CN105167190A - Finely cut tobacco leaves with flavone essence for cigarettes and method for preparing finely cut tobacco leaves - Google Patents
Finely cut tobacco leaves with flavone essence for cigarettes and method for preparing finely cut tobacco leaves Download PDFInfo
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- CN105167190A CN105167190A CN201510336913.5A CN201510336913A CN105167190A CN 105167190 A CN105167190 A CN 105167190A CN 201510336913 A CN201510336913 A CN 201510336913A CN 105167190 A CN105167190 A CN 105167190A
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- cigarette
- essence
- flavones
- flavones essence
- tobacco leaves
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- 229930003944 flavone Natural products 0.000 title claims abstract description 73
- 235000011949 flavones Nutrition 0.000 title claims abstract description 73
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 65
- 238000000034 method Methods 0.000 title claims abstract description 11
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title abstract description 15
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title abstract description 14
- 241000208125 Nicotiana Species 0.000 title abstract description 9
- 235000002637 Nicotiana tabacum Nutrition 0.000 title abstract description 9
- 150000002212 flavone derivatives Chemical class 0.000 title abstract 9
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000000853 adhesive Substances 0.000 claims abstract description 15
- 230000001070 adhesive effect Effects 0.000 claims abstract description 15
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims abstract description 10
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 claims abstract description 9
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 claims abstract description 9
- QUQPHWDTPGMPEX-UTWYECKDSA-N aurantiamarin Natural products COc1ccc(cc1O)[C@H]1CC(=O)c2c(O)cc(O[C@@H]3O[C@H](CO[C@@H]4O[C@@H](C)[C@H](O)[C@@H](O)[C@H]4O)[C@@H](O)[C@H](O)[C@H]3O)cc2O1 QUQPHWDTPGMPEX-UTWYECKDSA-N 0.000 claims abstract description 9
- 229960001285 quercetin Drugs 0.000 claims abstract description 9
- 235000005875 quercetin Nutrition 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 5
- 150000002213 flavones Chemical class 0.000 claims description 59
- 239000011122 softwood Substances 0.000 claims description 16
- 238000002360 preparation method Methods 0.000 claims description 11
- 239000002245 particle Substances 0.000 claims description 10
- XDQITMCFPPPMBC-TUANDBMESA-N scutelloside Natural products OC[C@H]1O[C@@H](O[C@@H]2O[C@@H]3C[C@H]4[C@H](O)[C@@H](O)[C@@](O)(CO3)[C@@H]24)[C@H](O)[C@@H](O)[C@@H]1O XDQITMCFPPPMBC-TUANDBMESA-N 0.000 claims description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 4
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 4
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 4
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 4
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims description 4
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 4
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 4
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 4
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 4
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 4
- 238000005304 joining Methods 0.000 claims description 2
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- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 35
- 239000000779 smoke Substances 0.000 abstract description 7
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- 239000007779 soft material Substances 0.000 abstract 4
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 abstract 1
- QUQPHWDTPGMPEX-UHFFFAOYSA-N Hesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(COC4C(C(O)C(O)C(C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-UHFFFAOYSA-N 0.000 abstract 1
- IPQKDIRUZHOIOM-UHFFFAOYSA-N Oroxin A Natural products OC1C(O)C(O)C(CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IPQKDIRUZHOIOM-UHFFFAOYSA-N 0.000 abstract 1
- IKIIZLYTISPENI-ZFORQUDYSA-N baicalin Chemical compound O1[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 IKIIZLYTISPENI-ZFORQUDYSA-N 0.000 abstract 1
- 229960003321 baicalin Drugs 0.000 abstract 1
- AQHDANHUMGXSJZ-UHFFFAOYSA-N baicalin Natural products OC1C(O)C(C(O)CO)OC1OC(C(=C1O)O)=CC2=C1C(=O)C=C(C=1C=CC=CC=1)O2 AQHDANHUMGXSJZ-UHFFFAOYSA-N 0.000 abstract 1
- APSNPMVGBGZYAJ-GLOOOPAXSA-N clematine Natural products COc1cc(ccc1O)[C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2 APSNPMVGBGZYAJ-GLOOOPAXSA-N 0.000 abstract 1
- 229940025878 hesperidin Drugs 0.000 abstract 1
- VUYDGVRIQRPHFX-UHFFFAOYSA-N hesperidin Natural products COc1cc(ccc1O)C2CC(=O)c3c(O)cc(OC4OC(COC5OC(O)C(O)C(O)C5O)C(O)C(O)C4O)cc3O2 VUYDGVRIQRPHFX-UHFFFAOYSA-N 0.000 abstract 1
- QUQPHWDTPGMPEX-QJBIFVCTSA-N hesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]4[C@@H]([C@H](O)[C@@H](O)[C@H](C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-QJBIFVCTSA-N 0.000 abstract 1
- LRDGATPGVJTWLJ-UHFFFAOYSA-N luteolin Natural products OC1=CC(O)=CC(C=2OC3=CC(O)=CC(O)=C3C(=O)C=2)=C1 LRDGATPGVJTWLJ-UHFFFAOYSA-N 0.000 abstract 1
- 235000009498 luteolin Nutrition 0.000 abstract 1
- IQPNAANSBPBGFQ-UHFFFAOYSA-N luteolin Chemical compound C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C(O)=C1 IQPNAANSBPBGFQ-UHFFFAOYSA-N 0.000 abstract 1
- ARGKVCXINMKCAZ-UHFFFAOYSA-N neohesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(CO)O3)OC3C(C(O)C(O)C(C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 229960003742 phenol Drugs 0.000 description 15
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 10
- -1 flavone compound Chemical class 0.000 description 10
- 239000003546 flue gas Substances 0.000 description 10
- 150000002989 phenols Chemical class 0.000 description 9
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- 230000003064 anti-oxidating effect Effects 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 4
- 229930003935 flavonoid Natural products 0.000 description 4
- 150000002215 flavonoids Chemical class 0.000 description 4
- 235000017173 flavonoids Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 235000013824 polyphenols Nutrition 0.000 description 4
- 150000003254 radicals Chemical class 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 2
- 102000019197 Superoxide Dismutase Human genes 0.000 description 2
- 108010012715 Superoxide dismutase Proteins 0.000 description 2
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- MLUCVPSAIODCQM-NSCUHMNNSA-N crotonaldehyde Chemical compound C\C=C\C=O MLUCVPSAIODCQM-NSCUHMNNSA-N 0.000 description 2
- MLUCVPSAIODCQM-UHFFFAOYSA-N crotonaldehyde Natural products CC=CC=O MLUCVPSAIODCQM-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
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- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
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Abstract
The invention discloses finely cut tobacco leaves with flavone essence for cigarettes and a method for preparing the finely cut tobacco leaves. The method includes the steps of weighing adhesive with the weight of 0.1%-1% of the weight of the flavone essence; dissolving the adhesive in water and then adding the dissolved adhesive into the flavone essence; uniformly stirring the dissolved adhesive and the flavone essence to obtain soft materials; extruding the soft materials in an extruding machine into strip shape and then rounding the strip shaped soft materials in a rounder; drying the rounded soft materials to obtain the finely cut tobacco leaves with the flavone essence. The flavone essence comprises, by weight, 30%-60% of luteolin, 15%-40% of baicalin, 15%-40% of quercetin and 10%-25% of hesperidin. The finely cut tobacco leaves with the flavone essence and the method have the advantages that the finely cut tobacco leaves have obvious merits in the aspect of reducing phenol in smoke, and the phenol reduction rate can reach 15-45%; the plant flavone essence has excellent natural smell and can be added to a cigarette holder, so that the cigarettes can have unique and strong extra aroma.
Description
Technical field
The invention belongs to technical field of cigarettes, be specifically related to a kind of cigarette flavones essence cigarette pearl and preparation method thereof.
Background technology
Natural plants is widely used in tobacco aromatics, is much wherein containing Flavonoid substances.According to the molecular characterization of Flavonoid substances and the power of interelectric active force, Primary Study finds that such material can produce furans and derivative thereof after burning cracking, these materials are the main aroma components in flue gas, camerlsed, fragrant and sweet, roasting perfume can be brought to flue gas, increase perfume quantity and aroma quality.Therefore, in the allotment of essence spice for cigarette, the use of a lot of flavonoids perfume material is had.
Much research also shows, flavone compound has multiple biologically active, except utilizing that it is antibacterial, anti-inflammatory, anti-sudden change, step-down, except the effect such as clearing heat and detoxicating, calm, diuresis, in anti-oxidant, anticancer, anti-cancer, suppresses also have remarkable result in lipase etc.It is the scavenger of most of oxygen radical, thus can the vigor of increased SOD (superoxide dismutase), reduces the generation of MDA (malondialdehyde) and OX-LDL (OxLDL ELISA).It can increase coronary flow, has antagonism to Myocardial Infarction; Protective effect is had to acute myocardial ischemia; Remarkable result is had to treatment coronary heart diseases and angina pectoris, hypertension etc.; To reduction diastolic pressure, prevent and treat arrhythmia cordis, cardiovascular disease and promoting blood circulation and removing blood stasisly also to play an important role.
Phenolic compound is the common compounds of occurring in nature, has the existence of phenolic compound in water, fuel, vehicle exhaust, air, wine and cigarette smoke.The phenolic compounds in cigarette smoke reported has kind more than 50, and wherein topmost phenolic compound comprises 7 kinds of compositions such as phenol, catechol, resorcinol, hydroquinones, o, m, p-cresols.
Phenolic compound can by directly entering blood circulation with the contact of skin, mucous membrane, causes protein denaturation, cytoclasis losing vigor.And induced by alkyl hydroxybenzene has endocrine disrupting activity, impact, be called as phenols environmental estrogens to mammal and hydrobiological reproductive development, part phenols component has genotoxicity and carcinogenic or promotion mutagenesis.Above 7 kinds of phenols components are all put in EPA harmful components list, and catechol is classified as the carcinogenic components of 2B level by IARC.State Bureau's key research project " the cigarette harmfulness Research on Index System " project that Zhengzhou tobacco research institute bears, by studying the relation of harmful components burst size and flue gas BA, finds that phenol affects one of topmost harmful components of cigarette mainstream flue gas harmfulness.
At present, what the method reducing phenol in flue gas mainly adopted is the method for adsorbing, because phenol is present in the granule phase substance of flue gas, can be retained down by the method for physical absorption from flue gas.The adsorbent of prior art application is mainly the larger porous material of surface area, while absorption, retaining phenol, also can adsorb aroma component and the flue gas moisture of part in flue gas, cause during cigarette smoking, easily producing stimulation, perfume quantity is not enough, aroma quality declines, and has a strong impact on cigarette smoking quality.
In prior art, the cigarette pearl containing essence and flavoring agent is put into filter tip, this cigarette pearl can make cigarette more raw fragrant in aspiration procedure, and strengthening fragrance or characteristic, make smoker obtain more comfortable experience.This cigarette pearl can only simply make cigarette raw fragrant in aspiration procedure, can not play the harmful substance produced when reducing smoking cigarette.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of antioxidation that utilizes and block cigarette flavones essence cigarette pearl of phenol generation and preparation method thereof, reach the effect reducing phenol in smoke.
The present invention solves the problems of the technologies described above adopted technical scheme: the preparation method providing cigarette flavones essence cigarette pearl, and described preparation method is as follows:
Take the adhesive that weight is flavones essence weight 0.1% ~ 1%, adhesive is with joining in flavones essence after water-soluble solution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, obtain the flavones essence cigarette pearl that particle size range is 0.5mm ~ 4mm, bulk density is 1.2g/ml ~ 1.8g/ml after drying;
Wherein: the weight percentages of components of described flavones essence is as follows:
Further, the DNA purity of described cyanidenon, scutelloside, Quercetin and aurantiamarin is 80 ~ 95%.
Further, described adhesive is one or more in PVP, hydroxypropyl cellulose, hydroxypropyl methylcellulose and carboxymethyl cellulose.These adhesives are adopted not only to be convenient to cigarette pearl shaping and do not affect judging parameter.
Further, the particle size range of described cigarette pearl is 0.8mm ~ 1.5mm, and bulk density is 1.4g/ml ~ 1.6g/ml.
Further, described drying is under temperature is 60 DEG C ~ 80 DEG C conditions dry 4 ~ 6 hours.
A kind of cigarette is with flavones essence cigarette pearl, and described flavones essence cigarette pearl is flavones essence cigarette pearl prepared by method described above.
Analyze according to organic chemistry basic theories, to affect in the oxidation resistant factor of flavone compound most importantly degree of hydroxylation and hydroxy position, phenolic hydroxyl group is the chief active group of flavone compound antioxidation, find that the hydroxyl activity difference on each ring of flavonoids is larger simultaneously, be mainly manifested in: B ring is the chief active position of flavone compound oxidation and removing free radicals, when this ring exists ortho-phenolic hydroxyl structure, antioxidation activity greatly strengthens; When on c ring, hydroxyl is connected with unsaturated double-bond, c ring also has stronger antioxidation activity; The phenolic hydroxyl group of A ring is the most weak.Phenolic hydroxyl group in flavones structure has for hydrogen activity, hydrogen atom can be supplied to active oxygen radical, form stable SA Phenoxy radical, thus avoids these active oxygen radicals to produce phenolic compound to the attack of aromatic rings.Phenolic hydroxyl group number in flavones molecule is more, the available hydrogen atom in order to be combined with living radical is more, therefore, flavone compound can utilize antioxidation to block the generation of phenol, thus has the effect reducing phenol release amount in flue gas preferably.
The present invention has the following advantages:
1, flavones essence cigarette pearl of the present invention has significant advantage in reduction phenol in smoke, and phenol reduced rate can reach 15 ~ 45%, natural, environmental protection, meets consumer to requirement that is healthy, low evil;
2, flavones essence of the present invention has excellent natural breath, be added on cigarette filter tip position, uniqueness, strong additional fragrance can be brought to cigarette, and not participate in cigarette burning, thus can not produce new undesirable substance because of cracking, meet consumer to requirement that is healthy, low evil;
3, flavones flavor of raw material wide material sources of the present invention, with low cost, easy to utilize.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Specific embodiment described herein only in order to explain the present invention, is not intended to limit the present invention.
Embodiment 1
By flavones essence according to ratio mixing in table 1, take the hydroxypropyl methylcellulose adhesive that weight is flavones essence weight 0.1%, join in flavones essence with after the water-soluble solution of 400ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 0.5mm, bulk density is 1.8g/ml after dry 6 hours under temperature is 60 DEG C of conditions.
Table 1
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 30％ | 25％ | 30％ | 15％ |
Embodiment 2
By flavones essence according to ratio mixing in table 2, take the hydroxypropyl methylcellulose adhesive that weight is flavones essence weight 0.5%, join in flavones essence with after the water-soluble solution of 450ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 0.8mm, bulk density is 1.6g/ml after dry 5.5 hours under temperature is 65 DEG C of conditions.
Table 2
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 40％ | 25％ | 30％ | 15％ |
Embodiment 3
By flavones essence according to ratio mixing in table 3, take the carboxymethyl cellulose binder that weight is flavones essence weight 0.8%, join in flavones essence with after the water-soluble solution of 500ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 1.0mm, bulk density is 1.6g/ml after dry 6 hours under temperature is 70 DEG C of conditions.
Table 3
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 50％ | 20％ | 20％ | 10％ |
Embodiment 4
By flavones essence according to ratio mixing in table 4, take the carboxymethyl cellulose binder that weight is flavones essence weight 0.8%, join in flavones essence with after the water-soluble solution of 500ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 6 hours under temperature is 75 DEG C of conditions.
Table 4
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 60％ | 15％ | 15％ | 10％ |
Embodiment 5
By flavones essence according to ratio mixing in table 5, take the hydroxypropyl cellulose adhesive that weight is flavones essence weight 1%, join in flavones essence with after the water-soluble solution of 550ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 5 hours under temperature is 70 DEG C of conditions.
Table 5
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 50％ | 30％ | 15％ | 15％ |
Embodiment 6
By flavones essence according to ratio mixing in table 6, take the hydroxypropyl cellulose adhesive that weight is flavones essence weight 1%, join in flavones essence with after the water-soluble solution of 550ml, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, upper fluid bed obtains the flavones essence cigarette pearl that particle diameter is 1.5mm, bulk density is 1.4g/ml after dry 4 hours under temperature is 80 DEG C of conditions.
Table 6
| Flavones kind | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Percentage by weight | 40％ | 20％ | 15％ | 25％ |
Flavones essence cigarette pearl prepared in above 6 embodiments is joined in cigarette filter stick, then detection of exhaust gas compositions is carried out to the cigarette made, and carry out phenol reduced rate and compare, specifically see the following form 7
Table 7
The smoke components of main reduction has phenol, crotonaldehyde, free radical, and smoke hazard index is also on a declining curve simultaneously, and concrete reduced rate the results are shown in following table 8
Table 8
| Sample number into spectrum | Phenol | Crotonaldehyde | Index | Free radical |
| Embodiment 1 | 15.5％ | 18.2％ | 12.8％ | 5.6％ |
| Embodiment 2 | 20.9％ | 17.3％ | 10.3％ | 12.6％ |
| Embodiment 3 | 24.8％ | 16.5％ | 12.8％ | 13.7％ |
| Embodiment 4 | 45.0％ | 36.2％ | 17.9％ | 19.6％ |
| Embodiment 5 | 42.6％ | 34.5％ | 15.4％ | 20.9％ |
| Embodiment 6 | 40.3％ | 31.6％ | 14.1％ | 17.5％ |
Join in cigarette filter stick by flavones essence cigarette pearl prepared in above 6 embodiments, then carry out sensory evaluation to the cigarette made, result is as table 9
Table 9
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.
Claims (6)
1. a cigarette preparation method for flavones essence cigarette pearl, is characterized in that: described preparation method is as follows:
Take the adhesive that weight is flavones essence weight 0.1% ~ 1%, adhesive is with joining in flavones essence after water-soluble solution, stir and make softwood, then softwood will be extruded-spheronizator, first be extruded into elongated strip by extruder, then round as a ball by spheronizator, obtain the flavones essence cigarette pearl that particle size range is 0.5mm ~ 4mm, bulk density is 1.2g/ml ~ 1.8g/ml after drying;
Wherein: the weight percentages of components of described flavones essence is as follows:
2. the preparation method of cigarette flavones essence cigarette pearl according to claim 1, is characterized in that: the DNA purity of described cyanidenon, scutelloside, Quercetin and aurantiamarin is 80 ~ 95%.
3. the preparation method of cigarette flavones essence cigarette pearl according to claim 1, is characterized in that: described adhesive is one or more in PVP, hydroxypropyl cellulose, hydroxypropyl methylcellulose and carboxymethyl cellulose.
4. the cigarette preparation method of flavones essence cigarette pearl according to claim 1 or 2 or 3, is characterized in that: the particle size range of described cigarette pearl is 0.8mm ~ 1.5mm, and bulk density is 1.4g/ml ~ 1.6g/ml.
5. the cigarette preparation method of flavones essence cigarette pearl according to claim 1 or 2 or 3, is characterized in that: described drying is under temperature is 60 DEG C ~ 80 DEG C conditions dry 4 ~ 6 hours.
6. cigarette is with a flavones essence cigarette pearl, it is characterized in that: the flavones essence cigarette pearl that described flavones essence cigarette pearl is prepared for method described in claim 1.
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