CN105326648B - A kind of whitening anti-wrinkling sleep mask with sheet microcapsules - Google Patents

A kind of whitening anti-wrinkling sleep mask with sheet microcapsules Download PDF

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Publication number
CN105326648B
CN105326648B CN201510858061.6A CN201510858061A CN105326648B CN 105326648 B CN105326648 B CN 105326648B CN 201510858061 A CN201510858061 A CN 201510858061A CN 105326648 B CN105326648 B CN 105326648B
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parts
mixed
microcapsules
sheet microcapsules
ppg
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CN201510858061.6A
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CN105326648A (en
Inventor
袁彦洁
卢颖
杜森垚
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Chongqing Xiaowan Biotechnology Co., Ltd.
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CHONGQING XIAOWAN TRADE Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11—Encapsulated compositions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A61K8/602—Glycosides, e.g. rutin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/733—Alginic acid; Salts thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The present invention discloses a kind of whitening anti-wrinkling sleep mask with sheet microcapsules, the facial mask in parts by weight, including following component：70 ~ 75 parts of water, 2 ~ 5 parts of glycerine, 5 ~ 10 parts of 17/6 copolymers of PEG/PPG, 8 ~ 12 parts of propane diols, 0.5 ~ 2 part of glycine betaine, 0.2 ~ 1 part of ammonium acryloyl taurate/VP copolymer, 0.2 ~ 1 part of Sodium Polyacrylate, 0.5 ~ 1 part of 1,2 ethohexadiol, 0.3 ~ 0.8 part of Phenoxyethanol, 0.01 ~ 0.05 part of 26 butylol polyether of PPG, 26,0.01 ~ 0.05 parts of 40 rilanit specials of PEG, 0.03 ~ 0.08 part of xanthans, 0.2 ~ 0.5 part of CI, 16035,0.01 ~ 0.03 parts of essence and 2 ~ 5 parts of sheet microcapsules.During using component of the present invention, the sheet microcapsules can be made to be softened in mask matrix of the present invention, it is easy to push away and smear out.

Description

A kind of whitening anti-wrinkling sleep mask with sheet microcapsules
Technical field
The invention belongs to microcapsules technology field, and in particular to a kind of whitening anti-wrinkling sleep surface containing sheet microcapsules Film.
Background technology
The active material of the external environments such as light, heat sensitivity will be embedded frequently with microcapsules technology, to extend activity During the effective active of material, these microcapsules for being embedded with active ingredient are added into after cosmetic base, it is not easy to quilt Chemical constituent in matrix is influenced, can stabilization is deposited in cosmetic base again into without being destroyed its specific activity .
But existing microcapsules cannot usually soften in cosmetic base, original hard quality is still kept, and then make Consumer is when using the cosmetics containing the microcapsules, it is impossible to easily pushes away microcapsules on the skin and smears out, causes on skin There is the microcapsules fragment of many hard, smear it is uneven, thus there are it is certain the problem of.
The content of the invention
For deficiencies of the prior art, the technical problems to be solved by the invention are：One kind how is provided to contain There is the whitening anti-wrinkling sleep mask of sheet microcapsules, the sheet microcapsules is obtained in whitening anti-wrinkling sleep mask soft Easily push away and smear out when changing, and then being smeared on the skin, will not make to occur pushing away on skin to smear non-uniform microcapsules fragment.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that：A kind of whitening with sheet microcapsules Crease-resistant sleep mask, in parts by weight, including following component：70 ~ 75 parts of water, 2 ~ 5 parts of glycerine, 5 ~ 10 parts of PEG/PPG-17/6 are total to Polymers, 8 ~ 12 parts of propane diols, 0.5 ~ 2 part of glycine betaine, 0.2 ~ 1 part of ammonium acryloyl taurate/VP copolymer, 0.2 ~ 1 part Sodium Polyacrylate, 0.5 ~ 1 part of 1,2- ethohexadiol, 0.3 ~ 0.8 part of Phenoxyethanol, 0.01 ~ 0.05 part of PPG-26- butylol polyether -26, 0.01 ~ 0.05 part of Cremophor RH40,0.03 ~ 0.08 part of xanthans, 0.2 ~ 0.5 part of CI, 16035,0.01 ~ 0.03 parts of perfume (or spice) Essence and 2 ~ 5 parts of sheet microcapsules；
The sheet microcapsules in parts by weight, including following component：55 parts of sodium alginates, 28 parts of agar, 6 parts of ethoxys Cellulose, 6 parts of Sodium Hyaluronates, 12 parts of glycerine, 2 parts of vitamin e acetates, 3 parts of rhodamine toner dew, 2 parts of ursin, 3 parts of tweens 20th, 0.2 part of red 30 color lake CI73360,0.2 part of titanium dioxide, 0.6 part of Phenoxyethanol, 0.3 part of Sensiva SC50 and 0.5 part 1, 2- ethohexadiols.
Compared with prior art, the present invention has the advantages that：
1st, the present invention is directed to the material character of used sheet microcapsules, is found by creative research, using this When inventing the component, by the interaction compatibility effect between each component, the sheet microcapsules can be made in mask matrix of the present invention In softened, and then be found through experiments that and the present invention be applied to skin with the whitening anti-wrinkling sleep masks of sheet microcapsules When upper, sheet microcapsules are easy to push away and smear out, and will not remain the fragment of microcapsules on the skin, have good spreading property.
2nd, the present invention makes the present invention carry the whitening anti-wrinkling of sheet microcapsules by the collaboration compatibility effect between each component Sleep mask can play consistently whitening and it is crease-resistant the effect of, will not make there is whitening and crease-resistant active ingredient in product It is interior destroyed during preservation, have good stability.
3rd, the present invention makes sheet microcapsules can be soft in mask matrix by the collaboration compatibility effect between each component Change, and will not too soften and cause microcapsule structure to destroy, capsule-core content leaks, there is good protection to make microcapsules With effectively extending the shelf life of product, there are good market prospects.
Embodiment
The present invention is described in further detail with reference to embodiment, in the present embodiment unless otherwise instructed, original used Material is commercially available.
Water and xanthans are uniformly mixed by whitening anti-wrinkling sleep mask of the present invention with sheet microcapsules, as water phase； By glycerine, PEG/PPG-17/6 copolymers, propane diols, glycine betaine, ammonium acryloyl taurate/VP copolymer, polypropylene Sour sodium, 1,2- ethohexadiols, Phenoxyethanol, PPG-26- butylol polyethers -26, Cremophor RH40, CI 16035 and essence mix Close, stir evenly, as oil phase；The water phase and oil phase are uniformly mixed, high-speed stirred is first carried out and stirs evenly, then carry out Matter, obtains homogeneous thing, and sheet microcapsules are added into homogeneous thing, obtains the whitening anti-wrinkling sleep mask with sheet microcapsules.
The sheet microcapsules are prepared with the following method：
1）Sodium alginate is configured to the solution that mass concentration is 2% with pure water, agar is configured to quality with pure water Concentration is 1% solution, and hydroxyethyl cellulose is configured to the solution that mass concentration is 1% with pure water, Sodium Hyaluronate is used Pure water is configured to the solution that mass concentration is 1%；
2）By step 1）After the solution of preparation is heated to 60 DEG C, mixed solution is simultaneously kept the temperature, spare；
3）Glycerine, vitamin e acetate, rhodamine toner dew, ursin and polysorbas20 are uniformly mixed；
4）Red 30 color lake CI73360 and titanium dioxide are milled mixing, and are mixed into step 3）In mixed raw material, stir Mix uniformly；
5）Phenoxyethanol, Sensiva SC50 and 1,2- ethohexadiols are mixed to join step 4）In mixed material, obtain To mixed material；
6）By step 5）Mixed material is heated to 75 DEG C, and adds step 2）In mixed solution, homogeneous is carried out, and protect The temperature for holding mixture is 60 ~ 70 DEG C, and it is spare to obtain homogeneous thing；
7）By step 6）Homogeneous thing pump after equal vacuum is exported and is added drop-wise on inclined-plane, and trickling on the inclined-plane has matter The calcium chloride solution that concentration is 2% is measured, obtains sheet microcapsules.
Embodiment 1：
A kind of sleep mask with sheet microcapsules, component are as shown in table 1 below：
1 component prescription table of table
Component Parts by weight
1 Water 72.7
2 Glycerine 3
3 PEG/PPG-17/6 copolymers 7
4 Propane diols 10
5 Glycine betaine 1
6 Ammonium acryloyldime-thyltaurate/VP copolymers 0.4
7 Sodium Polyacrylate 0.4
8 1,2- ethohexadiol 0.6
9 Phenoxyethanol 0.5
10 PPG-26- butylol polyethers -26 0.02
11 Cremophor RH40 0.02
12 Xanthans 0.05
13 CI 16035 0.3
14 （It is daily）Essence 0.01
15 Sheet microcapsules 3
Embodiment 2：
A kind of whitening anti-wrinkling sleep mask with sheet microcapsules, the component are as shown in table 2 below：
The component of 2 facial mask of table
Component Parts by weight
1 Water 70
2 Glycerine 2
3 PEG/PPG-17/6 copolymers 5
4 Propane diols 8
5 Glycine betaine 0.5
6 Ammonium acryloyldime-thyltaurate/VP copolymers 0.2
7 Sodium Polyacrylate 0.2
8 1,2- ethohexadiol 0.5
9 Phenoxyethanol 0.3
10 PPG-26- butylol polyethers -26 0.01
11 Cremophor RH40 0.01
12 Xanthans 0.03
13 CI 16035 0.2
14 （It is daily）Essence 0.01
15 Sheet microcapsules 2
Embodiment 3：
A kind of whitening anti-wrinkling sleep mask with sheet microcapsules, component prescription are as shown in table 3 below：
3 whitening anti-wrinkling sleep mask formula of table
Component Parts by weight
1 Water 75
2 Glycerine 5
3 PEG/PPG-17/6 copolymers 10
4 Propane diols 12
5 Glycine betaine 2
6 Ammonium acryloyldime-thyltaurate/VP copolymers 1
7 Sodium Polyacrylate 1
8 1,2- ethohexadiol 1
9 Phenoxyethanol 0.8
10 PPG-26- butylol polyethers -26 0.05
11 Cremophor RH40 0.05
12 Xanthans 0.08
13 CI 16035 0.5
14 （It is daily）Essence 0.03
15 Sheet microcapsules 5
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although applicant The present invention is described in detail with reference to preferred embodiment, it will be understood by those of ordinary skill in the art that, to the present invention's Technical solution technical scheme is modified or replaced equivalently, without departing from the objective and scope of technical solution of the present invention, should all cover Among scope of the presently claimed invention.

Claims (2)

  1. A kind of 1. whitening anti-wrinkling sleep mask with sheet microcapsules, it is characterised in that in parts by weight, including as follows into Point：70 ~ 75 parts of water, 2 ~ 5 parts of glycerine, 5 ~ 10 parts of PEG/PPG-17/6 copolymers, 8 ~ 12 parts of propane diols, 0.5 ~ 2 part of glycine betaine, 0.2 ~ 1 part of ammonium acryloyl taurate/VP copolymer, 0.2 ~ 1 part of Sodium Polyacrylate, 0.5 ~ 1 part of 1,2- ethohexadiol, 0.3 ~ 0.8 part of Phenoxyethanol, -26,0.01 ~ 0.05 parts of Cremophor RH40s of 0.01 ~ 0.05 part of PPG-26- butylol polyether, 0.03 ~ 0.08 part of xanthans, 0.2 ~ 0.5 part of CI, 16035,0.01 ~ 0.03 parts of essence and 2 ~ 5 parts of sheet microcapsules；
    The preparation method of the whitening anti-wrinkling sleep mask with sheet microcapsules, includes the following steps：
    Water and xanthans are uniformly mixed, as water phase；By glycerine, PEG/PPG-17/6 copolymers, propane diols, glycine betaine, third Alkene acyl dimethyltaurine ammonium/VP copolymers, Sodium Polyacrylate, 1,2- ethohexadiols, Phenoxyethanol, PPG-26- butylol polyethers- 26th, Cremophor RH40, CI 16035 and essence mixing, stir evenly, as oil phase；The water phase and oil phase are mixed Uniformly, first carry out high-speed stirred to stir evenly, then carry out homogeneous, obtain homogeneous thing, sheet microcapsules are added into homogeneous thing, are obtained To the whitening anti-wrinkling sleep mask with sheet microcapsules；
    Wherein, the sheet microcapsules in parts by weight, including following component：55 parts of sodium alginates, 28 parts of agar, 6 parts of hydroxyl second Base cellulose, 6 parts of Sodium Hyaluronates, 12 parts of glycerine, 2 parts of vitamin e acetates, 3 parts of rhodamine toner dew, 2 parts of ursin, 3 parts spit 20,0.2 parts of red 30 color lake CI73360 of temperature, 0.2 part of titanium dioxide, 0.6 part of Phenoxyethanol, 0.3 part of Sensiva SC50 and 0.5 part 1,2- ethohexadiols；
    The sheet microcapsules are prepared with the following method：
    1）Sodium alginate is configured to the solution that mass concentration is 2% with pure water, agar is configured to mass concentration with pure water For 1% solution, hydroxyethyl cellulose is configured to the solution that mass concentration is 1% with pure water, by Sodium Hyaluronate with pure Water is configured to the solution that mass concentration is 1%；
    2）By step 1）After the solution of preparation is heated to 60 DEG C, mixed solution is simultaneously kept the temperature, spare；
    3）Glycerine, vitamin e acetate, rhodamine toner dew, ursin and polysorbas20 are uniformly mixed；
    4）Red 30 color lake CI73360 and titanium dioxide are milled mixing, and are mixed into step 3）In mixed raw material, stirring is equal It is even；
    5）Phenoxyethanol, Sensiva SC50 and 1,2- ethohexadiols are mixed to join step 4）In mixed material, mixed Close raw material；
    6）By step 5）Mixed material is heated to 75 DEG C, and adds step 2）In mixed solution, homogeneous is carried out, and keeps mixed The temperature of compound is 60 ~ 70 DEG C, and it is spare to obtain homogeneous thing；
    7）By step 6）Homogeneous thing pump after equal vacuum is exported and is added drop-wise on inclined-plane, and trickling on the inclined-plane has the quality dense The calcium chloride solution for 2% is spent, obtains sheet microcapsules.
  2. 2. the whitening anti-wrinkling sleep mask of sheet microcapsules is carried according to claim 1, it is characterised in that with parts by weight Meter, including following component：72.7 parts of water, 3 parts of glycerine, 7 parts of PEG/PPG-17/6 copolymers, 10 parts of propane diols, 1 part of glycine betaine, 0.4 part of ammonium acryloyl taurate/VP copolymer, 0.4 part of Sodium Polyacrylate, 0.6 part of 1,2- ethohexadiol, 0.5 part of benzene oxygen Ethanol, -26,0.02 parts of Cremophor RH40s of 0.02 part of PPG-26- butylol polyether, 0.05 part of xanthans, 0.3 part of CI 16035th, 0.01 part of essence and 3 parts of sheet microcapsules.
CN201510858061.6A 2015-11-30 2015-11-30 A kind of whitening anti-wrinkling sleep mask with sheet microcapsules Active CN105326648B (en)

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109199926B (en) * 2018-10-26 2021-08-03 浙江大学华南工业技术研究院 Transparent sleep mask containing emollient oil and preparation method thereof
CN111773121A (en) * 2020-08-11 2020-10-16 黑龙江天龙药业有限公司 Moisture-preserving and whitening sleeping mask and preparation method thereof

Citations (2)

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Publication number Priority date Publication date Assignee Title
US6391288B1 (en) * 1999-07-27 2002-05-21 Shiseido Co., Ltd. Microcapsule and method of making the same
CN103932898A (en) * 2014-04-25 2014-07-23 北京博辉瑞进生物科技有限公司 Full-function facial mask and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6391288B1 (en) * 1999-07-27 2002-05-21 Shiseido Co., Ltd. Microcapsule and method of making the same
CN103932898A (en) * 2014-04-25 2014-07-23 北京博辉瑞进生物科技有限公司 Full-function facial mask and preparation method thereof

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Address after: 401519 Chongqing Hechuan Industrial Park weir village two

Patentee after: Chongqing Xiaowan Biotechnology Co., Ltd.

Address before: 401519 Chongqing Hechuan Industrial Park weir village two

Patentee before: CHONGQING XIAOWAN TRADE CO., LTD.