CN105325826A - Multifunctional nanometer carbon drink and preparing method thereof - Google Patents
Multifunctional nanometer carbon drink and preparing method thereof Download PDFInfo
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- CN105325826A CN105325826A CN201510907456.0A CN201510907456A CN105325826A CN 105325826 A CN105325826 A CN 105325826A CN 201510907456 A CN201510907456 A CN 201510907456A CN 105325826 A CN105325826 A CN 105325826A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/44—Elemental carbon, e.g. charcoal, carbon black
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Abstract
The invention discloses a multifunctional nanometer carbon drink which is prepared from nanometer carbon and water. The drink is prepared through the process of grinding, mixing and sterilizing. The content of the nanometer carbon is 1-100000 micrograms/ml. The invention further discloses a preparing method for the multifunctional nanometer carbon drink. According to the preparing method, the raw materials comprise the nanometer carbon and the water, the nanometer carbon is added into the water and ground to prepare nanometer carbon paste, the nanometer carbon paste is taken and mixed into the water, and the sterilizing process is carried out to obtain the drink. The multifunctional nanometer carbon drink can effectively clear waste in the gastrointestinal tract, can adsorb harmful substances such as creatinine and uric acid, has sterilizing and bacterium resisting functions, and has no toxic or side effects on the human body completely as the action principle of the nanometer carbon is a physical effect. The preparing method for the multifunctional nanometer carbon drink is simple, high in operability, easy to standardize and worthy of popularization in the industry.
Description
Technical field
The invention belongs to food technology field, be specifically related to a kind of nano-sized carbon multifunctional beverage and preparation method thereof.
Background technology
Beverage belongs to people and to live indispensable food.People are to the lifting of food variation requirement thereupon, and the single beverage for quenching one's thirst can not meet the demand in market, so beverage miscellaneous emerges in an endless stream, can feel different colours from difference, then to difference in functionality.From drinks analysis, there is the energy drink for regaining one's strength of body in present market, and as red ox, Dong Pengte drink and K can the brands such as ginseng, also has the vegetable and fruit beverage for replenishing vitamins, also has the animals and plants dairy beverage for supplementary protein.Above-mentioned functions beverage is mainly emphasized to supplement the nutrients, but under existing living standard, enough nutrition can be provided in human body, even occur the phenomenon of overnutrition in the food that people take in.Market also has a class cleaning type beverage, and as intestines tea is clear, but this type of its cleaning effect of cleaning type beverage is only limitted to absorption, and effect is very limited.
Summary of the invention
The object of the invention is to solve the problem, a kind of nano-sized carbon multifunctional beverage enterogastric diseases being played to alleviation and even healing effect is provided.
Another object of the present invention is to the preparation method that a kind of above-mentioned nano-sized carbon multifunctional beverage is provided.
For solving the problems of the technologies described above, technical scheme of the present invention is: a kind of nano-sized carbon multifunctional beverage, and its raw material comprises nano-sized carbon and water, and be prepared from after grinding, allotment, sterilization process, wherein nano-sized carbon content is 1 μ g ~ 100000 μ g/ml.
Preferably, described raw material also comprises surfactant, and described surface-active contents is 0g ~ 1g/ml.
Preferably, described surfactant comprises one or more in anion surfactant, cationic surfactant and ionic surface active agent.
Preferably, described nano-sized carbon to comprise in active carbon, carbon black, CNT, microcrystalline carbon, carbon aerogels, Graphene one or more.
Preferably, described water is deionized water, distilled water, mineral water or one or more in purifying waste water.
Nanometer carbon nanobeads, there is good chemical stability, larger specific area and good surface-active, therefore, after nano-sized carbon enters human body, effectively can adsorb remains of pesticide in alimentary canal and human body, bactericide, heavy metal, bioxin and various pathogenic bacteria and toxin thereof, the harmful substance such as creatinine and uric acid can also be adsorbed, also there is sterilization antibacterial action simultaneously.
Surfactant is for improving the storage stability of nano-sized carbon dispersion liquid.
The preparation method of nano-sized carbon multifunctional beverage provided by the invention, raw material comprises nano-sized carbon and water, nano-sized carbon is added to the water through grinding obtained nano-sized carbon slurry, then gets nano-sized carbon slurry preparation and enter in water, through sterilization process, nano-sized carbon content is 1 μ g ~ 100000 μ g/ml.
Preferably, the method specifically comprises the following steps:
S1: prepared by nano-sized carbon slurry:
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: get nano-sized carbon and be added to the water, gained slurry, after 2 ~ 12 hours, is carried out sand milling 2 ~ 12 hours by ball milling again, the nano-sized carbon slurry of obtained 50 ~ 170nm;
S2: prepared by beverage:
S21: get gained nano-sized carbon slurry in S1 and be added to the water, be stirred to liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 1 μ g ~ 100000 μ g/ml;
S22: sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, filling obtained nano-sized carbon multifunctional beverage finished product.
Preferably, the method also comprises step:
S211: add surfactant in S21 gained nano-sized carbon dispersion liquid, surfactant addition is 0g ~ 1g/ml.
Preferably, in described step S11, S21, sterilizing adopts steam sterilization.
What deserves to be explained is, in the present invention, sterilization process, except carrying out for raw material, instrument and equipment and step S21 gained nano-sized carbon dispersion liquid, also can enter overall sterilizing, to make sterilization effect more desirable to filling rear gained beverage product.
The invention has the beneficial effects as follows: nano-sized carbon multifunctional beverage provided by the invention, due to containing nano-sized carbon raw material, effectively can adsorb the remains of pesticide in alimentary canal and human body, bactericide, heavy metal, bioxin, various pathogenic bacteria and toxin thereof, damage harmful health or pathogenic refuse etc., the harmful substance such as creatinine, uric acid can also be adsorbed, there is the effect of cleaning intestines and stomach rubbish.This nano-sized carbon multifunctional beverage also has sterilization antibacterial action, and the action principle of nano-sized carbon is physical action, to the side effect of human body totally nontoxic.The preparation method of nano-sized carbon multifunctional beverage provided by the invention, simply workable, be easy to standardization, be worth popularization in the field of business.
Accompanying drawing explanation
Fig. 1 is preparation method's step schematic diagram of nano-sized carbon multifunctional beverage of the present invention.
Detailed description of the invention
In order to make the object, technical solutions and advantages of the present invention clearly, below in conjunction with specific embodiments and the drawings, the present invention is described in further detail.
As shown in Figure 1, preparation method's step schematic diagram of nano-sized carbon multifunctional beverage of the present invention, comprises the following steps:
Step S1: prepared by nano-sized carbon slurry:
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: get nano-sized carbon and be added to the water, gained slurry, after 2 ~ 12 hours, is carried out sand milling 2 ~ 12 hours by ball milling again, the nano-sized carbon slurry of obtained 50 ~ 170nm;
S13: detect absorbance;
S2: prepared by beverage:
S21: get gained nano-sized carbon slurry in S1 and be added to the water, be stirred to liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 1 μ g ~ 100000 μ g/ml;
S22: sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, filling obtained nano-sized carbon multifunctional beverage finished product;
S23: sampling Detection particle diameter, carbon content, content of beary metal and bacterial content;
S24: packaging warehouse-in.
What deserves to be explained is, the detection of step S13 absorbance, is the initial survey to nano-sized carbon content, in strict accordance with as calculated and because of add nano-sized carbon content carry out the preparation of nano-sized carbon slurry, also can not carry out the initial survey of this step.Sampling Detection particle diameter, carbon content, content of beary metal and bacterial content in step S23, be the quality in order to ensure product, whether whether it carry out, and is not the key point of preparation nano-sized carbon multifunctional beverage of the present invention and preparation method thereof.
Embodiment 1
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: measure carbon aerogels 1 ㎏, add in 100 ㎏ deionized waters, ball milling 2 hours, rotational speed of ball-mill is 200r/min, and the slurry after ball milling is carried out sand milling 2 ~ 12 hours again, sand milling rotating speed 800r/min, the nano-sized carbon aeroge slurry of obtained 170nm;
S13: detect absorbance;
S2: prepared by beverage:
S21: get gained nano-sized carbon aeroge slurry 1 ㎏ in S1, add in 500L ultra-pure water, dropping limit, limit is stirred, until liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 50 μ g/ml;
S22: steam sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, vapor (steam) temperature 121 DEG C, 30 minutes time, filling obtained nano-sized carbon multifunctional beverage finished product.
S23: sampling Detection particle diameter, carbon content, content of beary metal and bacterial content;
S24: packaging warehouse-in.
Embodiment 2
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: measure carbon aerogels 1 ㎏, add in 100 ㎏ deionized waters, ball milling 6 hours, rotational speed of ball-mill is 200r/min, and the slurry after ball milling is carried out sand milling 6 hours again, sand milling rotating speed 800r/min, the nano-sized carbon aeroge slurry of obtained 70nm;
S13: detect absorbance;
S2: prepared by beverage:
S21: get gained nano-sized carbon aeroge slurry 1 ㎏ in S1, add in 500L ultra-pure water, dropping limit, limit is stirred, until liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 50 μ g/ml;
S22: steam sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, vapor (steam) temperature 121 DEG C, 30 minutes time, filling obtained nano-sized carbon multifunctional beverage finished product.
S23: sampling Detection particle diameter, carbon content, content of beary metal and bacterial content;
S24: packaging warehouse-in.
Embodiment 3
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: measure carbon aerogels 1 ㎏, add in 100 ㎏ deionized waters, ball milling 12 hours, rotational speed of ball-mill is 200r/min, and the slurry after ball milling is carried out sand milling 12 hours again, sand milling rotating speed 800r/min, the nano-sized carbon aeroge slurry of obtained 50nm;
S13: detect absorbance;
S2: prepared by beverage:
S21: get gained nano-sized carbon aeroge slurry 1 ㎏ in S1, add in 500L ultra-pure water, dropping limit, limit is stirred, until liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 50 μ g/ml;
S22: steam sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, vapor (steam) temperature 121 DEG C, 30 minutes time, filling obtained nano-sized carbon multifunctional beverage finished product.
S23: sampling Detection particle diameter, carbon content, content of beary metal and bacterial content;
S24: packaging warehouse-in.
To the nano-sized carbon multifunctional beverage obtained by above-described embodiment 1 ~ 3, carry out the detection of granularity, carbon content, absorbance, content of beary metal and bacterial content, the results are shown in following table:
| Granularity (nm) | Carbon content (μ g/ml) | Absorbance | Lead, cadmium, and mercury arsenic total amount | Bacteria total amount | |
| Embodiment 1 | 170 | 50 | 1.04A | Do not detect | Do not detect |
| Embodiment 2 | 70 | 50 | 1.01A | Do not detect | Do not detect |
| Embodiment 3 | 55 | 50 | 0.97A | Do not detect | Do not detect |
To the nano-sized carbon multifunctional beverage obtained by above-described embodiment 1 ~ 3, antibacterial experiment is carried out according to standard " QB/T2591-2003 antibiotic plastic-Anti-microbial Performance Tests method and antibacterial effect ", adopt experimental strain: Escherichia coli, staphylococcus aureus and helicobacter pylori, the results are shown in following table:
The nano-sized carbon multifunctional beverage obtained to embodiment 3 carries out clinical trial, adopt case: habitual enteritis, hydrochloric acid in gastric juice (gastritis) and halitosis, each case 100 people, age is uniformly distributed between 20 ~ 60 years old, and men and women is 50 people respectively, drink nano-sized carbon multifunctional beverage of the present invention continuous March, 10ml/ props up, every day three, monthly check once, the results are shown in following table:
Nano-sized carbon multifunctional beverage provided by the invention, containing nano-sized carbon raw material, effectively can adsorb the remains of pesticide in alimentary canal and human body, bactericide, heavy metal, bioxin, various pathogenic bacteria and toxin thereof, damage harmful health or pathogenic refuse etc., the harmful substance such as creatinine, uric acid can also be adsorbed, there is the effect of cleaning intestines and stomach rubbish.This nano-sized carbon multifunctional beverage also has sterilization antibacterial action.Can intuitively be learnt by above-mentioned antibacterial experiment and case experimental result, nano-sized carbon multifunctional beverage provided by the invention, has good antibacterial effect, has effective healing ability to gastrointestinal disease simultaneously.The action principle of nano-sized carbon is physical action, and therefore this nano-sized carbon multifunctional beverage is to the side effect of human body totally nontoxic.Further, the preparation method of nano-sized carbon multifunctional beverage provided by the invention, simply workable, be easy to standardization, be worth popularization in the field of business.
Those of ordinary skill in the art will appreciate that, embodiment described here is to help reader understanding's principle of the present invention, should be understood to that protection scope of the present invention is not limited to so special statement and embodiment.Those of ordinary skill in the art can make various other various concrete distortion and combination of not departing from essence of the present invention according to these technology enlightenment disclosed by the invention, and these distortion and combination are still in protection scope of the present invention.
Claims (9)
1. a nano-sized carbon multifunctional beverage, is characterized in that: its raw material comprises nano-sized carbon and water, and be prepared from after grinding, allotment, sterilization process, wherein nano-sized carbon content is 1 μ g ~ 100000 μ g/ml.
2. nano-sized carbon multifunctional beverage according to claim 1, is characterized in that: described raw material also comprises surfactant, described surface-active contents is 0g ~ 1g/ml.
3. nano-sized carbon multifunctional beverage according to claim 2, is characterized in that: described surfactant comprise in anion surfactant, cationic surfactant and ionic surface active agent one or more.
4. nano-sized carbon multifunctional beverage according to claim 1, is characterized in that: described nano-sized carbon to comprise in active carbon, carbon black, CNT, microcrystalline carbon, carbon aerogels, Graphene monomer/mixture one or more.
5. nano-sized carbon multifunctional beverage according to claim 1, is characterized in that: described water is deionized water, distilled water, mineral water or one or more in purifying waste water.
6. the preparation method of the arbitrary described nano-sized carbon multifunctional beverage of Claims 1 to 5, it is characterized in that: raw material comprises nano-sized carbon and water, nano-sized carbon is added to the water through grinding obtained nano-sized carbon slurry, getting nano-sized carbon slurry preparation again enters in water, through sterilization process, nano-sized carbon content is 1 μ g ~ 100000 μ g/ml.
7. the preparation method of nano-sized carbon multifunctional beverage according to claim 6, is characterized in that: the method specifically comprises the following steps:
S1: prepared by nano-sized carbon slurry:
S11: washing and sterilizing process is carried out to raw material, instrument and equipment;
S12: get nano-sized carbon and be added to the water, gained slurry, after 2 ~ 12 hours, is carried out sand milling 2 ~ 12 hours by ball milling again, the nano-sized carbon slurry of obtained 50 ~ 170nm;
S2: prepared by beverage:
S21: get gained nano-sized carbon slurry in S1 and be added to the water, be stirred to liquid stable homogeneous, obtained nano-sized carbon content is the nano-sized carbon dispersion liquid of 1 μ g ~ 100000 μ g/ml;
S22: sterilizing is carried out to S21 gained nano-sized carbon dispersion liquid, filling obtained nano-sized carbon multifunctional beverage finished product.
8. the preparation method of nano-sized carbon multifunctional beverage according to claim 7, is characterized in that: the method also comprises step:
S211: add surfactant in S21 gained nano-sized carbon dispersion liquid, surfactant addition is 0g ~ 1g/ml.
9. the preparation method of nano-sized carbon multifunctional beverage according to claim 7, is characterized in that: in described step S11, S21, sterilizing adopts steam sterilization.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510907456.0A CN105325826A (en) | 2015-12-09 | 2015-12-09 | Multifunctional nanometer carbon drink and preparing method thereof |
| PCT/CN2016/078247 WO2017096735A1 (en) | 2015-12-09 | 2016-04-01 | Nanocarbon multifunctional beverage and preparation method therefor |
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| CN201510907456.0A CN105325826A (en) | 2015-12-09 | 2015-12-09 | Multifunctional nanometer carbon drink and preparing method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106036798A (en) * | 2016-06-20 | 2016-10-26 | 浙江旺林生物科技有限公司 | Application of micron-grade bamboo plant carbon black in xylitol |
| CN106072613A (en) * | 2016-06-20 | 2016-11-09 | 浙江旺林生物科技有限公司 | The money plant white carbon black application in Herba Hordei Vulgaris powder of a kind of micron order bamboo |
| CN106107962A (en) * | 2016-06-20 | 2016-11-16 | 浙江旺林生物科技有限公司 | The money plant white carbon black application in pine pollen tablets of a kind of micron order bamboo |
| WO2017096735A1 (en) * | 2015-12-09 | 2017-06-15 | 四川百草通科新材料科技有限公司 | Nanocarbon multifunctional beverage and preparation method therefor |
| CN107509851A (en) * | 2017-09-29 | 2017-12-26 | 杭州高烯科技有限公司 | A kind of graphene chewing gum and preparation method thereof |
| CN113073121A (en) * | 2021-04-06 | 2021-07-06 | 江苏南创化学与生命健康研究院有限公司 | Nano carbon material containing high-polymerization-degree polyphosphate and preparation method of high-polymerization-degree polyphosphate |
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| CN113769716B (en) * | 2021-07-05 | 2023-11-10 | 昆明理工大学 | Preparation method and application of novel rubber seed shell-based composite material |
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| WO2017096735A1 (en) * | 2015-12-09 | 2017-06-15 | 四川百草通科新材料科技有限公司 | Nanocarbon multifunctional beverage and preparation method therefor |
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| CN106107962A (en) * | 2016-06-20 | 2016-11-16 | 浙江旺林生物科技有限公司 | The money plant white carbon black application in pine pollen tablets of a kind of micron order bamboo |
| CN107509851A (en) * | 2017-09-29 | 2017-12-26 | 杭州高烯科技有限公司 | A kind of graphene chewing gum and preparation method thereof |
| CN113073121A (en) * | 2021-04-06 | 2021-07-06 | 江苏南创化学与生命健康研究院有限公司 | Nano carbon material containing high-polymerization-degree polyphosphate and preparation method of high-polymerization-degree polyphosphate |
| CN113073121B (en) * | 2021-04-06 | 2023-05-05 | 江苏南创化学与生命健康研究院有限公司 | Nanocarbon material containing high-polymerization-degree polyphosphate and preparation method of high-polymerization-degree polyphosphate |
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| Publication number | Publication date |
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| WO2017096735A1 (en) | 2017-06-15 |
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Application publication date: 20160217 |