CN105154228A - Plant flavone essence cigarette bead for cigarette and preparation method thereof - Google Patents

Plant flavone essence cigarette bead for cigarette and preparation method thereof Download PDF

Info

Publication number
CN105154228A
CN105154228A CN201510337696.1A CN201510337696A CN105154228A CN 105154228 A CN105154228 A CN 105154228A CN 201510337696 A CN201510337696 A CN 201510337696A CN 105154228 A CN105154228 A CN 105154228A
Authority
CN
China
Prior art keywords
cigarette
plant flavone
flavone essence
essence
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510337696.1A
Other languages
Chinese (zh)
Other versions
CN105154228B (en
Inventor
宋旭艳
黄龙
魏敏
陈义坤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Huanghelou Science and Technology Park Group Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Huanghelou Science and Technology Park Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd, Huanghelou Science and Technology Park Group Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN201510337696.1A priority Critical patent/CN105154228B/en
Publication of CN105154228A publication Critical patent/CN105154228A/en
Application granted granted Critical
Publication of CN105154228B publication Critical patent/CN105154228B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses a plant flavone essence cigarette bead for a cigarette and a preparation method. The preparation method comprises the following steps: weighing an adhesive accounting for 0.1 to 1% of the weight of plant flavone essence; dissolving the adhesive with water, then adding dissolved adhesive into the plant flavone essence and carrying out uniform mixing through stirring so as to prepare a soft material; extruding the obtained soft material with an extruder to obtain an elongated strip-like material; then rounding the material with a rounding machine; and carrying out drying so as to obtain the plant flavone essence cigarette bead. The plant flavone essence comprises, by weight, 40 to 70% of catechin, 10 to 30% of luteolin, 10 to 30% of hesperetin and 5 to 20% of kaempferol. The plant flavone essence cigarette bead has substantial advantages in reduction of phenol in smoke, wherein the reduction rate of phenol can reach 15 to 45%, and the reduction rate of free radicals is 8 to 25%. The plant flavone essence cigarette bead has excellent natural smell and brings comfortable aromatic smell to a cigarette; and when one smokes the cigarette, other harmful substances in smoke can be reduced to a certain extent.

Description

Cigarette is with plant flavone essence cigarette pearl and preparation method thereof
Technical field
The invention belongs to technical field of cigarettes, be specifically related to a kind of cigarette plant flavone essence cigarette pearl and preparation method thereof.
Background technology
Natural phant is widely used in tobacco aromatics using, is much wherein containing Flavonoid substances.According to the molecular characterization of Flavonoid substances and the power of interelectric reactive force, preliminary study finds that such material can produce furans and derivative thereof after burning cracking, these materials are the main aroma components in flue gas, camerlsed, fragrant and sweet, roasting perfume can be brought to flue gas, increase perfume quantity and aroma quality.Therefore, in the allotment of essence spice for cigarette, the use of a lot of flavonoid perfume material is had.
Much research also shows, flavonoid compound has multiple biological activity, except utilizing that it is antibacterial, anti-inflammatory, anti-mutation, step-down, except the effect such as clearing heat and detoxicating, calm, diuresis, in anti-oxidant, anticancer, anti-cancer, suppresses also have unusual effect in lipase etc.It is the scavenging agent of most of oxyradical, thus can the vigor of increased SOD (superoxide dismutase), reduces the generation of MDA (malondialdehyde) and OX-LDL (Ox LDL).It can increase coronary flow, has antagonistic action to Myocardial Infarction; Provide protection is had to acute myocardial ischemia; Unusual effect is had to treatment coronary heart diseases and angina pectoris, hypertension etc.; To reduction diastolic pressure, prevent and treat irregular pulse, cardiovascular diseases and promoting blood circulation and removing blood stasisly also to play an important role.
Phenolic compound is the common compounds of occurring in nature, has the existence of phenolic compound in water, fuel, vehicle exhaust, air, wine and cigarette smoke.The phenolic compounds in cigarette smoke reported has kind more than 50, and wherein topmost phenolic compound comprises 7 kinds of compositions such as phenol, catechol, Resorcinol, Resorcinol, o, m, p-cresols.
Phenolic compound can by directly entering blood circulation with the contact of skin, mucous membrane, causes protein denaturation, cytoclasis losing vigor.And induced by alkyl hydroxybenzene has endocrine disrupting activity, impact, be called as phenols environmental estrogens to Mammals and hydrobiological reproductive development, part phenols component has genotoxicity and carcinogenic or promotion mutagenesis.Above 7 kinds of phenols components are all put in EPA objectionable constituent list, and catechol is classified as the carcinogenic components of 2B level by IARC.State Bureau's key research project " the cigarette hazardness Research on Index System " project that Zhengzhou tobacco research institute bears, by studying the relation of objectionable constituent burst size and flue gas biologic activity, finds that phenol affects one of topmost objectionable constituent of cigarette mainstream flue gas hazardness.
At present, what the method reducing phenol in flue gas mainly adopted is the method for adsorbing, because phenol is present in the granule phase substance of flue gas, can be retained down by the method for physical adsorption from flue gas.The sorbent material of prior art application is mainly the larger porous material of surface-area, while absorption, retaining phenol, also can adsorb aroma component and the flue gas moisture of part in flue gas, cause during cigarette smoking, easily producing stimulation, perfume quantity is not enough, aroma quality declines, and has a strong impact on cigarette smoking quality.
In prior art, the cigarette pearl containing essence and flavoring agent is put into filter tip, this cigarette pearl can make cigarette more raw fragrant in aspiration procedure, and strengthening fragrance or characteristic, make smoker obtain more comfortable experience.This cigarette pearl can only simply make cigarette raw fragrant in aspiration procedure, can not play the objectionable impurities produced when reducing smoking cigarette.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of antioxygenation that utilizes and block cigarette plant flavone essence cigarette pearl of phenol generation and preparation method thereof, reach the effect reducing phenol in smoke.
The present invention solves the problems of the technologies described above adopted technical scheme: the preparation method providing a kind of cigarette plant flavone essence cigarette pearl, and described preparation method is as follows:
Take the tackiness agent that weight is plant flavone essence weight 0.1% ~ 1%, join in plant flavone essence after tackiness agent water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, obtain the plant flavone essence cigarette pearl that particle size range is 0.5mm ~ 4mm, bulk density is 1.2g/ml ~ 1.8g/ml after drying;
Wherein: the weight percentages of components of described plant flavone essence is as follows:
Further, the DNA purity of described catechin, luteolin, Hesperitin and kaempferol is 80 ~ 95%.
Further, described tackiness agent is one or more in polyvidone, hydroxypropylcellulose, Vltra tears and carboxymethyl cellulose.
Further, the particle size range of described cigarette pearl is 0.8mm ~ 1.5mm, and bulk density is 1.4g/ml ~ 1.6g/ml.
Further, described drying is under temperature is 60 DEG C ~ 80 DEG C conditions dry 4 ~ 6 hours.
A kind of cigarette is with plant flavone essence cigarette pearl, and described plant flavone essence cigarette pearl is plant flavone essence cigarette pearl prepared by method described above.
Analyze according to organic chemistry basic theories, to affect in the oxidation resistant factor of flavonoid compound most importantly degree of hydroxylation and hydroxy position, phenolic hydroxyl group is the chief active group of flavonoid compound antioxygenation, find that the hydroxyl activity difference on each ring of flavonoid is larger simultaneously, be mainly manifested in: B ring is the chief active position of flavonoid compound oxidation and removing free radicals, when this ring exists ortho-phenolic hydroxyl structure, anti-oxidant activity greatly strengthens; When on c ring, hydroxyl is connected with unsaturated double-bond, c ring also has stronger anti-oxidant activity; The phenolic hydroxyl group of A ring is the most weak.Phenolic hydroxyl group in flavones structure has for hydrogen activity, hydrogen atom can be supplied to active oxygen radical, form stable SA Phenoxy radical, thus avoids these active oxygen radicals to produce phenolic compound to the attack of aromatic nucleus.Phenolic hydroxyl group number in flavones molecule is more, the available hydrogen atom in order to be combined with living radical is more, therefore, flavonoid compound can utilize antioxygenation to block the generation of phenol, thus has the effect reducing phenol release amount in flue gas preferably.
The present invention has the following advantages:
1, plant flavone essence cigarette pearl of the present invention has significant advantage in reduction phenol in smoke, and phenol reduced rate can reach 15 ~ 45%, free radical reduced rate is 8 ~ 25%, natural, environmental protection, meets human consumer to requirement that is healthy, low evil;
2, plant flavone essence cigarette pearl of the present invention has excellent natural breath, comfortable perfume of smelling is brought to feel to cigarette, during cigarette suction, also certain reducing effect can be produced to other objectionable impurities in flue gas, and can not have a negative impact to cigarette smoking quality, improve cigarette smoking quality further;
3, plant flavone flavor of raw material wide material sources of the present invention, with low cost, easy to utilize.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Specific embodiment described herein only in order to explain the present invention, is not intended to limit the present invention.
Embodiment 1
By plant flavone essence according to ratio mixing in table 1, take the Vltra tears tackiness agent that weight is plant flavone essence weight 0.1%, with joining in plant flavone essence after 400ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 0.5mm, bulk density is 1.8g/ml after dry 6 hours under temperature is 60 DEG C of conditions.
Table 1
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 40% 15% 25% 20%
Embodiment 2
By plant flavone essence according to ratio mixing in table 2, take the Vltra tears tackiness agent that weight is plant flavone essence weight 0.5%, with joining in plant flavone essence after 450ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 0.8mm, bulk density is 1.6g/ml after dry 5.5 hours under temperature is 65 DEG C of conditions.
Table 2
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 50% 15% 15% 20%
Embodiment 3
By plant flavone essence according to ratio mixing in table 3, take the carboxymethyl cellulose binder that weight is plant flavone essence weight 0.8%, with joining in plant flavone essence after 500ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 1.0mm, bulk density is 1.6g/ml after dry 6 hours under temperature is 70 DEG C of conditions.
Table 3
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 60% 20% 10% 10%
Embodiment 4
By plant flavone essence according to ratio mixing in table 4, take the carboxymethyl cellulose binder that weight is plant flavone essence weight 0.8%, with joining in plant flavone essence after 500ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 6 hours under temperature is 75 DEG C of conditions.
Table 4
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 65% 15% 10% 10%
Embodiment 5
By plant flavone essence according to ratio mixing in table 5, take the hydroxypropylcellulose tackiness agent that weight is plant flavone essence weight 1%, with joining in plant flavone essence after 550ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 5 hours under temperature is 70 DEG C of conditions.
Table 5
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 60% 20% 15% 5%
Embodiment 6
By plant flavone essence according to ratio mixing in table 6, take the hydroxypropylcellulose tackiness agent that weight is plant flavone essence weight 1%, with joining in plant flavone essence after 550ml water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, upper fluidized-bed obtains the plant flavone essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 4 hours under temperature is 80 DEG C of conditions.
Table 6
Flavones kind Catechin Luteolin Hesperitin Kaempferol
Weight percent 50% 25% 15% 10%
Plant flavone essence cigarette pearl prepared in above 6 embodiments is joined in cigarette filter stick, then detection of exhaust gas compositions is carried out to the cigarette made, and carry out phenol reduced rate and compare, specifically see the following form 7
Table 7
The smoke components of main reduction has phenol, crotonic aldehyde, free radical, and smoke hazard index is also on a declining curve simultaneously, and concrete reduced rate the results are shown in following table 8
Table 8
Sample number into spectrum Phenol Crotonic aldehyde Index Free radical
Embodiment 1 14.7% 13.5% 14.1% 9.2%
Embodiment 2 20.2% 15.5% 12.8% 13.3%
Embodiment 3 30.2% 12.8% 15.4% 16.4%
Embodiment 4 36.4% 32.4% 19.2% 21.1%
Embodiment 5 41.9% 29.1% 17.9% 20.7%
Embodiment 6 39.5% 28.4% 15.4% 22.2%
Join in cigarette filter stick by plant flavone essence cigarette pearl prepared in above 6 embodiments, then carry out sensory evaluation to the cigarette made, result is as table 9
Table 9
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.

Claims (6)

1. a cigarette preparation method for plant flavone essence cigarette pearl, is characterized in that: described preparation method is as follows:
Take the tackiness agent that weight is plant flavone essence weight 0.1% ~ 1%, join in plant flavone essence after tackiness agent water dissolution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by forcing machine, then round as a ball by spheronizator, obtain the plant flavone essence cigarette pearl that particle size range is 0.5mm ~ 4mm, bulk density is 1.2g/ml ~ 1.8g/ml after drying;
Wherein: the weight percentages of components of described plant flavone essence is as follows:
2. the preparation method of cigarette plant flavone essence cigarette pearl according to claim 1, is characterized in that: the DNA purity of described catechin, luteolin, Hesperitin and kaempferol is 80 ~ 95%.
3. the preparation method of cigarette plant flavone essence cigarette pearl according to claim 1, is characterized in that: described tackiness agent is one or more in polyvidone, hydroxypropylcellulose, Vltra tears and carboxymethyl cellulose.
4. the cigarette preparation method of plant flavone essence cigarette pearl according to claim 1 or 2 or 3, is characterized in that: the particle size range of described cigarette pearl is 0.8mm ~ 1.5mm, and bulk density is 1.4g/ml ~ 1.6g/ml.
5. the cigarette preparation method of plant flavone essence cigarette pearl according to claim 1 or 2 or 3, is characterized in that: described drying is under temperature is 60 DEG C ~ 80 DEG C conditions dry 4 ~ 6 hours.
6. cigarette is with a plant flavone essence cigarette pearl, it is characterized in that: the plant flavone essence cigarette pearl that described plant flavone essence cigarette pearl is prepared for method described in claim 1.
CN201510337696.1A 2015-06-17 2015-06-17 Cigarette is with plant flavone essence cigarette pearl and preparation method thereof Active CN105154228B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510337696.1A CN105154228B (en) 2015-06-17 2015-06-17 Cigarette is with plant flavone essence cigarette pearl and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510337696.1A CN105154228B (en) 2015-06-17 2015-06-17 Cigarette is with plant flavone essence cigarette pearl and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105154228A true CN105154228A (en) 2015-12-16
CN105154228B CN105154228B (en) 2018-07-03

Family

ID=54795282

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510337696.1A Active CN105154228B (en) 2015-06-17 2015-06-17 Cigarette is with plant flavone essence cigarette pearl and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105154228B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106136194A (en) * 2016-06-28 2016-11-23 天津春发生物科技集团有限公司 A kind of natural compound freshening seasoning and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101016288A (en) * 2007-03-06 2007-08-15 川渝中烟工业公司 Method of stabilizing bioactivity of flavones substance
CN101653290A (en) * 2009-08-26 2010-02-24 甘全军 Cigarette containing rosmarinic acid and preparation method thereof
CN101864694A (en) * 2010-06-13 2010-10-20 玉溪市星源油墨厂 Tea flavonoids containing water-based coating for cigarette plug wrap paper
CN102061174A (en) * 2010-10-29 2011-05-18 华南农业大学 Squalene and tea polyphenol composition and application thereof in cigarettes
CN104068467A (en) * 2014-07-01 2014-10-01 安徽中烟工业有限责任公司 Electronic cigarette liquid rich in plant flavone

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101016288A (en) * 2007-03-06 2007-08-15 川渝中烟工业公司 Method of stabilizing bioactivity of flavones substance
CN101653290A (en) * 2009-08-26 2010-02-24 甘全军 Cigarette containing rosmarinic acid and preparation method thereof
CN101864694A (en) * 2010-06-13 2010-10-20 玉溪市星源油墨厂 Tea flavonoids containing water-based coating for cigarette plug wrap paper
CN102061174A (en) * 2010-10-29 2011-05-18 华南农业大学 Squalene and tea polyphenol composition and application thereof in cigarettes
CN104068467A (en) * 2014-07-01 2014-10-01 安徽中烟工业有限责任公司 Electronic cigarette liquid rich in plant flavone

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106136194A (en) * 2016-06-28 2016-11-23 天津春发生物科技集团有限公司 A kind of natural compound freshening seasoning and preparation method thereof

Also Published As

Publication number Publication date
CN105154228B (en) 2018-07-03

Similar Documents

Publication Publication Date Title
CN101138432B (en) Cigarette containing Chinese medicinal herb additive agent and method of producing the same
KR20140004754A (en) Smoking articles
CN105167190A (en) Finely cut tobacco leaves with flavone essence for cigarettes and method for preparing finely cut tobacco leaves
CN105167191A (en) Finely cut tobacco leaves with flavonoid compound essence for cigarettes and method for preparing finely cut tobacco leaves
CN101947435A (en) Chitosan polycation additive for reducing phenols in cigarette smoke
CN109852476A (en) A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application
CN101141891B (en) Instant tip rod appended solution when sucking cigarette and producing method and application
CN105996122A (en) Cigarette filter stick for reducing cigarette aldehyde substances
CN109174004A (en) A kind of active carbon that improves is to the method and application of essence sustained release performance
CN103141940A (en) Entrapment agent for selectively lowering crotonaldehyde content in cigarette smoke and filter stick
CN105154228A (en) Plant flavone essence cigarette bead for cigarette and preparation method thereof
CN103829372B (en) For reducing additive of Blausure (German) and preparation method and application in cigarette smoke
CN105154227A (en) Plant flavone essence cigarette bead for cigarette, and preparation method and application thereof
CN101642286A (en) Filtering agent for harmful gas in cigarette, production method thereof and application thereof
CN105167194B (en) Cigarette mouth stick and preparation method thereof of the essence containing plant flavone
CN105124759B (en) Cigarette mouth stick and preparation method thereof of the essence containing flavone compound
CN110403236B (en) Cigarette dry bead filter rod with function of improving smoke permeation
CN100512689C (en) Additive for lowering tar and free radical content in cigarette smoke and its adding method
CN103859590B (en) CO and the additive of cigarette filter stick of releasing content of coke tar and preparation method and application in main flume can be reduced simultaneously
CN103271440B (en) Cigarette purifying and harm-reducing reagent and particles and preparation method of cigarette and particles
CN105962413A (en) Cigarette filter stick achieving stable aroma
CN105901764A (en) Cigarette filter stick for improving cigarette smoking quality
CN105749883A (en) Adsorbent for adsorbing harmful substances in cigarette smoke
CN104705783A (en) Filter tip additive material capable of improving sensory characteristics of smoke and application thereof
CN103222683B (en) Cigarette filter rod provided with natural mineral and plant fiber composite additive

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant