CN105348874A - Colorized cement paint and preparation method thereof - Google Patents
Colorized cement paint and preparation method thereof Download PDFInfo
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- CN105348874A CN105348874A CN201510901397.6A CN201510901397A CN105348874A CN 105348874 A CN105348874 A CN 105348874A CN 201510901397 A CN201510901397 A CN 201510901397A CN 105348874 A CN105348874 A CN 105348874A
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Abstract
The invention discloses colorized cement paint and a preparation method thereof. The colorized cement paint is prepared from an aqueous agent and pigment, the aqueous agent is prepared from, by weight, 10%-80% of alkali metal silicate solution, 10%-80% of silica sol, 1%-15% of polyacrylate emulsifier solution, 1%-15% of colloid stabilizer, 0.1%-3% of thickener and 0.1%-3% of defoaming agent, and the pigment is prepared from, by weight, 1%-30% of glass powder, 1%-35% of silicon dioxide and minerals thereof, 1%-93% of metal powder, 1%-75% of metallic oxide, 1%-35% of metal hydroxide, 1%-6% of natural mineral pigment and 1%-60% of synthetic inorganic pigment. The colorized cement paint has alkaline, inorganic and water resistant characteristics, the film-forming property is good, the adhesive force is strong, and the colorized cement paint can be directly coated on a substrate.
Description
Technical field
The present invention relates to a kind of coating, particularly a kind of cement lithin paint.
The invention still further relates to the preparation method of above-mentioned cement lithin paint.
Background technology
Mankind's activity exacerbates environmental pollution, and the volatile organic compounds (VOC) that especially fossil energy and various manufacturing activity produce makes environmental stress increasingly severe.Reducing VOC content in air, reducing energy consumption is the day by day urgent problem of coating industry one, water-borne coatings, powder coating, photo-cured coating and high solid coating become the direction of following paint development as four large novel environment-friendly coating, and the environmental protection coating material of low temperature and even ambient cure is in the ascendant especially.
Cement, is often referred to silicate cement, and use water is solidifying agent, and can realize ambient cure.This illustrates that cement is a kind of environmental protection, energy-conservation environment-friendly material., although cement is a kind of widely used environment-friendly material, Portland cement is difficult to use as coated material.
First, cement color is more single, and owing to containing the impurity elements such as iron in raw material, after high temperature sintering, most cement is grey black, the color that very difficult imparting is enriched more.Want the cement obtaining various colors, i.e. " colored cement ", white cement can only be adopted to add the mode of pigment.A large amount of gypsum (calcium sulfate) composition is contained in white cement, and the gypsum raw material that to be a kind of water tolerance poor.Therefore, want the light cement obtaining water-tolerant, can only be produced by purer raw material, the cost of preparation is relatively high.
Secondly, even if by adopting the mode of high-purity raw to obtain light cement type, because ordinary Portland cement in use has strict demand to the consumption of solidifying agent water.Water cement ratio refers to the consumption of coagulation water in soil and the ratio of cement consumption.Water cement ratio affects the degree of compactness after concrete rheological property, grout coherent structure and its sclerosis, and thus when composition material is given, water cement ratio is the significant parameter determining concrete strength, weather resistance and other series of physical mechanical properties.Just have an optimum ratio to cement, the excessive or too small performances such as intensity that all can make are affected.And use as coating, just require good workability, add a large amount of water unavoidably, to improve its mobility.Add that cement slurry is large as coated material surface-area, moisture evaporation is fast, and the required normal moisture that thes cement solidifies also is difficult to ensure.These factors have a strong impact on strength of coating, limit the application of Portland cement as coating.
Further, itself be difficult in cement construction obtain thinner coating, add that cement shrinks in condensation cure process comparatively large, be easy to cracking, affect attachment and the intensity of coating, also unsightly.
Above various reasons, has had a strong impact on the use of cement as coated material.Be with coloured cement, i.e. " colored cement ", use mainly as engineering materials, such as lay color road, still difficult " colored cement " seen for coated material.
Summary of the invention
The present invention is to solve deficiency of the prior art, and provide a kind of alkaline, inorganic, water-fast and clean, good film-forming property, strong adhesion, can be applied directly to the cement lithin paint on ground.
The technical scheme of a kind of cement lithin paint of the present invention is:
A kind of cement lithin paint, comprise aqua and colorant, each component percentage of described aqua is respectively: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%; The each component percentage of described colorant is respectively: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%.
The technical scheme of a kind of cement lithin paint of the present invention can also be:
Described alkali metal silicate solutions is at least one in potassium silicate solution, lithium silicate solution and sodium silicate solution.
Described metal-powder is at least one in zinc powder and aluminium powder, and described natural mineral pigment is at least one in natural yellow earth, natural red soil and color sand.
A kind of cement lithin paint of the present invention, comprise aqua and colorant, each component percentage of described aqua is respectively: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%; The each component percentage of described colorant is respectively: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%.Like this, aqua adopts the alkali metal silicate solutions of widespread use, silicon sol is main raw, alkali metal silicate solutions possesses water-soluble, silicon sol is the dispersion liquid of nano level silica dioxide granule in water or in solvent, the content of organic compound is few, effectively can stop the growth of algae, fungi, mould etc., keep the long-acting cleaning of coating.Meanwhile, inorganic paint more can resist ultraviolet destruction, has more weather resistance than organic coating of the prior art (silicon third, pure third, styrene-acrylic coating etc.).And colorant is formulated by mineral compound, metal-powder, natural mineral pigment and synthetic pigment, all belongs to environmental friendliness raw material.By regulating each component percentages of colorant, the different application effect of coating can be obtained.Coating can extensively be coated on the grounds such as cement, brick, wall, metal and plastics, is even difficult to common water borne coating such as stainless steel, organic coating, plastics the material adhering to film forming, also has extraordinary sticking power.
Another object of the present invention there is provided a kind of alkaline, inorganic, water-fast, and good film-forming property, and strong adhesion, can be applied directly to the preparation method of the cement lithin paint on ground.
The technical scheme of the making method of a kind of cement lithin paint of the present invention is:
The preparation method of cement lithin paint, comprises the steps:
(1) aqua raw material prepares: each component is according to following weight percentage proportioning: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%;
(2) aqua batching: sequentially add the alkali metal silicate solutions in step (1), silicon sol, polyacrylic ester breast, deflocculant liquid, thickening material and thickening material in reactor, reaction is heated to 35-80 DEG C, and be incubated 2-12 hour, then form described aqua through overcooling, filtration;
(3) Pigment Material prepares: each component is according to following weight percentage proportioning: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%.
(4) colorant batching: the mineral compound in step (3), metal-powder, natural mineral pigment and synthetic pigment are worn into fine powder, then stirs with blender, mix, be packaged as described colorant;
(5) take the described aqua in step (2) and the described colorant in step (4) proportionally stirs, mix, obtain cement lithin paint.
In the preparation process of cement lithin paint mainly based on mechanical stirring, and Heating temperature is in proper range, without the need to carrying out in High Temperature High Pressure situation, and save energy, simple possible.In preparation process, without the generation of sewage and obnoxious flavour, safe and reliable, can mass-producing, industrialization, raw material availability is high.
The technical scheme of the making method of a kind of cement lithin paint of the present invention can also be: the described aqua in described step (5) and described colorant mix according to the ratio of 1:0.5 to 1:8.
The making method of a kind of cement lithin paint of the present invention, in preparation process mainly based on mechanical stirring, and Heating temperature is in proper range, without the need to carrying out in High Temperature High Pressure situation, save energy, simple possible.In preparation process, without the generation of sewage and obnoxious flavour, safe and reliable, can mass-producing, industrialization, raw material availability is high.
Embodiment
Below in conjunction with specific embodiment, a kind of cement lithin paint of the present invention and preparation method thereof is further described.
A kind of cement lithin paint, comprise aqua and colorant, each component percentage of described aqua is respectively: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%; The each component percentage of described colorant is respectively: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%.Like this, aqua adopts the alkali metal silicate solutions of widespread use, silicon sol is main raw, alkali metal silicate solutions possesses water-soluble, silicon sol is the dispersion liquid of nano level silica dioxide granule in water or in solvent, the content of organic compound is few, and solution is in comparatively strong basicity, effectively can stop the growth of algae, fungi and mould etc., keep the long-acting cleaning of coating.Meanwhile, the content of aqua organic compound is few, more can resist ultraviolet destruction, has more weather resistance than organic coating of the prior art (silicon third, pure third, styrene-acrylic coating etc.).Alkalimetal silicate and silicon sol and polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%, after overcuring, containing a large amount of high reactivity silicone hydroxyl (silanol base) in water-soluble macromolecule, not only can there is self condensation reaction in these silicone hydroxyl, also can with other inorganic materials such as base material, as concrete, glass, sandstone, quartz, metallic zinc, metallic aluminium, clay and the base material such as various mineral dye and filler, there is " petrochemical industry " reaction, and then form firm inorganic coating.Each component of colorant all belongs to environmental friendliness raw material.When after aqua and coloring material for mixing, petrochemical industry reaction can be there is each other in aqua and colorant, and mixed aqua and colorant define cement lithin paint, can and base material between there is petrochemical industry and react, further preferably, the cement lithin paint mixed was finished in 8 hours, or added a large amount of aqua continuation dilutions.Further, by regulating each component percentages of colorant, the different application effect of coating can be obtained.Such as, if only use metal-powder in colorant, such as zinc powder, coordinates the aqua being rich in lithium silicate or potassium silicate, then can obtain the inorganic zinc-rich protective system of dry film Zn content superelevation, can give steel long-lasting protection.For another example, colorant adopts a large amount of natural mineral pigment, as natural yellow earth or red soil, coordinate synthetic inorganic pigment, coordinate obtained cement lithin paint with aqua, the thickness of base material 2-5mm can be penetrated into, and with base material, " petrochemical industry " occurs and react, become firm inorganic coating.The colorant scope of cement lithin paint of the present invention is not limited only to zinc powder, natural yellow earth or red soil, other multiple inorganic mineral or mineral compound and mineral dye, all can with aqua generation wide application, form the inorganic coating of multicolour and purposes.Cement lithin paint of the present invention can extensively be coated on the grounds such as cement, brick, wall, metal and plastics, further, cement lithin paint of the present invention is even difficult to common water borne coating such as stainless steel, organic coating, plastics the material adhering to film forming, also has good sticking power.
On the basis of a kind of cement lithin paint technique scheme of the present invention, Ke Yishi: described alkali metal silicate solutions is at least one in potassium silicate solution, lithium silicate solution and sodium silicate solution.Wherein, potassium silicate solution, lithium silicate solution and sodium silicate solution are water-soluble silicate solution, and water-soluble silicate is mineral compound, are a kind of mineral tamanoris.And the modulus of potassium silicate solution, lithium silicate solution and sodium silicate solution is comparatively large, and silica content is more, the viscosity also thickness of solution, be easy to decompose sclerosis, cohesive force increases, and can be convenient to aqua and colorant and to react and shaping.
Further preferred technical scheme can be: described metal-powder is at least one in zinc powder and aluminium powder, and described natural mineral pigment is at least one in natural yellow earth, natural red soil and color sand.Like this, can the per-cent of natural mineral pigment be known by regulation and control metal-powder and be mixed with the coating of different color, effect and application.Such as: when in colorant, zinc powder accounts for larger per-cent, corrosion resistance coating can be obtained; And when natural yellow earth or red soil or color sand account for larger per-cent in colorant, the decorative paint of bright-colored environmental protection again can be obtained.Preferably, silicon-dioxide and mineral thereof are superfine quartz sand or mica powder, and metal oxide is high activity modified zinc oxide, and metal hydroxides is aluminium hydroxide.
On the basis of preparation method's technique scheme of a kind of cement lithin paint of the present invention, Ke Yishi: the preparation method of cement lithin paint, comprises the steps:
(1) aqua raw material prepares: each component is according to following weight percentage proportioning: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%;
(2) aqua batching: sequentially add the alkali metal silicate solutions in step (1), silicon sol, polyacrylic ester breast, deflocculant liquid, thickening material and thickening material in reactor, reaction is heated to 35-80 DEG C, and be incubated 2-12 hour, then form described aqua through overcooling, filtration;
(3) Pigment Material prepares: each component is according to following weight percentage proportioning: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural or synthetic mineral filler 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%;
(4) colorant batching: the mineral compound in step (3), metal-powder, natural mineral pigment and synthetic pigment are worn into fine powder, then stirs with blender, mix, be packaged as described colorant;
(5) take the described aqua in step (2) and the described colorant in step (4) proportionally stirs, mix, obtain cement lithin paint.
In the preparation process of cement lithin paint mainly based on mechanical stirring, and Heating temperature is in proper range, without the need to carrying out in High Temperature High Pressure situation, and save energy, simple possible.In preparation process, without the generation of sewage and obnoxious flavour, safe and reliable, can mass-producing, industrialization, raw material availability is high.
Preferred technical scheme can be further: the described aqua in described step (5) and described colorant mix according to the ratio of 1:0.5 to 1:8.Like this, according to the required blending ratio that can control or regulate aqua and colorant, with the cement lithin paint of obtained different color and performance.Preferably, the blending ratio of aqua and colorant is between 1:0.5 to 1:8, and the performance of the colored cement obtained is best, and also can add the pure water being no more than aqua 10% when colorant consumption is too much and dilute.
In the raw material of the cement lithin paint of specific embodiment of the invention scheme 1-3, component and weight percentage thereof see the following form:
In order to observe the practical function of the present invention's " cement lithin paint ", we prepare raw material according to the proportioning of embodiment 1-3 in above table, and are prepared into experimental group product 1-3 respectively according to the preparation method of described cement lithin paint.Meanwhile, the Portland cement 3 kinds set product 1-3 in contrast that on market, pattern is different is chosen.
We select acceptable substrate, such as: brick, wall, metal, plastics etc., and experimental group product and control group product are coated on respectively on base material respectively.After the curing reaction of 15 days, we can pass through water tolerance and the coating situation of observation and test experiments set product and control group product.
In embodiment 1, obtained cement lithin paint, relative to Portland cement, test result is as follows:
In embodiment 2, when colorant is by formula, and when zinc powder is ultra-fine pure zinc powder (800 order), adopt aqua/colorant=1:5, there is good corrosion resistance nature (base material is steel, and embodiment 2 is tested in ambient cure for 30 days afterwards):
| Test event | Embodiment 2 | Common zinc rich paint |
| Color | Dark grey | Dark grey |
| Thickness | 50u | 50u |
| Sticking power | Well | Well |
| Dry film Zn content (%) | 80％ | 80％ |
| Resistance to neutral salt spray performance (h) | 2000 | 2000 |
In embodiment 3, obtained cement lithin paint, relative to Portland cement, test result is as follows
Above-mentionedly only a kind of specific embodiment in the present invention to be illustrated, but can not as protection scope of the present invention, every equivalence change of making according to the design spirit in the present invention or modify, all should to think and fall into protection scope of the present invention.
Claims (5)
1. a cement lithin paint, it is characterized in that: comprise aqua and colorant, each component percentage of described aqua is respectively: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%; The each component percentage of described colorant is respectively: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%.
2. according to a kind of cement lithin paint described in claim 1, it is characterized in that: described alkali metal silicate solutions is at least one in potassium silicate solution, lithium silicate solution and sodium silicate solution.
3. according to a kind of cement lithin paint described in claim 1, it is characterized in that: described metal-powder is at least one in zinc powder and aluminium powder, and described natural mineral pigment is at least one in natural yellow earth, natural red soil and color sand.
4. the preparation method of cement lithin paint according to claim 1, is characterized in that comprising the steps:
(1) aqua raw material prepares: each component is according to following weight percentage proportioning: alkali metal silicate solutions 10-80%, silicon sol 10-80%, polyacrylate dispersion 1-15%, deflocculant 1-15%, thickening material 0.1-3% and defoamer 0.1-3%
(2) aqua batching: order adds alkali metal silicate solutions, silicon sol, polyacrylic ester breast, deflocculant and the thickening material in step (1) in reactor, reaction is heated to 35-80 DEG C, and be incubated 2-12 hour, then form described aqua through overcooling, filtration;
(3) Pigment Material prepares: each component is according to following weight percentage proportioning: glass powder 1-30%, silicon-dioxide and mineral 1-35% thereof, metal-powder 1-93%, metal oxide 1-75%, metal hydroxides 1-35%, natural mineral pigment 1-60% and synthetic inorganic pigment 1-60%;
(4) colorant batching: the raw material in step (3) is worn into fine powder, then stirs with blender, mix, be packaged as described colorant;
(5) take the described aqua in step (2) and the described colorant in step (4) proportionally, mix, obtain cement lithin paint.
5. the preparation method of cement lithin paint according to claim 4, is characterized in that: the described aqua in described step (5) and described colorant mix according to the ratio of 1:0.5 to 1:8.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108947452A (en) * | 2017-05-22 | 2018-12-07 | 四会市中日化工实业有限公司 | A kind of novel concrete coating |
| CN110527362A (en) * | 2019-09-09 | 2019-12-03 | 王学芳 | Chemically react colour system material, preparation method and coating material prepared therefrom |
| CN111116144A (en) * | 2020-01-03 | 2020-05-08 | 江苏西尔玛道路环保材料有限公司 | Colored polymer cement mortar coating and preparation method and application thereof |
| CN111647288A (en) * | 2020-04-13 | 2020-09-11 | 赵梓权 | Environment-friendly coating and preparation method thereof |
| CN112251058A (en) * | 2020-10-20 | 2021-01-22 | 深圳广田高科新材料有限公司 | Urban green road inorganic silicate coating and preparation method thereof |
| CN115044259A (en) * | 2022-05-27 | 2022-09-13 | 昆明璋润涂装工程有限公司 | Micro cement coating and construction method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115044259A (en) * | 2022-05-27 | 2022-09-13 | 昆明璋润涂装工程有限公司 | Micro cement coating and construction method thereof |
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| CN105348874B (en) | 2017-11-14 |
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