CN104745303A - Spice for cigarettes and application thereof - Google Patents
Spice for cigarettes and application thereof Download PDFInfo
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- CN104745303A CN104745303A CN201510166699.3A CN201510166699A CN104745303A CN 104745303 A CN104745303 A CN 104745303A CN 201510166699 A CN201510166699 A CN 201510166699A CN 104745303 A CN104745303 A CN 104745303A
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- Prior art keywords
- cut
- honey
- longan
- steamer
- excess
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
- A24B15/306—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation one reactant being an amino acid or a protein, e.g. Maillard's reaction
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a spice for cigarettes and an application thereof. The spice is prepared in a manner that longan honey is subjected to steam distillation and a maillard reaction and mixed with ingredients. After the obtained spice is added to a flue-cured type cigarette leaf group, through a sense organ smoke panel test, the spice plays an important role in improving the quality of a cigarette. The spice is simple and convenient in method and technology; equipment is simple; the cost is low; the pollution is little; the extraction efficiency is high; composition analysis indicates that the contents of overall aroma-active components of a product are high; the aroma-active components are rich in variety; and through sensory evaluation, the product can effectively improve the smoke quality of the cigarette.
Description
Technical field
The invention belongs to cigaret additive technical field, being specifically related to a kind of take longan, honey as tobacco aromatics using prepared by raw material.The invention still further relates to the embody rule of described spices in production of cigarettes simultaneously.
Background technology
Along with the development and progression of society, the health perception of human consumer improves gradually, and people progressively change smoking property of cigarette custom, and low-coke tar cigarette obtains the concern of consumers in general.In order to meet the demand of people, tobacco workers, by studying for a long period of time, have defined the method for a series of reduction tar: improve air permeance for cigarette paper, adopt the filter tip of differing materials structure, punching dilution, expanded cut tobacco stem and tobacco sheet.In Cigarette processing process, the technical measures of reducing tar and reducing harm are in Cigarette processing process, and merely reducing tar content is not difficult matter already, and its difficulty is how while reduction tar content, not weaken cigarette fragrance as far as possible, does not destroy aromatic style.In order to solve this difficult problem, a large amount of spices technology obtains research and apply in low-coke tar cigarette.
Longan, honey is also known as " longan honey ", top grade in honey, mainly be distributed in South China of China, and Taiwan, as provinces such as Guangdong, Guangxi, Fujian, nectarine is amber, food flavor is sweet, and not easily crystallization, has the enhanced aroma of longan, in the single nectar of China, its protein content is the highest, reaches 1.699%.It has nourishing blood to tranquillize the mind, effect of beneficial spleen, beauty treatment, clearing heat and moistening dryness, invigorating the spleen and replenishing QI of whetting the appetite, and the palpitation and restlessness caused the heart spleen deficiency of blood, insomnia hypomnesis have auxiliary curative effect.Be particularly suitable for women to eat.
Current, longan, honey uses mainly as drink, and is that raw material is prepared the technology of tobacco aromatics using there is not been reported with longan, honey.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, providing a kind of is raw material with longan, honey, effectively can improve the tobacco aromatics using of cigarette suction comfort.
The present invention also aims to provide the embody rule of described tobacco aromatics using in production of cigarettes.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage ratio of the present invention is mass percent.
A kind of tobacco aromatics using, is prepared by following method:
(1) join in thermostat water bath by 1L deionized water, constant water bath temperature, at 60 ~ 70 DEG C, adds longan, honey while stirring, and stirring velocity is 100 ~ 300rpm/min;
(2) after longan, honey adds, heating raised temperature to 90 ~ 95 DEG C, now have a large amount of foam to produce, heating rate is raised again after foam condensation, condensation volatile matter is to collect cut, non-volatile matter, as heating up in a steamer excess, when fraction collection is to stopping during described longan, honey weight 20 ~ 30% collecting, obtains the first cut;
(3) to heating up in a steamer in excess the amino acid adding and account for described longan, honey weight 10% ~ 15% and the water accounting for described longan, honey weight 1 ~ 2 times, at 100-105 DEG C, reacting 1 ~ 3h, excess Maillard reaction thing must be heated up in a steamer;
(4) join in thermostat water bath by 1L deionized water, constant water temperature 65 ~ 75 DEG C, add while stirring and heat up in a steamer excess Maillard reaction thing, stirring velocity is 50 ~ 200rpm/min;
(5) heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into this cut weight for described in heat up in a steamer 30 ~ 35% of excess Maillard reaction thing weight time stop collecting, obtain the second cut;
(6) described tobacco aromatics using is namely obtained after the first cut and the second cut being mixed according to the mass ratio of 1:1.5 ~ 3.
Preferably, the viscosity of the longan, honey in step (1) is 2000 ~ 3000cP;
Preferably, in step (1), the feed ratio of longan, honey and water is 1: 0.5 ~ 2, g:mL;
Preferably, the amino acid described in step (3) be glycine, L-Ala, Pidolidone a kind of or be the mixture of three seed amino acids;
Preferably, the feed ratio heating up in a steamer excess Maillard reaction thing and water in step (4) is 1: 1 ~ 2, g:mL.
The invention still further relates to the embody rule of described tobacco aromatics using in production of cigarettes, namely use described tobacco aromatics using to the method for cigarette flavouring, be specially: be made into the solution that mass concentration is 5 ~ 10% after described tobacco aromatics using ethanol or glycerol being dissolved, by 0.001 ~ 0.01% of tobacco quality, solution added on pipe tobacco by spray pattern in charging process.Increase fragrance can be made during smoking cigarette to coordinate, increase cigarette perfume, increase the sweet sense of flue gas, effectively improve cigarette comfort level.
Relative to prior art, the present invention has following beneficial effect:
1) the present invention utilizes longan, honey, and the technology combined by wet distillation and Maillard reaction prepares tobacco aromatics using, and applies it in cigarette, technique is simply applicable, required equipment is simple, and cost is low and pollute little, has the important market development and application prospect.
2) tobacco aromatics using made by is applied to effect in cigarette clearly, can play the effect improving the breath of cigarette delicate fragrance, increase the sweet sense of flue gas and raising cigarette comfortableness.
Accompanying drawing explanation
Fig. 1 is the process flow diagram of preparation method of the present invention.
Fig. 2 is the aroma component total ion current figure of tobacco aromatics using of the present invention.
Embodiment
Below in conjunction with drawings and Examples, the present invention is described in further detail, but drawings and Examples are not limited to the technical solution.
Embodiment 1
1L deionized water is joined in thermostat water bath, constant water bath temperature is at 60 DEG C, and longan, honey and water feed intake in 1: 0.5 (g:mL) ratio, add longan, honey while stirring, mixing control is 100rpm/min, after longan, honey adds, heating raised temperature to 90 DEG C, now has a large amount of foam and produces, heating rate is raised again after foam condensation, collecting cut, when fraction collection is to stopping during honey weight 20% collecting, obtaining the first cut.Heat up in a steamer excess and add the glycine of longan, honey weight 10%% and the water of weight 1 times, 1h is reacted at 100 DEG C, excess Maillard reaction thing must be heated up in a steamer, 1L deionized water is joined in thermostat water bath, constant water temperature 65 DEG C, by preparation heat up in a steamer excess Maillard reaction thing and water feeds intake according to the ratio of 1: 0.5 (g:mL), add while stirring and heat up in a steamer excess Maillard reaction thing, stirring velocity is 50rpm/min, heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into when this cut weight accounts for heat up in a steamer excess Maillard reaction thing weight 30% and stop collecting, obtain the second cut.Namely required tobacco aromatics using A is obtained after first cut and the second cut being mixed according to the mass ratio of 1:1.5.
Embodiment 2
1L deionized water is joined in thermostat water bath, constant water bath temperature is at 70 DEG C, and longan, honey and water feed intake in 1: 2 (g:mL) ratio, add longan, honey while stirring, mixing control is 300rpm/min, after longan, honey adds, heating raised temperature to 95 DEG C, now has a large amount of foam and produces, heating rate is raised again after foam condensation, collecting cut, when fraction collection is to stopping during honey weight 30% collecting, obtaining the first cut.Heat up in a steamer excess and add the L-Ala of longan, honey weight 15%% and the water of weight 2 times, 3h is reacted at 105 DEG C, excess Maillard reaction thing must be heated up in a steamer, 1L deionized water is joined in thermostat water bath, constant water temperature 75 DEG C, by preparation heat up in a steamer excess Maillard reaction thing and water feeds intake according to the ratio of 1: 2 (g:mL), add while stirring and heat up in a steamer excess Maillard reaction thing, stirring velocity is 200rpm/min, heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into and stop collecting when this cut weight accounts for heat up in a steamer excess Maillard reaction thing weight 35%, obtain the second cut.Namely required tobacco aromatics using B is obtained after first cut and the second cut being mixed according to the mass ratio of 1:3.
Embodiment 3
1L deionized water is joined in thermostat water bath, constant water bath temperature is at 65 DEG C, and longan, honey and water feed intake in 1: 1 (g:mL) ratio, add longan, honey while stirring, mixing control is 200rpm/min, after longan, honey adds, heating raised temperature to 95 DEG C, now has a large amount of foam and produces, heating rate is raised again after foam condensation, collecting cut, when fraction collection is to stopping during honey weight 25% collecting, obtaining the first cut.Heat up in a steamer excess and add the Pidolidone of longan, honey weight 10%% and the water of weight 1.5 times, 2h is reacted at 102 DEG C, excess Maillard reaction thing must be heated up in a steamer, 1L deionized water is joined in thermostat water bath, constant water temperature 75 DEG C, by preparation heat up in a steamer excess Maillard reaction thing and water feeds intake according to the ratio of 1: 1 (g:mL), add while stirring and heat up in a steamer excess Maillard reaction thing, stirring velocity is 100rpm/min, heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into and stop collecting when this cut weight accounts for heat up in a steamer excess Maillard reaction thing weight 30%, obtain the second cut.Namely required tobacco aromatics using C is obtained after first cut and the second cut being mixed according to the mass ratio of 1:2.
Embodiment 4
1L deionized water is joined in thermostat water bath, constant water bath temperature is at 65 DEG C, and longan, honey and water feed intake in 1: 1 (g:mL) ratio, add longan, honey while stirring, mixing control is 200rpm/min, after longan, honey adds, heating raised temperature to 90 DEG C, now has a large amount of foam and produces, heating rate is raised again after foam condensation, collecting cut, when fraction collection is to stopping during honey weight 25% collecting, obtaining the first cut.Heating up in a steamer excess, to add longan, honey weight 10%% mass ratio be glycine: L-Ala: the mixture of Pidolidone=1:1:1, add the water of longan, honey weight 1.5 times simultaneously, 2h is reacted at 100 DEG C of temperature, excess Maillard reaction thing must be heated up in a steamer, 1L deionized water is joined in thermostat water bath, constant water temperature 75 DEG C, by preparation heat up in a steamer excess Maillard reaction thing and water feeds intake according to the ratio of 1: 1 (g:mL), add while stirring and heat up in a steamer excess Maillard reaction thing, stirring velocity is 200rpm/min, heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into and stop collecting when this cut weight accounts for heat up in a steamer excess Maillard reaction thing weight 35%, obtain the second cut.Namely required tobacco aromatics using D is obtained after first cut and the second cut being mixed according to the mass ratio of 1:1.
Comparative example
1L deionized water is joined in thermostat water bath, constant water bath temperature is at 65 DEG C, longan, honey and water feed intake in 1: 1 (g:mL) ratio, add longan, honey while stirring, after foam condensation, adding longan, honey weight 10%% mass ratio is glycine: L-Ala: the mixture of Pidolidone=1:1:1,2h is reacted at 105 DEG C, cut is collected in heating, be collected into and stop collecting when this cut weight accounts for heat up in a steamer excess Maillard reaction thing weight 30%, this cut is tobacco aromatics using A as a comparison.
Application Example:
Different thinners can be selected according to the difference of extracted tobacco aromatics using, thinner can select ethanol or glycerol, be made into the solution that concentration is 5 ~ 10%, be sprayed at the tobacco leaf surface of flue-cured tobacco, fountain height is 0.001%, 0.005%, 0.01% of flue-cured tobacco weight, to not add the fire-cured tobacco type leaf group of tobacco aromatics using in contrast, conveniently cigarette process makes cigarette product.
Cigarette product will be made and carry out sensory quality assessment, result is as shown in table 1, as can be seen from Table 1, be compared to blank sample and add the cigarette contrasting tobacco aromatics using A, the cigarette that with the addition of embodiment tobacco aromatics using obviously can increase fragrance Harmony, increases cigarette perfume, reduces dry sensation, increase back sweet sense.Result also shows, it is better that the addition of tobacco aromatics using in pipe tobacco to control when 0.005% concentration effect, and cigarette flavor Harmony is better, the comfortable and noresidue of pleasant impression.The amount of adding tobacco aromatics using in reality obtains according to various parameter setting test.
The evaluation and analysis result of tobacco aromatics using prepared by table 1 in Virginian-type cigarette leaf group
From the Data Comparison of embodiment and comparative example above, redistillation after directly carrying out Maillard reaction using honey as sugared source using the cut obtained as tobacco aromatics using, its flavouring effect is unsatisfactory, various Sensory quality index is all not high.By contrast, first distillation is first carried out to honey in the present invention and process to obtain the first cut, and then make to heat up in a steamer excess and amino acid generation Maillard reaction, the second cut is distilled to obtain again to heating up in a steamer excess maillard reaction product, as tobacco aromatics using after making the first cut mix with the second cut again, then flavouring Be very effective.This phenomenon had no relevant report in the past.
Above content is the further description made the present invention in conjunction with concrete preferred implementation.For general technical staff of the technical field of the invention, the obvious modification made without departing from the inventive concept of the premise, performance or purposes identical, all should be considered as protection scope of the present invention.
Claims (6)
1. a tobacco aromatics using, is characterized in that, it is prepared by following method:
(1) join in thermostat water bath by 1L deionized water, constant water bath temperature, at 60 ~ 70 DEG C, adds longan, honey while stirring in this deionized water, and stirring velocity is 100-300rpm/min;
(2) after longan, honey adds, heating raised temperature to 90 ~ 95 DEG C, and raise heating rate again after foam condensation to be generated, condensation volatile matter is to collect cut, non-volatile matter is as heating up in a steamer excess, when fraction collection is to stopping during described longan, honey weight 20 ~ 30% collecting, obtain the first cut;
(3) to heating up in a steamer in excess the amino acid adding and account for described longan, honey weight 10%-15% and the water accounting for described longan, honey weight 1 ~ 2 times, at 100-105 DEG C, reacting 1 ~ 3h, excess Maillard reaction thing must be heated up in a steamer;
(4) join in thermostat water bath by 1L deionized water, constant water temperature 65-75 DEG C, heat up in a steamer excess Maillard reaction thing described in adding while stirring, stirring velocity is 50-200rpm/min;
(5) heating up in a steamer after excess Maillard reaction thing adds, cut is collected in heating, be collected into this cut weight for described in heat up in a steamer the 30-35% of excess Maillard reaction thing weight time stop collecting, obtain the second cut.
(6) described tobacco aromatics using is namely obtained after the first cut and the second cut being mixed according to the mass ratio of 1:1.5 ~ 3.
2. tobacco aromatics using according to claim 1, is characterized in that: the longan, honey viscosity in step (1) is 2000 ~ 3000cP.
3. tobacco aromatics using according to claim 1, is characterized in that: in step (1), the feed ratio of longan, honey and water is 1: 0.5 ~ 2, g:mL.
4. tobacco aromatics using according to claim 1, is characterized in that: the amino acid described in step (3) is glycine, L-Ala, Pidolidone a kind of or be the mixture of three seed amino acids;
5. tobacco aromatics using according to claim 1, is characterized in that: the feed ratio heating up in a steamer excess Maillard reaction thing and water in step (4) is 1: 1 ~ 2, g:mL.
6. use tobacco aromatics using according to claim 1 to the method for cigarette flavouring, it is characterized in that: after described tobacco aromatics using ethanol or glycerol being dissolved, be made into the solution that mass concentration is 5 ~ 10%, by tobacco quality 0.001 ~ 0.01% by this spray solution on pipe tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510166699.3A CN104745303A (en) | 2015-04-10 | 2015-04-10 | Spice for cigarettes and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510166699.3A CN104745303A (en) | 2015-04-10 | 2015-04-10 | Spice for cigarettes and application thereof |
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| CN104745303A true CN104745303A (en) | 2015-07-01 |
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| CN201510166699.3A Pending CN104745303A (en) | 2015-04-10 | 2015-04-10 | Spice for cigarettes and application thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029688A (en) * | 2015-07-28 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette additive using honey and preparation method thereof |
| CN105124736A (en) * | 2015-09-02 | 2015-12-09 | 云南中烟工业有限责任公司 | Method of promoting moisturizing and aroma enhancement effects of cigarettes by means of cloves |
| CN105146713A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing lavandula angustifolia |
| CN105146715A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing althaea rosea |
| CN105146712A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing red rose |
| CN105146708A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing agastache rugosa |
| CN105146709A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing pelargonium graveolens |
| CN105146711A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing coptis chinensis |
| CN105567425A (en) * | 2016-01-15 | 2016-05-11 | 红云红河烟草(集团)有限责任公司 | Compound honey suitable for tobacco charging |
| CN105738530A (en) * | 2016-04-29 | 2016-07-06 | 江苏中烟工业有限责任公司 | Method for optioning aroma component in natural moss perfume spice |
| CN106509980A (en) * | 2016-11-29 | 2017-03-22 | 湖北中烟工业有限责任公司 | Preparation method of sun-cured yellow tobacco extracts used for novel tobaccos |
| CN106723315A (en) * | 2016-12-01 | 2017-05-31 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN111375364A (en) * | 2018-12-29 | 2020-07-07 | 贵州中烟工业有限责任公司 | Method for preparing spice by using arillus longan extract as raw material and adopting microchannel reactor and application of method |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029688A (en) * | 2015-07-28 | 2015-11-11 | 湖北中烟工业有限责任公司 | Cigarette additive using honey and preparation method thereof |
| CN105146709A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing pelargonium graveolens |
| CN105146713A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing lavandula angustifolia |
| CN105146715A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing althaea rosea |
| CN105146712A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing red rose |
| CN105146708A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing agastache rugosa |
| CN105124736A (en) * | 2015-09-02 | 2015-12-09 | 云南中烟工业有限责任公司 | Method of promoting moisturizing and aroma enhancement effects of cigarettes by means of cloves |
| CN105146711A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing coptis chinensis |
| CN105567425A (en) * | 2016-01-15 | 2016-05-11 | 红云红河烟草(集团)有限责任公司 | Compound honey suitable for tobacco charging |
| CN105567425B (en) * | 2016-01-15 | 2020-02-07 | 红云红河烟草(集团)有限责任公司 | Compound honey suitable for tobacco charging |
| CN105738530A (en) * | 2016-04-29 | 2016-07-06 | 江苏中烟工业有限责任公司 | Method for optioning aroma component in natural moss perfume spice |
| CN106509980A (en) * | 2016-11-29 | 2017-03-22 | 湖北中烟工业有限责任公司 | Preparation method of sun-cured yellow tobacco extracts used for novel tobaccos |
| CN106723315A (en) * | 2016-12-01 | 2017-05-31 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN106723315B (en) * | 2016-12-01 | 2018-12-28 | 华宝香精股份有限公司 | A kind of preparation method of electronic cigarette raw material |
| CN111375364A (en) * | 2018-12-29 | 2020-07-07 | 贵州中烟工业有限责任公司 | Method for preparing spice by using arillus longan extract as raw material and adopting microchannel reactor and application of method |
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