CN108478519A - A kind of fossil water light stoste containing fullerene - Google Patents
A kind of fossil water light stoste containing fullerene Download PDFInfo
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- CN108478519A CN108478519A CN201810364300.6A CN201810364300A CN108478519A CN 108478519 A CN108478519 A CN 108478519A CN 201810364300 A CN201810364300 A CN 201810364300A CN 108478519 A CN108478519 A CN 108478519A
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/673—Vitamin B group
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The fossil water light stoste containing fullerene that the invention discloses a kind of, including the following raw material is prepared：Water, oligopeptides 1, butanediol, glycine betaine, ethoxy urea, biological carbohydrate gum 1, glycerine, fullerene, rose wate, trehalose, fermentation of bacillus product, saccharomycetes to make fermentation product, tranexamic acid, Sodium Hyaluronate, Magnolia binodii bud/flower extract, peppermint leaf extract, niacinamide, 1,2 hexylene glycols, 1 methyl hydantoin, 2 acid imide, hamamelis extract, tara gum, xanthans, dextrin, allantoin.Water light stoste of the present invention has effects that good removing free radical, whitening, moisturizing.
Description
Technical field
The present invention relates to cosmetic field more particularly to a kind of fossil water light stostes containing fullerene.
Background technology
Fullerene（Fullerene) it is a kind of allotrope of carbon.It is any to be made of a kind of element of carbon, with spherical ellipse
Substance existing for round shape or tubular structure can be called fullerene.Fullerene is similar with graphite-structure, but the knot of graphite
There was only hexatomic ring in structure, and there may be five-membered rings in fullerene.Fullerene is known as " diamond alkene ", is added in cosmetics rich
Alkene is strangled, can be prepared by sun-proof articles to the absorption of ultraviolet light using it.Fullerene has strong anti-oxidation, Neng Gouyan simultaneously
Slow skin aging.Fullerene molecule can be catalyzed and remove free radical, recombine free radical, therefore fullerene molecule can incite somebody to action oneself
Inactive molecular product is converted by base.Fullerene is proved to be safe and non-toxic substance, can be as the ingredient of cosmetics
One of.
However, fullerene molecule property not soluble in water itself seriously limits its application in biomedical sector,
Therefore improving the water solubility of C60 becomes the key of research, and work could be played in Physiological Medium by increasing the water solubility of C60 molecules
With.Three kinds of modes are mainly used at present：First is to be wrapped up C60 fullerenes using special structure, is made so-called
Wrap up particle.The second way is that the suspension of C60 fullerenes is made using some cosolvents.The third mode is to utilize one
A little hydrophilic molecules and C60 fullerenes are done in conjunction with increasing the solubility of C60 fullerene molecules.Patent
201310095499.4 disclosing a kind of fullerene-vitamin-water soluble polymer ternary complex preparation method, mainly carry
The performance of height removal free radical, and the function without skin whitening, moisturizing.
Therefore, using fullerene, exploitation is a kind of not only to have had the performance for removing very much free radical by force, but also long with whitening, moisture retention
Imitate the multifunctional product of the performances such as moisturizing, it would be highly desirable to solve.
Invention content
To solve the deficiency that product in the prior art removes free radical, whitening, performance of keeping humidity, a kind of mine containing fullerene is provided
Object water light stoste can have the multi-efficiencies such as anti-oxidant, whitening, moisturizing.
To realize the above-mentioned technical purpose, it is resolved by following technical solution：
A kind of fossil water light stoste containing fullerene, including the following raw material：
Water, oligopeptides -1, butanediol, glycine betaine, ethoxy urea, biological carbohydrate gum -1, glycerine, fullerene, rose wate, trehalose,
Fermentation of bacillus product, saccharomycetes to make fermentation product, tranexamic acid, Sodium Hyaluronate, Magnolia binodii bud/flower extract, dried peppermint leaf
Extract, niacinamide, 1,2- hexylene glycols, 1- methyl hydantoin -2- acid imides, hamamelis extract, tara gum, Huang
Virgin rubber, dextrin, allantoin.
Preferably, the stoste, including following raw material：
40-80 parts of water, -1 1-5 parts of oligopeptides, 0.5-2.0 parts of butanediol, 0.5-1.0 parts of glycine betaine, ethoxy urea 0.4-0.6
Part, biological -1 1-3 parts of carbohydrate gum, 1-2 parts of glycerine, 1-5 parts of fullerene, 0.5-3 parts of rose wate, trehalose 0.4-0.8
Part, 2-5 parts of fermentation of bacillus product, 1-5 parts of saccharomycetes to make fermentation product, 0.05-0.2 parts of tranexamic acid, Sodium Hyaluronate
0.5-1.0 parts, Magnolia binodii bud/1-3 parts of flower extract, 2-8 parts of peppermint leaf extract, 0.5-2.0 parts of niacinamide, 1,2- oneself
0.5-0.8 parts of glycol, 0.4-0.7 parts of 1- methyl hydantoins -2- acid imides, 0.9-3.0 parts of hamamelis extract,
0.1-1.0 parts of tara gum, 0.1-1.0 parts of xanthans, 0.5-0.8 parts of dextrin, 3.0-6.0 parts of allantoin.
Preferably, the stoste, including following raw material：
60 parts of water, 2 parts of oligopeptides -1,1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum,
1.5 parts of glycerine, 3.0 parts of fullerene, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, yeast
2 parts of bacterium tunning, 0.1 part of tranexamic acid, 0.9 part of Sodium Hyaluronate, Magnolia binodii bud/2 parts of flower extract, dried peppermint leaf extraction
4 parts of object, 0.6 part of niacinamide, 0.7 part of 1,2- hexylene glycols, 0.6 part of 1- methyl hydantoin -2- acid imides, hamamelis
2.0 parts of extract, 0.5 part of tara gum, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
Preferably, the saccharomycetes to make fermentation product is saccharomycete/zinc tunning, saccharomycete/calcium tunning, yeast
One or more in bacterium/magnesium tunning, saccharomycete/iron tunning, saccharomycete/silicon tunning.
Preferably, the yeast tunning includes following parts by weight substance：Saccharomycete/zinc tunning 0.5-1.0
Part, saccharomycete/0.5-1.0 parts of calcium tunning, saccharomycete/0.5-1.0 parts of magnesium tunning, saccharomycete/iron tunning
0.5-1.0 parts, saccharomycete/0.5-1.0 parts of silicon tunning.
Preferably, the tunning includes following parts by weight substance：Saccharomycete/0.6 part of zinc tunning, yeast
Bacterium/0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, saccharomycete/0.8 part of iron tunning, saccharomycete/silicon hair
0.7 part of ferment product.
The preparation method of the stoste, including following preparation process：
1. weighing glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, 1- methyl second according to mass parts
Interior uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 80-90 DEG C, keep temperature 30-
60min obtains mixture 1；
2. mixture 1 is cooled to 70-75 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, obtains
Mixture 2；
3. by parts by weight fullerene, allantoin, niacinamide, tranexamic acid, weight percent is the ethyl alcohol of 40-60%, is stirred evenly,
It is heated to 70-80 DEG C, temperature 1-3h is kept, obtains mixture 3；
4. by step 2., 3. in mixture 2,3 system of mixture be cooled to 50-60 DEG C respectively, then by mixture 2, mixture 3
It is mixed, is stirred evenly, obtain mixture 4；
5. mixture 4 continues to be cooled to 35-45 DEG C, parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation production is added
Object, Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and adjust PH to 6.5-
6.8, stir evenly the fossil water light stoste to get the fullerene.
Preferably, the saccharomycetes to make fermentation product is saccharomycete/zinc tunning, saccharomycete/calcium tunning, yeast
One or more in bacterium/magnesium tunning, saccharomycete/iron tunning, saccharomycete/silicon tunning.
Preferably, the mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
Preferably, 1. the temperature is 85 DEG C to step；
4. the temperature is 40 DEG C to step.
Advantageous effect：Product of the present invention, added with fullerene and allantoin, niacinamide, tranexamic acid under the action of ethyl alcohol,
Compound is formed, there is extraordinary stability and water solubility, with the product of its preparation, not only there is very strong removing free radical
Ability, also have effects that skin whitening, moisturizing, by the compound and saccharomycete/zinc tunning, saccharomycete/calcium tunning,
Saccharomycete/magnesium tunning, saccharomycete/iron tunning, saccharomycete/silicon tunning, oligopeptides -1, fermentation of bacillus production
Object, saccharomycetes to make fermentation product, Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate
It is used in conjunction with, there is synergy, significantly promote the effect of removing free radical, whitening, moisturizing of cosmetics.
Specific embodiment
A kind of preparation of the fossil water light stoste containing fullerene of embodiment 1
A kind of fossil water light stoste containing fullerene, including following raw material：
40 parts of water, 1 part of oligopeptides -1,0.5 part of butanediol, 0.5 part of glycine betaine, 0.4 part of ethoxy urea, biological -1 1 part of carbohydrate gum,
1 part of glycerine, 1- parts of fullerene, 0.5 part of rose wate, 0.4 part of trehalose, 2 parts of fermentation of bacillus product, saccharomycete
1 part of tunning, 0.05 part of tranexamic acid, 0.5 part of Sodium Hyaluronate, Magnolia binodii bud/1 part of flower extract, dried peppermint leaf extraction
2 parts of object, 0.5 part of niacinamide, 0.5 part of 1,2- hexylene glycols, 0.4 part of 1- methyl hydantoin -2- acid imides, hamamelis
0.9 part of extract, 0.1 part of tara gum, 0.1 part of xanthans, 0.5 part of dextrin, 3.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/0.5 part of zinc tunning, saccharomycete/
0.5 part of calcium tunning, saccharomycete/1 part of magnesium tunning, saccharomycete/1 part of iron tunning, saccharomycete/silicon tunning 1
Part.
The preparation method of the stoste, including following preparation process：
1. weighing glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, 1- methyl second according to mass parts
Interior uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 80 DEG C, keep temperature 30min, obtain
Mixture 1；
2. mixture 1 is cooled to 70 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Close object 2；
3. by parts by weight fullerene, allantoin, niacinamide, tranexamic acid, the ethyl alcohol that weight percent is 40% stirs evenly, and heats
To 70 DEG C, temperature 1h is kept, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 50 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 35 DEG C, be added parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product,
Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and PH to 6.5 is adjusted, stirring is equal
The even fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
A kind of preparation of the fossil water light stoste containing fullerene of embodiment 2
A kind of fossil water light stoste containing fullerene, including following raw material：
60 parts of water, 2 parts of oligopeptides -1,1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum,
1.5 parts of glycerine, 3.0 parts of fullerene, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, yeast
2 parts of bacterium tunning, 0.1 part of tranexamic acid, 0.9 part of Sodium Hyaluronate, Magnolia binodii bud/2 parts of flower extract, dried peppermint leaf extraction
4 parts of object, 0.6 part of niacinamide, 0.7 part of 1,2- hexylene glycols, 0.6 part of 1- methyl hydantoin -2- acid imides, hamamelis
2.0 parts of extract, 0.5 part of tara gum, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/0.6 part of zinc tunning, saccharomycete/
0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, saccharomycete/0.8 part of iron tunning, saccharomycete/silicon fermentation production
0.7 part of object.
The preparation method of the stoste, including following preparation process：
1. weighing glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, 1- methyl second according to mass parts
Interior uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 85 DEG C, keep temperature 40min, obtain
Mixture 1；
2. closing object 1 is cooled to 72 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Object 2；
3. parts by weight fullerene, allantoin, niacinamide, tranexamic acid, the ethyl alcohol that weight percent is 50%, stir evenly, are heated to
75 DEG C, temperature 2h is kept, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 55 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 40 DEG C, be added parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product,
Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and PH to 6.7 is adjusted, stirring is equal
The even fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
A kind of preparation of the fossil water light stoste containing fullerene of embodiment 3
A kind of fossil water light stoste containing fullerene, including following raw material：
80 parts of water, 5 parts of oligopeptides -1,2.0 parts of butanediol, 1.0 parts of glycine betaine, 0.6 part of ethoxy urea, biological -1 3 part of carbohydrate gum,
2 parts of glycerine, 5 parts of fullerene, 3 parts of rose wate, 0.8 part of trehalose, 5 parts of fermentation of bacillus product, saccharomycetes to make fermentation
5 parts of product, 0.2 part of tranexamic acid, 1.0 parts of Sodium Hyaluronate, Magnolia binodii bud/3 parts of flower extract, peppermint leaf extract 8
Part, 2.0 parts of niacinamide, 0.8 part of 1,2- hexylene glycols, 0.7 part of 1- methyl hydantoin -2- acid imides, hamamelis extraction
3.0 parts of object, 1.0 parts of tara gum, 1.0 parts of xanthans, 0.8 part of dextrin, 6.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/1.0 parts of zinc tunning, saccharomycete/
1.0 parts of calcium tunning, saccharomycete/0.5 part of magnesium tunning, saccharomycete/0.5 part of iron tunning, saccharomycete/silicon fermentation production
0.5 part of object.
The preparation method of the stoste, including following preparation process：
1. weighing glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, 1- methyl second according to mass parts
Interior uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 90 DEG C, keep temperature 60min, obtain
Mixture 1；
2. mixture 1 is cooled to 75 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Close object 2；
3. by parts by weight fullerene, allantoin, niacinamide, tranexamic acid, the ethyl alcohol that weight percent is 60% stirs evenly, and heats
To 80 DEG C, temperature 3h is kept, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 60 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 45 DEG C, be added parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product,
Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and PH to 6.8 is adjusted, stirring is equal
The even fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
A kind of preparation of 1 water light stoste of comparative example
A kind of preparation of water light stoste, including following raw material：
60 parts of water, 2 parts of oligopeptides -1,1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum,
1.5 parts of glycerine, 3.0 parts of fullerene, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, yeast
2 parts of bacterium tunning, 0.9 part of Sodium Hyaluronate, Magnolia binodii bud/2 parts of flower extract, 4 parts of peppermint leaf extract, niacinamide
0.6 part, 0.7 part of 1,2- hexylene glycols, 0.6 part of 1- methyl hydantoin -2- acid imides, 2.0 parts of hamamelis extract, thorn
0.5 part of mysorethorn glue, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/0.6 part of zinc tunning, saccharomycete/
0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, saccharomycete/0.8 part of iron tunning, saccharomycete/silicon fermentation production
0.7 part of object.
The preparation method of the stoste, including following preparation process：
1. according to mass parts weigh glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, in 1- methyl second
Uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 85 DEG C, keep temperature 40min, obtain mixed
Close object 1；
2. closing object 1 is cooled to 72 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Object 2；
3. parts by weight fullerene, allantoin, niacinamide, the ethyl alcohol that weight percent is 20%, stir evenly, 75 DEG C are heated to, is protected
Temperature 2h is held, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 55 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 40 DEG C, be added parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product,
Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and PH to 6.7 is adjusted, stirring is equal
The even fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-nicotinoyl amine compound；
Comparative example 1 the difference from example 2 is that, mixture 3 be fullerene-allantoin-niacinamide, be free of tranexamic acid, and
The concentration of ethyl alcohol used is different.
A kind of preparation of 2 water light stoste of comparative example
A kind of preparation of water light stoste, including following raw material：
60 parts of water, 2 parts of oligopeptides -1,1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum,
1.5 parts of glycerine, 3.0 parts of fullerene, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, yeast
2 parts of bacterium tunning, 0.1 part of tranexamic acid, 0.9 part of Sodium Hyaluronate, Magnolia binodii bud/2 parts of flower extract, dried peppermint leaf extraction
4 parts of object, 0.6 part of niacinamide, 0.7 part of 1,2- hexylene glycols, 0.6 part of 1- methyl hydantoin -2- acid imides, hamamelis
2.0 parts of extract, 0.5 part of tara gum, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/0.6 part of zinc tunning, saccharomycete/
0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, saccharomycete/0.8 part of iron tunning, saccharomycete/silicon fermentation production
0.7 part of object.
The preparation method of the stoste, including following preparation process：
1. according to mass parts weigh glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, in 1- methyl second
Uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 85 DEG C, keep temperature 40min, obtain mixed
Close object 1；
2. closing object 1 is cooled to 72 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Object 2；
3. parts by weight fullerene, allantoin, niacinamide, tranexamic acid, the ethyl alcohol that weight percent is 50%, stir evenly, heat
To 75 DEG C, temperature 2h is kept, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 55 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 40 DEG C, be added parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product,
Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and PH to 6.7 is adjusted, stirring is equal
The even fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
Comparative example 2 the difference from example 2 is that, comparative example 2 be free of saccharomycetes to make fermentation product.
A kind of preparation of 3 water light stoste of comparative example
A kind of preparation of water light stoste, including following raw material：
60 parts of water, 2 parts of oligopeptides -1,1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum,
1.5 parts of glycerine, 3.0 parts of fullerene, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, yeast
2 parts of bacterium tunning, 0.1 part of tranexamic acid, 0.9 part of Sodium Hyaluronate, 0.6 part of niacinamide, 0.7 part of 1,2- hexylene glycols, 1- first
0.6 part of base hydantoins -2- acid imides, 0.5 part of tara gum, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
The saccharomycetes to make fermentation product includes following parts by weight substance：Saccharomycete/0.6 part of zinc tunning, saccharomycete/
0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, saccharomycete/0.8 part of iron tunning, saccharomycete/silicon fermentation production
0.7 part of object.
The preparation method of the stoste, including following preparation process：
1. according to mass parts weigh glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, in 1- methyl second
Uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 85 DEG C, keep temperature 40min, obtain mixed
Close object 1；
2. closing object 1 is cooled to 72 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, is mixed
Object 2；
3. parts by weight fullerene, allantoin, niacinamide, tranexamic acid, the ethyl alcohol that weight percent is 50%, stir evenly, are heated to
75 DEG C, temperature 2h is kept, mixture 3 is obtained；
4. 2., 3. middle mixture 2,3 system of mixture are cooled to 55 DEG C, then mixture 2, mixture 3 are carried out respectively by step
Mixing, stirs evenly, obtains mixture 4；
5. mixture 4 continues to be cooled to 40 DEG C, parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation product is added,
And PH to 6.7 is adjusted, stir evenly the fossil water light stoste to get the fullerene.
The mixture 3 is i.e. fullerene-allantoin-niacinamide-tranexamic acid compound；
Comparative example 3 the difference from example 2 is that, comparative example 2 without Magnolia binodii bud/flower extract, peppermint leaf extract, north
U.S. hamamelis extract, rose wate.
Experiment：
Experimental group：Embodiment 1-3 products obtained therefroms are respectively experimental group 1-3, and comparative example 1-3 is respectively control group 1-3, commercially available whitening
Tender skin stoste position comparative example 4.
1. Scavenging ability
Table 1 detects inventive samples and comparative example and the antioxygenic activity of commercial samples（AOA）, AOA expression titration 100g institutes
The coulomb amount of the material consumption of analysis.Such as table 1.
Table 1：
By upper table visitor it is found that the cosmetics obtained by the present invention are significantly higher than comparative example and commercial product, show that the present invention's is anti-
Oxidability is strong, can effectively remove free radical.
2. white-skinned face function
Skin complexion L values are measured, the skin color tester produced using German Courage Khazaka (CK) company
Colorimeter CL400 use the variation of front and back skin L values by measuring product, assess its shadow to the bright degree of skin
It rings, three groups of subjects identical to initial L value average value are detected, every group of 10 people, and the period is 2 weeks, and results are averaged, such as
Table 2：
Table 2：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
| 0 week | 43.2 | 44.1 | 45.6 | 45.8 | 44.7 | 43.5 | 46.3 |
| 2 weeks | 68.9 | 75.4 | 72.1 | 48.3 | 50.2 | 51.4 | 50.7 |
As can be seen from the above table, for L values of the invention after using product 2 weeks, growth rate is apparently higher than comparative example and commercial product,
Show that white-skinned face function of the invention is notable, it is high using the bright degree of rear skin.
3. the hydrauture of skin
Measure the hydrauture of skin, 0 week and the average value using product after 2 weeks of 7 groups of subjects of detection, every group of 10 people, period
It it is 2 weeks, as a result such as table 3：
Table 3：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
| 0 | 23.1 | 23.6 | 24.1 | 23.6 | 23.0 | 24.2 | 24.5 |
| 2 weeks | 50.6 | 60.1 | 55.1 | 35.4 | 35.6 | 40.1 | 30.1 |
As shown in Table 3, after product use of the present invention, subjects skin's hydrauture increases faster, hence it is evident that better than comparative example and commercially available
Product shows that moistening effect of the present invention is good, can repair dry skin, keeps moisture of skin sufficient.
Above-mentioned detailed description is illustrating for one of them possible embodiments of the present invention, the embodiment not to
The scope of the claims of the present invention is limited, all equivalence enforcements or change without departing from carried out by the present invention are intended to be limited solely by the technology of the present invention
In the range of scheme.
Claims (10)
1. a kind of fossil water light stoste containing fullerene, which is characterized in that include the following raw material：
Water, oligopeptides -1, butanediol, glycine betaine, ethoxy urea, biological carbohydrate gum -1, glycerine, fullerene, rose wate, trehalose,
Fermentation of bacillus product, saccharomycetes to make fermentation product, tranexamic acid, Sodium Hyaluronate, Magnolia binodii bud/flower extract, dried peppermint leaf
Extract, niacinamide, 1,2- hexylene glycols, 1- methyl hydantoin -2- acid imides, hamamelis extract, tara gum, Huang
Virgin rubber, dextrin, allantoin.
2. stoste according to claim 1, which is characterized in that include following raw material：40-80 parts of water, oligopeptides -1
1-5 parts, it is 0.5-2.0 parts of butanediol, 0.5-1.0 parts of glycine betaine, 0.4-0.6 parts of ethoxy urea, biological -1 1-3 parts of carbohydrate gum, sweet
1-2 parts oily, 1-5 parts of fullerene, 0.5-3 parts of rose wate, 0.4-0.8 parts of trehalose, fermentation of bacillus product 2-5
Part, 1-5 parts of saccharomycetes to make fermentation product, 0.05-0.2 parts of tranexamic acid, 0.5-1.0 parts of Sodium Hyaluronate, Magnolia binodii bud/flower carry
Take 1-3 parts of object, 2-8 parts of peppermint leaf extract, 0.5-2.0 parts of niacinamide, 0.5-0.8 parts of 1,2- hexylene glycols, in 1- methyl second
0.4-0.7 parts of uride -2- acid imides, 0.9-3.0 parts of hamamelis extract, 0.1-1.0 parts of tara gum, xanthans
0.1-1.0 parts, 0.5-0.8 parts of dextrin, 3.0-6.0 parts of allantoin.
3. stoste according to claim 2, which is characterized in that include following raw material：60 parts of water, oligopeptides -1 2
Part, 1.0 parts of butanediol, 0.8 part of glycine betaine, 0.5 part of ethoxy urea, biological -12 parts of carbohydrate gum, 1.5 parts of glycerine, fullerene 3.0
Part, 2.0 parts of rose wate, 0.6 part of trehalose, 3 parts of fermentation of bacillus product, 2 parts of saccharomycetes to make fermentation product, tranexamic acid
0.1 part, 0.9 part of Sodium Hyaluronate, Magnolia binodii bud/2 parts of flower extract, 4 parts of peppermint leaf extract, 0.6 part of niacinamide,
0.7 part of 1,2- hexylene glycols, 0.6 part of 1- methyl hydantoin -2- acid imides, 2.0 parts of hamamelis extract, tara gum
0.5 part, 0.6 part of xanthans, 0.7 part of dextrin, 4.0 parts of allantoin.
4. according to any stostes of claim 1-3, which is characterized in that the saccharomycetes to make fermentation product be saccharomycete/
Zinc tunning, saccharomycete/calcium tunning, saccharomycete/magnesium tunning, saccharomycete/iron tunning, saccharomycete/silicon hair
One or more in ferment product.
5. according to any stostes of claim 1-3, which is characterized in that the yeast tunning includes following weight
Part substance：Saccharomycete/0.5-1.0 parts of zinc tunning, saccharomycete/0.5-1.0 parts of calcium tunning, saccharomycete/magnesium fermentation production
0.5-1.0 parts of object, saccharomycete/0.5-1.0 parts of iron tunning, saccharomycete/0.5-1.0 parts of silicon tunning.
6. according to any stostes of claim 1-3, which is characterized in that the tunning includes following parts by weight object
Matter：Saccharomycete/0.6 part of zinc tunning, saccharomycete/0.6 part of calcium tunning, saccharomycete/0.8 part of magnesium tunning, yeast
Bacterium/0.8 part of iron tunning, saccharomycete/0.7 part of silicon tunning.
7. according to the preparation method of any stostes of claim 1-3, which is characterized in that include following preparation process：
1. weighing glycine betaine, biological carbohydrate gum -1, glycerine, trehalose, niacinamide, 1,2- hexylene glycols, 1- methyl second according to mass parts
Interior uride -2- acid imides, xanthans, tara gum, dextrin, water, stir evenly, and are heated to 80-90 DEG C, keep temperature 30-
60min obtains mixture 1；
2. mixture 1 is cooled to 70-75 DEG C, parts by weight butanediol, ethoxy urea, Sodium Hyaluronate is added, stirs evenly, obtains
Mixture 2；
3. by parts by weight fullerene, allantoin, niacinamide, tranexamic acid, weight percent is the ethyl alcohol of 40-60%, is stirred evenly,
It is heated to 70-80 DEG C, temperature 1-3h is kept, obtains mixture 3；
4. by step 2., 3. in mixture 2,3 system of mixture be cooled to 50-60 DEG C respectively, then by mixture 2, mixture 3
It is mixed, is stirred evenly, obtain mixture 4；
5. mixture 4 continues to be cooled to 35-45 DEG C, parts by weight oligopeptides -1, fermentation of bacillus product, saccharomycetes to make fermentation production is added
Object, Magnolia binodii bud/flower extract, hamamelis extract, peppermint leaf extract, rose wate, and adjust PH to 6.5-
6.8, stir evenly the fossil water light stoste to get the fullerene.
8. preparation method according to claim 7, which is characterized in that the saccharomycetes to make fermentation product is saccharomycete/zinc
Tunning, saccharomycete/calcium tunning, saccharomycete/magnesium tunning, saccharomycete/iron tunning, saccharomycete/silicon fermentation
One or more in product.
9. preparation method according to claim 7, which is characterized in that the mixture 3 is i.e. fullerene-allantoin-cigarette
Amide-tranexamic acid compound.
10. preparation method according to claim 7, which is characterized in that 1. the temperature is 85 DEG C to step；Step 4. institute
The temperature stated is 40 DEG C.
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| CN109276523A (en) * | 2018-11-30 | 2019-01-29 | 兰海宁 | A kind of peppermint facial mask liquid and preparation method thereof |
| CN109316360A (en) * | 2018-10-10 | 2019-02-12 | 广州雷诺生物科技有限公司 | A kind of fullerene intensively lifts Essence |
| CN109718194A (en) * | 2018-12-09 | 2019-05-07 | 广州珈源日化用品有限公司 | A kind of yeast extract, oligopeptides -1 and the compact micro- face stoste of acetyl group hexapeptide -1 |
| CN109793697A (en) * | 2019-03-25 | 2019-05-24 | 韩兴旺 | A kind of Anti-allergic cosmetic composition and its preparation process containing plant active peptides |
| CN109846726A (en) * | 2018-10-10 | 2019-06-07 | 广州雷诺生物科技有限公司 | A kind of fullerene skin activating water and preparation method thereof |
| CN109966203A (en) * | 2019-04-02 | 2019-07-05 | 北京旋光普利生物医药科技开发有限公司 | A kind of preparation of hydrosol fullerene facial mask |
| CN110538135A (en) * | 2019-10-11 | 2019-12-06 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil essence and preparation method thereof |
| CN110585098A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil smoothing toner and preparation method thereof |
| CN110897987A (en) * | 2019-12-16 | 2020-03-24 | 广州熙然化妆品有限公司 | Composition for resisting wrinkles and tightening skin and application of composition in cosmetics |
| CN110917118A (en) * | 2020-01-02 | 2020-03-27 | 广州博美芬生物科技有限公司 | Mask for inhibiting melanin from refluxing and percutaneous absorption to balance microecology |
| CN113616534A (en) * | 2021-08-25 | 2021-11-09 | 上海美浮特生物科技有限公司 | Composition for inhibiting PAR-2 from activating keratinocytes and application of composition in facial mask |
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|---|---|---|---|---|
| CN109316360A (en) * | 2018-10-10 | 2019-02-12 | 广州雷诺生物科技有限公司 | A kind of fullerene intensively lifts Essence |
| CN109846726A (en) * | 2018-10-10 | 2019-06-07 | 广州雷诺生物科技有限公司 | A kind of fullerene skin activating water and preparation method thereof |
| CN109276523A (en) * | 2018-11-30 | 2019-01-29 | 兰海宁 | A kind of peppermint facial mask liquid and preparation method thereof |
| CN109718194A (en) * | 2018-12-09 | 2019-05-07 | 广州珈源日化用品有限公司 | A kind of yeast extract, oligopeptides -1 and the compact micro- face stoste of acetyl group hexapeptide -1 |
| CN109793697A (en) * | 2019-03-25 | 2019-05-24 | 韩兴旺 | A kind of Anti-allergic cosmetic composition and its preparation process containing plant active peptides |
| CN109966203A (en) * | 2019-04-02 | 2019-07-05 | 北京旋光普利生物医药科技开发有限公司 | A kind of preparation of hydrosol fullerene facial mask |
| CN110538135A (en) * | 2019-10-11 | 2019-12-06 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil essence and preparation method thereof |
| CN110585098A (en) * | 2019-10-11 | 2019-12-20 | 茂名市瑜丰沉香创意产业有限公司 | Agilawood essential oil smoothing toner and preparation method thereof |
| CN110897987A (en) * | 2019-12-16 | 2020-03-24 | 广州熙然化妆品有限公司 | Composition for resisting wrinkles and tightening skin and application of composition in cosmetics |
| CN110917118A (en) * | 2020-01-02 | 2020-03-27 | 广州博美芬生物科技有限公司 | Mask for inhibiting melanin from refluxing and percutaneous absorption to balance microecology |
| CN113616534A (en) * | 2021-08-25 | 2021-11-09 | 上海美浮特生物科技有限公司 | Composition for inhibiting PAR-2 from activating keratinocytes and application of composition in facial mask |
| CN113616534B (en) * | 2021-08-25 | 2023-09-15 | 上海美浮特生物科技有限公司 | PAR-2-activating-inhibiting keratinocyte composition and application thereof in mask |
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