agent be 2-amino-2-methyl-1-propanol, the antifreezing agent be ethylene glycol or propane diols,
The Opacifying polymers are the microspheric aqueous emulsion polymer with core/shell structure of not film forming.
It is preferred that, the dispersant be ammonium polyacrylate dipersant or one kind in polycarboxylate sodium's dispersant or they
Any combination.
It is preferred that, the wetting agent is poly- hydroxy alkyl ether nonionic wetting agent.
It is preferred that, the defoamer be mineral oil defoaming agent or one kind in water-based organic silicon defoamer or they
Any combination.
It is preferred that, the filler is one kind in powdered whiting, calcined kaolin, barium sulfate, talcum powder and mica powder
Or their any combination.
It is preferred that, the waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer.
It is preferred that, the coalescents be alcohol ester-12, dipropylene glycol methyl ether or dipropylene in one kind or they
Any combination.
It is preferred that, the thickener is a kind of or their times in alkali swelling type thickener or polyurethanes thickener
Meaning combination.
Scheme (two)：
One kind prepares the flat method for applying basic shallow foundation paint of computer color-mixed exterior wall described in scheme (one), and this method includes following
The step of sequentially carrying out：
1) under 500-800 revs/min of rotating speed, 9.77-25.2 parts of water are sequentially added in a reservoir and 0.2-0.6 parts fine
Dimension element, keeps the rotating speed scattered 5-10 minutes；
2) then improve rotating speed to 800-1200 revs/min, add 0.05-0.25 part pH adjusting agents, 0.5-1 parts it is scattered
Agent, 0.1-0.4 parts of wetting agents, 0.8-1.5 parts of antifreezing agents, 0-0.4 parts of wetting antifreezing agents, 0.2-0.4 parts of defoamers, 12-20 parts
Titanium dioxide, 22-35 part filler；
Then rotating speed is improved afterwards to 1500-1800 revs/min, and fineness is dispersed under the rotating speed more than zero and is less than or waits
In 60 microns；
3) finally, reduction rotating speed to 600-800 revs/min, sequentially added under the rotating speed 20-30 parts of emulsions, 3-6 parts not
Transparent polymer, 0.2-0.4 part defoamer, 1-2 parts of coalescents, 0.1-0.3 parts of sterilization antiseptics, 0.2-0.4 parts of mould inhibitors,
0.1-0.5 parts of thickeners and 0.5-3 parts of waterproofing agent of organosilicon, disperse 10-15 minutes under the rotating speed.
The present invention has advantages below compared with prior art：
(1) present invention is with strong points, and specially the performance requirement according to needed for exterior wall paint carries out formula design, prepared base
The properties (such as abrasion resistance, water resistance, alkali resistance, weatherability) of plinth paint are very excellent；
(2) by preferred thickened systems, wetting and dispersing system, antifoaming system etc., the present invention not only with the market popular colour
The compatibility and color developing of slurry are very excellent, accurate and favorable reproducibility of mixing colours；And smooth smooth, froth breaking is exceedingly fast, resisted during construction
Splashing is excellent, paint film richness high.
(3) the preparation method simple and fast and production process are easy to management and control, manufacturing cost is low and different batches between stability
Good, the color recalled is accurately and reliably.
(4) storage stability is good, and after 50 DEG C of thermmal storages 60 days, the viscosity B coefficent of base paint is no more than 5KU, and and mill base
The properties such as compatibility, color developing do not influenceed by thermmal storage.
(5) waterproofing agent of organosilicon is added, film of the invention has outstanding water resistance, water resistance at initial stage and resistance to rain at initial stage
Trace, the paint marketing such as even if being rained after construction in 24h, film of the invention is also not in bubbling, come off, rainprint, speck.
Embodiment
With reference to specific embodiment, the present invention will be described in detail.
(1) embodiment is as follows：
Embodiment one：
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the paint is matched according to following parts by weight by following components and prepared
Form：
| Water | 9.77-25.2 part |
| Cellulose | 0.2-0.6 parts |
| PH adjusting agent | 0.05-0.25 parts |
| Dispersant | 0.5-1 parts |
| Wetting agent | 0.1-0.4 parts |
| Antifreezing agent | 0.8-1.5 parts |
| Soak antifreezing agent | 0-0.4 parts |
| Defoamer | 0.4-0.8 parts |
| Titanium dioxide | 12-20 parts |
| Filler | 22-35 parts |
| Emulsion | 20-30 parts |
| Opacifying polymers | 3-6 parts |
| Coalescents | 1-2 parts |
| Sterilization antiseptic | 0.1-0.3 parts |
| Mould inhibitor | 0.2-0.4 parts |
| Thickener | 0.1-0.5 parts |
| Waterproofing agent of organosilicon | 0.5-3 parts |
It is preferred that, the pH adjusting agent be 2-amino-2-methyl-1-propanol, the antifreezing agent be ethylene glycol or propane diols,
The Opacifying polymers are Tao Shi Unihub E.
It is preferred that, the dispersant be ammonium polyacrylate dipersant or one kind in polycarboxylate sodium's dispersant or they
Any combination.
It is preferred that, the wetting agent is poly- hydroxy alkyl ether nonionic wetting agent.
It is preferred that, the defoamer be mineral oil defoaming agent or one kind in water-based organic silicon defoamer or they
Any combination.
It is preferred that, the filler is one kind in powdered whiting, calcined kaolin, barium sulfate, talcum powder and mica powder
Or their any combination.
It is preferred that, the waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer.
It is preferred that, the coalescents be alcohol ester-12, dipropylene glycol methyl ether or dipropylene in one kind or they
Any combination.
It is preferred that, the thickener is a kind of or their times in alkali swelling type thickener or polyurethanes thickener
Meaning combination.
Embodiment two：
One kind prepares the flat method for applying basic shallow foundation paint of computer color-mixed exterior wall described in scheme (one), and this method includes following
The step of sequentially carrying out：
1) under 500-800 revs/min of rotating speed, 9.77-25.2 parts of water are sequentially added in a reservoir and 0.2-0.6 parts fine
Dimension element, keeps the rotating speed scattered 5-10 minutes；
2) then improve rotating speed to 800-1200 revs/min, add 0.05-0.25 part pH adjusting agents, 0.5-1 parts it is scattered
Agent, 0.1-0.4 parts of wetting agents, 0.8-1.5 parts of antifreezing agents, 0-0.4 parts of wetting antifreezing agents, 0.2-0.4 parts of defoamers, 12-20 parts
Titanium dioxide, 22-35 part filler；
Then rotating speed is improved afterwards to 1500-1800 revs/min, and fineness is dispersed under the rotating speed more than zero and is less than or waits
In 60 microns；
3) finally, reduction rotating speed to 600-800 revs/min, sequentially added under the rotating speed 20-30 parts of emulsions, 3-6 parts not
Transparent polymer, 0.2-0.4 part defoamer, 1-2 parts of coalescents, 0.1-0.3 parts of sterilization antiseptics, 0.2-0.4 parts of mould inhibitors,
0.1-0.5 parts of thickeners and 0.5-3 parts of waterproofing agent of organosilicon, disperse 10-15 minutes under the rotating speed.
(2) embodiment is as follows：The present invention is further illustrated below by embodiment：
Embodiment 1
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the raw material that it is matched by following weight is sequentially carried out according to following
The step of be prepared from：
1) 22.4 parts of water and 0.2 part of cellulose are sequentially added under 500 revs/min of rotating speed, 5 points are disperseed under the rotating speed
Clock；
2) be subsequently added under 800 revs/min of rotating speed 0.25 part of pH adjusting agent, 0.5 part of dispersant, 0.1 part of wetting agent,
1.2 parts of antifreezing agents, 0.4 part of wetting antifreezing agent, 0.325 part of defoamer, 20 parts of titanium dioxides, 18 parts of powdered whitings and 4 parts of micas
Powder, improves rotating speed to 1500 revs/min, fineness is dispersed under the rotating speed less than or equal to 60 microns afterwards；
3) reduction rotating speed is to 600 revs/min, sequentially added under the rotating speed 25 parts of emulsions, 3 parts of Opacifying polymers,
0.325 part of defoamer, 1.5 parts of coalescents, 0.1 part of sterilization antiseptic, 0.2 part of mould inhibitor, 0.5 part of thickener and 2 parts are organic
Silicon waterproofing agent, disperses 15 minutes to well mixed under the rotating speed.
Embodiment 2
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the raw material that it is matched by following weight is sequentially carried out according to following
The step of be prepared from：
1) 9.77 parts of water and 0.35 part of cellulose are sequentially added under 800 revs/min of rotating speed, 10 are disperseed under the rotating speed
Minute；
2) be subsequently added under 1200 revs/min of rotating speed 0.15 part of pH adjusting agent, 1 part of dispersant, 0.4 part of wetting agent,
1.5 parts of antifreezing agents, 0 part of wetting antifreezing agent, 0.4 part of defoamer, 12 parts of titanium dioxides, 30 parts of powdered whitings and 5 parts of calcining kaolinites
Soil, improves rotating speed to 1800 revs/min, fineness is dispersed under the rotating speed less than or equal to 60 microns afterwards；
3) reduction rotating speed sequentially adds 30 parts of emulsions, 6 parts of Opacifying polymers, 0.4 to 800 revs/min under the rotating speed
Part defoamer, 2 parts of coalescents, 0.18 part of sterilization antiseptic, 0.25 part of mould inhibitor, 0.1 part of thickener and 0.5 part of organosilicon are prevented
Aqua, disperses 10 minutes to well mixed under the rotating speed.
Embodiment 3
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the raw material that it is matched by following weight is sequentially carried out according to following
The step of be prepared from：
1) 25.2 parts of water and 0.45 part of cellulose are sequentially added under 650 revs/min of rotating speed, 7 are disperseed under the rotating speed
Minute；
2) be subsequently added under 1000 revs/min of rotating speed 0.1 part of pH adjusting agent, 0.7 part of dispersant, 0.2 part of wetting agent,
0.8 part of antifreezing agent, 0.25 part of wetting antifreezing agent, 0.2 part of defoamer, 17 parts of titanium dioxides, 23 parts of powdered whitings and 3 parts of talcums
Powder, improves rotating speed to 1600 revs/min, fineness is dispersed under the rotating speed less than or equal to 60 microns afterwards；
3) reduction rotating speed sequentially adds 20 parts of emulsions, 4 parts of Opacifying polymers, 0.2 to 700 revs/min under the rotating speed
Part defoamer, 1 part of coalescents, 0.25 part of sterilization antiseptic, 0.3 part of mould inhibitor, 0.35 part of thickener and 3 parts of organic silicon water-proofings
Agent, disperses 12 minutes to well mixed under the rotating speed.
Embodiment 4
A kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, and the raw material that it is matched by following weight is sequentially carried out according to following
The step of be prepared from：
1) 18.2 parts of water and 0.6 part of cellulose are sequentially added under 700 revs/min of rotating speed, 9 points are disperseed under the rotating speed
Clock；
2) 0.05 part of pH adjusting agent, 0.8 part of dispersant, 0.3 part of wetting are subsequently added under 1100 revs/min of rotating speed
Agent, 1 part of antifreezing agent, 0.15 part of wetting antifreezing agent, 0.275 part of defoamer, 15 parts of titanium dioxides, 25 parts of powdered whitings and 5 parts
Talcum powder, improves rotating speed to 1700 revs/min, fineness is dispersed under the rotating speed less than or equal to 60 microns afterwards；
3) reduction rotating speed is to 750 revs/min, sequentially added under the rotating speed 25 parts of emulsions, 5 parts of Opacifying polymers,
0.275 part of defoamer, 1.5 parts of coalescents, 0.3 part of sterilization antiseptic, 0.4 part of mould inhibitor, 0.15 part of thickener and 1 part are organic
Silicon waterproofing agent, disperses 13 minutes to well mixed under the rotating speed.
In various embodiments above：
Cellulose is preferred to use the sub- 250HBR across dragon production；
PH adjusting agent is preferred to use the AMP-95 of Tao Shi productions；
Dispersant is preferred to use the SN-5040 of Sheng Nuopuke productions；
Wetting agent is preferred to use the SN-WET 996 of Sheng Nuopuke productions；
Wetting antifreezing agent is preferred to use the FT-68 of ashland production；
Antifreezing agent is preferred to use the propane diols of Depew Chemical Manufacture；
Defoamer is preferred to use the NXZ of Hai Chuan productions and the CF18404 of Blackburn production；
Titanium dioxide is preferred to use the 902+ of Du Pont's production；
Powdered whiting is preferred to use the 800 mesh coarse whitings of agriculture-countryside-farmer；
Calcined kaolin is preferred to use the ultra-fine high white calcined kaolin for covering west production；
Mica powder is preferred to use the ultrafine mica powder of US business's chemistry；
Talcum powder is preferred to use the MS-1250 of wide good fortune production；
Emulsion is preferred to use 6266 pure-acrylic emulsions of BASF production；
Opacifying polymers are preferred to use the Unihub E of Tao Shi productions；
Coalescents are preferred to use the texanol of Yi Shiman productions；
Sterilization antiseptic is preferred to use the HF of Sol production；
Mould inhibitor is preferred to use the EPW of Sol production；
Thickener is preferred to use the RM-8W of TT935 and the Tao Shi production of ROHM AND HAAS production.
Waterproofing agent of organosilicon is preferred to use the WR 1195 of sea profit chemical industry.
Enter according to the national standard GB/T 9755-2014 basis shallow foundation paints that apply flat to the computer color-mixed exterior wall obtained by each embodiment
Row test, every technical performance data are as shown in the table：
The flat color developing and the following table of colour killing force data for applying basic shallow foundation paint of computer color-mixed exterior wall obtained by each embodiment
It is shown：
Shown by the every experimental data and the practical application of each embodiment in table, in the present invention prepared by each embodiment
The flat properties for applying basic shallow foundation paint of computer color-mixed exterior wall meet GB/T 9755-2014《The outer Wall of synthetic resin emulsion is applied
Material》The technical requirements of the high-class product of middle exterior wall paint, and it is very excellent with the compatibility and color developing of the popular mill base of in the market,
Toning is accurate and favorable reproducibility；The preparation method simple and fast and production process are easy to management and control, and manufacturing cost is low and different batches
Between stability it is good, the color recalled is accurately and reliably.
Simply technical scheme is explained in detail for above-mentioned embodiment, the present invention not only only office
It is limited to above-described embodiment, every any improvement or replacement according to the principle of the invention all should be within protection scope of the present invention.
Claims (4)
1. a kind of computer color-mixed exterior wall is flat to apply basic shallow foundation paint, it is characterised in that：The paint is by following components according to following parts by weight
Number proportioning is formulated：
The waterproofing agent of organosilicon is the water-based emulsion of siloxane polymer；
The Opacifying polymers are the microspheric aqueous emulsion polymer with core/shell structure of not film forming；
The dispersant is ammonium polyacrylate dipersant or one kind or their any combination in polycarboxylate sodium's dispersant；
The wetting agent is poly- hydroxy alkyl ether nonionic wetting agent；
The defoamer is a kind of or their any combination in mineral oil defoaming agent or water-based organic silicon defoamer；
The filler is a kind of or their times in powdered whiting, calcined kaolin, barium sulfate, talcum powder or mica powder
Meaning combination；
The thickener is a kind of or their any combination in alkali swelling type thickener or polyurethanes thickener；
The emulsion uses 6266 pure-acrylic emulsions that BASF is produced.
2. computer color-mixed exterior wall according to claim 1 is flat to apply basic shallow foundation paint, it is characterised in that：The pH adjusting agent is
2-amino-2-methyl-1-propanol；The antifreezing agent is ethylene glycol or propane diols.
3. computer color-mixed exterior wall according to claim 1 is flat to apply basic shallow foundation paint, it is characterised in that：The coalescents are
One kind or their any combination in alcohol ester-12, dipropylene glycol methyl ether or dipropylene.
4. a kind of flat preparation method for applying basic shallow foundation paint of computer color-mixed exterior wall prepared any one of claim 1-3,
It is characterized in that：The preparation method of the paint includes following the step of sequentially carry out：
1) under 500-800 revs/min of rotating speed, 9.77-25.2 parts of water and 0.2-0.6 parts of fibers are sequentially added in a reservoir
Element, keeps the rotating speed scattered 5-10 minutes；
2) then improve rotating speed to 800-1200 revs/min, add 0.05-0.25 parts of pH adjusting agents, 0.5-1 parts of dispersants,
0.1-0.4 parts of wetting agents, 0.8-1.5 parts of antifreezing agents, 0-0.4 parts of wetting antifreezing agents, 0.2-0.4 parts of defoamers, 12-20 parts of titanium whites
Powder and 22-35 parts of fillers；
Then rotating speed is improved to 1500-1800 revs/min, fineness is dispersed under the rotating speed more than zero and micro- less than or equal to 60
Rice；
3) finally, reduction rotating speed is to 600-800 revs/min, sequentially add 20-30 parts of emulsions, 3-6 parts of Opacifying polymers,
0.2-0.4 parts of defoamers, 1-2 parts of coalescents, 0.1-0.3 parts of sterilization antiseptics, 0.2-0.4 parts of mould inhibitors, 0.1-0.5 parts of increasings
Thick dose and 0.5-3 parts of waterproofing agent of organosilicon, 600-800 revs/min of holding are scattered 10-15 minutes.
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|---|---|---|---|
| CN201510891527.2A CN105400345B (en) | 2015-12-07 | 2015-12-07 | Computer color-mixed exterior wall is flat to apply basic shallow foundation paint and preparation method thereof |
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| CN105400345B true CN105400345B (en) | 2017-08-25 |
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| CN106699007B (en) * | 2017-01-05 | 2019-01-29 | 辽宁意邦新型材料科技集团有限公司 | A kind of preparation method and lacquer obtained by this method of lacquer |
| CN114479585B (en) * | 2020-10-26 | 2023-02-10 | 立邦涂料（中国）有限公司 | Rain mark resistant high-color-retention high-polymer exterior wall coating and preparation method thereof |
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| JP2008121022A (en) * | 2000-09-20 | 2008-05-29 | Nippon Paint Co Ltd | Method for providing and obtaining color matched powder coating |
| CN101338164A (en) * | 2008-08-18 | 2009-01-07 | 中山市三和气雾有限公司 | Computer color-mixed base paint |
| CN101735702B (en) * | 2010-02-04 | 2014-12-10 | 安徽天锦云漆业有限公司 | External insulation elastic self-cleaning waterproof paint |
| CN102604500B (en) * | 2012-03-13 | 2016-01-20 | 三棵树涂料股份有限公司 | Phase transformation heat-insulation and heat-preservation interior wall coating and preparation method thereof |
| CN104745013A (en) * | 2015-03-30 | 2015-07-01 | 广西吉宽太阳能设备有限公司 | Heat-insulating coating for external wall |
| CN104962186B (en) * | 2015-07-02 | 2018-11-06 | 上海嘉宝莉涂料有限公司 | Energy conservation and environmental protection inner wall surface paint and preparation method thereof |
| CN105017905A (en) * | 2015-08-13 | 2015-11-04 | 董善刚 | High-weather-resistance nano-modified haze removal exterior wall coating |
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