CN103704883B - Preparing and application of natural product powder composite particle with aroma enhancement effect in cigarette filter - Google Patents
Preparing and application of natural product powder composite particle with aroma enhancement effect in cigarette filter Download PDFInfo
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Abstract
The invention discloses preparing and application of natural product powder composite particles with the aroma enhancement effect in a cigarette filter. 8-30 parts of ground coffee, 1.5-5 parts of sweetened natural plant powder, 0.3-1.5 parts of pearl powder and 100 parts of multi-hole corn starch are evenly mixed and moistened by deionized water comprising reducing sugar. Wet granulation, microwave shaping, microwave drying and sieving are carried out on the mixture and high-strength natural product powder composite multi-hole starch crystalline particles are obtained. The particles are added to cigarette filter rods to make binary or ternary composite filter rods, so that the content of nutrition components such as specific coffee volatile fatty acid and specific pearl powder amino acid can be added to smoke. It is indicated through cigarette sensory evaluation that the natural product powder composite particles added to the filter rods can boost the aroma amount of the smoke of cigarettes, improve aroma quality and harmony, reduce impure gases and stimulation, boost sweet feelings and integrally improve the inherent quality of the cigarettes.
Description
Technical field
The present invention relates to cigarette material preparing technical field, be specifically related to a kind of to there is the preparation method of the natural product powder composite particle of flavouring effect and the application in cigarette thereof.
Background technology
Being widely current of tobacco is one and has the global problem of serious consequence to public health, and therefore smoking and health problem are worldwide important topics.The current whole world about has more than 1,000,000,000 smokers, wherein Chinese nearly 3.5 hundred million smokers, accounts for 35% of whole world sum." World Health Organization's Framework Convention on Tobacco Control " (WHO FCTC) requires the basis of science, technology and economic problems that consideration is current and relevant promotes Tobacco use control measure.Due to smoking, consumer is numerous, and comprehensive ban on opium-smoking and the opium trade temporarily cannot realize, and reduces cigarette smoke and the harmfulness of human body is just become to the effective way alleviating smoking and health problem.In recent years; for reducing cigarette harmfulness; the health of protection smoking consumer; researcher has expanded in Harm reduction techniques field and has studied widely; a lot of harm reduction material added in cigarette filter is able to development & application, but wherein the raw material packet of a lot of harm reduction material, containing chemical materials, uses for a long time in a large number; while the harm of minimizing cigarette smoke, new hidden danger may be produced to human body again.Therefore, the ecology of flue gas harm reduction, particularly gain effect will be had, green, environment-friendly materials will be applied to cigarette product and are only the important research direction of more shooting the arrow at the target.
On the other hand, in global range, tobacco business all reduces cigarette smoke harm by tar content in lasting reduction cigarette smoke, but the lasting reduction of tar, also make the fragrance of traditional cigarette constantly thin out with suction taste, be difficult to the requirement reaching consumer, for this reason, need to carry out suitable compensating aroma.Current compensating aroma is main or undertaken by the mode of adding fragrance matter in cigarette shreds, and natural or artificial fragrance matter can produce some uncontrollable materials through burning, and wherein some may have potential impact to health for this.What make full use of pure natural has flavouring functional material, is added that to carry out cigarette compensating aroma be the more significant mode of one by cigarette filter, and not only compensation effect is more direct, and avoids because burning produces the material that may have potential impact to health.
Porous-starch is a kind of novel, safe sorbing material, be applied in cigarette filter, harmful components in adsorbable flue gas, and flue gas excitant can be reduced, improve flue gas suction quality, if but it is directly added in cigarette cellulose acetate filter, there is granularity too thin, be difficult to the problems such as industrial applications.CN101531779A, CN101314645A, CN101314646A disclose the granulating technique of porous-starch and the application process in cigarette thereof.But these methods exist, and porous-starch particle yield is low, intensity difference and chemical adhesive used exist the defects such as potential safety hazard, seriously constrain its application in cigarette.CN103054181A discloses a kind of coffee or cocoa power composite particle filter stick material and preparation method thereof, but the method exists directly pulverizes the method for adding by coffee or cocoa, simple and the relative coarseness of technology, coffee aroma is easy to lost, is difficult to ensure fragrance stability.CN103271443A discloses a kind of preparation method of coffee starch composite particles and the application in cigarette filter thereof, it has had larger improvement than aforementioned patent in maintenance granule coffee fragrance, but through conventional method granulation after its particle preparation flow adopts coffee and the root of kudzu vine directly to pulverize, coffee is relative with starch combining form simple, particle lacks the micropore of absorption flue gas harmful substance, therefore not strong to the crown_interception of flue gas harmful substance; Although the coffee particles prepared in addition has coffee aroma, fail some dry property and astringent sense of effectively removing in coffee aroma, make to prepare in smoking property of cigarette process and sometimes there is lingual surface and remain the situations such as a little picotement.
The present invention utilizes Corn Porous Starch to do carrier, by ground coffee, increases sweet natural vegetable powder, pearl powder and reduced sugar and supports on porous-starch, combine ground coffee, increase sweet natural vegetable powder, pearl powder and Corn Porous Starch unique effects separately.Simultaneously, the present invention not only overcomes the shortcomings such as the interpolation inconvenience of applying appearance in previously fine-powdered material cigarette filter and high expensive, and at utmost remove and mask the intrinsic dry property of coffee aroma neutral and alkali composition and astringent sense by the interpolation reduction smoke pH of reduced sugar, by techniques such as granulation, microwave sizing, microwave dehydration oven dry, by ground coffee, increase the compound porous starch of natural product powder such as sweet natural vegetable powder, pearl powder and make certain order number, there is the crystalline particles of a large amount of adsorbable harmful matter in cigarette microcellular structure.Particle is applied in cigarette filter, both in the elimination dry property of coffee aroma and astringent sense basis, significantly can increase cigarette flavor, can reduce again cigarette smoke harm.
Summary of the invention
Object of the present invention is intended to, for the fragrance disappearance improving and make up low burnt tar cigarette mouthfeel, provide a kind of preparation method with the natural product powder composite particle of flavouring effect.
A kind of natural product powder composite particle with flavouring effect, it is characterized in that, raw material is with parts by weight, composed as follows: 8-30 part ground coffee, 1.5-5 part increase sweet natural vegetable powder, 0.3-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 80-100 part reduced sugar deionized water solutions; Be optimized for 10-25 part ground coffee, 2-5 part increase sweet natural vegetable powder, 0.5-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 90-100 part reduced sugar deionized water solutions; Be optimized for 15-20 part ground coffee further, 2-3 part increase sweet natural vegetable powder, 1-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 100 parts of reduced sugar deionized water solutions.
A kind of natural product powder composite particle with flavouring effect provided by the invention, the sweet natural vegetable powder of described increasing is licorice powder, dark plum powder, sweetleaf inulin or its mixture.
A kind of natural product powder composite particle with flavouring effect provided by the invention, described ground coffee is broken into fine powder by coffee bean powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill; The sweet natural vegetable powder of described increasing is broken into fine powder by former Plant Powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill; Described pearl powder is broken into fine powder by pearl powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill.
A kind of natural product powder composite particle with flavouring effect provided by the invention, described reduced sugar is glucose, fructose, maltose or its mixture, and described reduced sugar deionized water solution concentration is 2%-20%.Be preferably 3%-15%; More preferably 5%-10%.
A kind of preparation method with the natural product powder composite particle of flavouring effect provided by the invention, : can by ground coffee, increase sweet natural vegetable powder, pearl powder adds among porous-starch in proportion, mix, the deionized water solution slowly adding reduced sugar soaks, then by the ground coffee after wetting, increase sweet natural vegetable powder, pearl powder, the screen cloth that porous-starch mixture passes certain order number by pressing method is prepared into particle, particle is put into micro-wave oven being no more than at 100 DEG C and is carried out microwave gelation sizing, dry, then sieve, obtain the compound porous starch crystalline particles of natural product powder.
Provided by the invention have in preparation method's preferred version of the natural product powder composite particle of flavouring effect, and after the compound porous starch granulation of described natural product powder, microwave gelation sizing is under not dehumidifier state, with 20 kilowatts/m
2the compound porous starch granules of Microwave Power Density discontinuity process natural product powder amount to 4-6 minute; Described microwave drying is under dehumidifier state, with 20 kilowatts/m
2the compound porous starch granules of Microwave Power Density discontinuity process natural product powder amount to 6 ~ 9 minutes.
The present invention also aims to provide the above-mentioned application of natural product powder composite particle in cigarette filter with flavouring effect.
A kind of application of natural product powder composite particle in cigarette filter with flavouring effect of the present invention, be included in filter stick formation process, the natural product powder composite particle of 80 ~ 120mg is added, the fine Three-element composite filter core of obtained vinegar fibre-composite particles-vinegar in cavity reserved between the fine filter core of the conventional vinegar of two-section; Or in filter stick formation process, in cavity reserved between the fine filter core of two-section groove vinegar, add the natural product powder composite particle of 80 ~ 120mg, obtained furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core.
A kind of application of natural product powder composite particle in cigarette filter with flavouring effect of the present invention, comprising falls apart natural product powder composite particle is spread across on the tow of cigarette filter rod, obtainedly loads the fine filter stick of natural product powder composite particle vinegar; Again fine for loading natural product powder composite particle vinegar filter stick is connected with the fine filter stick of conventional vinegar or furrowfilter rod, obtained binary or Three-element composite filter core.
The described natural product powder composite particle with flavouring effect being fallen apart in the present invention is spread across on cigarette filter rod tow, refer in vinegar fibre filter stick formation process, described natural product powder composite particle is sprinkled upon on filter stick tow by the addition of 10 ~ 25mg/10mm tow is loose equably.
The effect that the natural product powder composite particle with flavouring effect of the present invention is applied in cigarette filter, comprise: the most characteristic flavor compounds containing the nutritional labelings such as the peculiar amino acid of pearl powder and natural coffee in particle volatility semi-volatility component, wherein the ratio natural coffee of principal character flavor component palmitic acid also has significantly increases, described natural product powder composite particle is made an addition to after cigarette filter rod is applied to cigarette, cigarette smoke perfume quantity can be increased, improve aroma quality and harmony, reduce assorted gas and excitant, increase sweet sense, the interior quality of Integral lifting cigarette.
Compared with prior art, the present invention has following beneficial effect:
The natural product powder composite particle 1, with flavouring effect combines ground coffee, increases sweet natural vegetable powder, pearl powder, effect of reduced sugar and porous-starch;
2, the present invention obtains the natural product powder composite particle of high yield, high strength by specific granulation, microwave sizing, stoving process.
3, have in the natural product powder composite particle volatility semi-volatility component of flavouring effect and comprise characteristic chicken flavor composition in the nutritional labelings such as the peculiar amino acid of pearl powder and natural coffee powder, the fragrant composition of some feature increases trend in addition.
The natural product powder composite particle 4, with flavouring effect is added in cigarette filter, can effectively eliminate on the basis of dry property and astringent sense in coffee aroma, increase cigarette smoke perfume quantity, improve aroma quality and harmony, reduce assorted gas and excitant, increase sweet sense, the interior quality of Integral lifting cigarette.
Accompanying drawing explanation
Fig. 1 is preparation technology's flow chart that the present invention has the natural product powder composite particle of flavouring effect;
Fig. 2 is the natural product powder composite particle sample volatility semi-volatility component analyzing total ion flow graph that the present invention has flavouring effect;
Fig. 3 is the structural representation that natural product powder composite particle the present invention with flavouring effect is applied to furrowfilter rod-particle-furrowfilter rod Three-element composite filter core;
1. filter cores in figure: the fine filter core of 1a., 1c. groove vinegar, 1b. natural product powder composite particle; 2. integument in; 3. outer casing.
Fig. 4 is the structural representation of natural product powder composite particle the present invention with flavouring effect when being applied to furrowfilter rod-particle/vinegar fibre-furrowfilter rod ternary composite filter tip;
1. filter cores in figure: the fine filter core of 1a., 1c. groove vinegar, the fine filter core of 1d. natural product powder composite particle/vinegar; 2. integument in; 3. tundish covering layer; 4. outer casing.
Detailed description of the invention
Technical scheme of the present invention is based on ground coffee, increases sweet natural vegetable powder, pearl powder, reduced sugar and the porous-starch unique effects in cigarette smoke flavouring harm reduction gain.
Following implementation process and embodiment are intended to further illustrate the present invention and should not regard limitation of the invention as.
Embodiment 1
Take 300g ground coffee, 50g increases sweet natural vegetable powder (licorice powder 25g, dark plum powder 10g, sweetleaf inulin 15g), and 15g pearl powder, joins in 1Kg Corn Porous Starch, and mix.Get 1000mL20% glucose deionized water solution evenly to spray in above-mentioned mixed powder, powder is soaked.The powder after soaking is made to be less than 20 object particles by 20 eye mesh screens are obtained by extruder grain mode.Above-mentioned particle is put into micro-wave oven, under not dehumidifier state, amounts to 6 minutes with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2 and shape for gelation; Then, under dehumidifier state, amount to 9 minutes for drying natural product powder composite particle with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2, above microwave treatment wants control temperature to be no more than 100 DEG C.Gained particle crosses 20 orders and 40 mesh standard sieves respectively, obtains the natural product powder composite particle that 20 order-40 orders have flavouring effect.
Embodiment 2
Take 200g ground coffee, 35g increases sweet natural vegetable powder (dark plum powder 35g), and 10g pearl powder, joins in 1Kg Corn Porous Starch, and mix.Get 1000mL10% fructose deionized water solution evenly to spray in above-mentioned mixed powder, powder is soaked.The powder after soaking is made to be less than 20 object particles by 20 eye mesh screens are obtained by extruder grain mode.Above-mentioned particle is put into micro-wave oven, under not dehumidifier state, amounts to 6 minutes with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2 and shape for gelation; Then, under dehumidifier state, amount to 8 minutes for drying natural product powder composite particle with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2, above microwave treatment wants control temperature to be no more than 100 DEG C.Gained particle crosses 20 orders and 40 mesh standard sieves respectively, obtains the natural product powder composite particle that 20 order-40 orders have flavouring effect.
Embodiment 3
Take 100g ground coffee, 25g increases sweet natural vegetable powder (licorice powder 25g), and 5g pearl powder, joins in 1Kg Corn Porous Starch, and mix.Get 900mL5% maltose deionized water solution evenly to spray in above-mentioned mixed powder, powder is soaked.The powder after soaking is made to be less than 20 object particles by 20 eye mesh screens are obtained by extruder grain mode.Above-mentioned particle is put into micro-wave oven, under not dehumidifier state, amounts to 5 minutes with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2 and shape for gelation; Then, under dehumidifier state, amount to 7 minutes for drying natural product powder composite particle with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2, above microwave treatment wants control temperature to be no more than 100 DEG C.Gained particle crosses 20 orders and 40 mesh standard sieves respectively, obtains the natural product powder composite particle that 20 order-40 orders have flavouring effect.
Embodiment 4
Take 80g ground coffee, 15g increases sweet natural vegetable powder (sweetleaf inulin 15g), and 3g pearl powder, joins in 1Kg Corn Porous Starch, and mix.Get 800mL2% reduced sugar deionized water solution (glucose 1%, fructose 1%) evenly to spray in above-mentioned mixed powder, powder is soaked.Wetting rear powder is made to be less than 20 object particles by 20 eye mesh screens are obtained by extruder grain mode.Above-mentioned particle is put into micro-wave oven, under not dehumidifier state, amounts to 4 minutes with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2 and shape for gelation; Then, under dehumidifier state, amount to 6 minutes for drying natural product powder composite particle with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2, above microwave treatment wants control temperature to be no more than 100 DEG C.Gained particle crosses 20 orders and 40 mesh standard sieves respectively, obtains the natural product powder composite particle that 20 order-40 orders have flavouring effect.
Embodiment 5
Take 150g ground coffee, 20g increases sweet natural vegetable powder (sweetleaf inulin 10g, dark plum powder 10g), and 8g pearl powder, joins in 1Kg Corn Porous Starch, and mix.Get 900mL10% reduced sugar deionized water solution (glucose 5%, fructose 3%, maltose 2%) evenly to spray in above-mentioned mixed powder, powder is soaked.The powder after soaking is made to be less than 20 object particles by 20 eye mesh screens are obtained by extruder grain mode.Above-mentioned particle is put into micro-wave oven, under not dehumidifier state, amounts to 5 minutes with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2 and shape for gelation; Then, under dehumidifier state, amount to 8 minutes for drying natural product powder composite particle with the Microwave Power Density discontinuity process particle of 20 kilowatts/m2, above microwave treatment wants control temperature to be no more than 100 DEG C.Gained particle crosses 20 orders and 40 mesh standard sieves respectively, obtains the natural product powder composite particle that 20 order-40 orders have flavouring effect.
Application Example 1
Apply the natural product powder composite particle with flavouring effect of the present invention, by filter stick formation equipment and particle feeding equipment, 100mg natural product powder composite particle is added in 6mm cavity reserved between the fine filter core of every two-section groove vinegar, be prepared into furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core, the addition often propping up natural product powder composite particle in the ternary composite filter tip of cigarette is 100mg, and the structure of filter stick as shown in Figure 3.Contrast filter stick is the furrowfilter rod-particle-furrowfilter rod ternary composite filter stick with launder adding the particle that 100mg uses merely porous-starch to prepare through microwave treatment.Utilize above-mentioned two kinds of filter stick setting-outs to produce cigarette, except filter stick, the cigarette material of test cigarette is identical with control sample with tobacco leaf formulation.The physical index of sample cigarette filter rod is in table 1, and the cigarette sample smoking result that setting-out is produced is in table 2.In cigarette smoke, analysis of amino acids the results are shown in Table 3.
Table 1 furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core and contrast filter stick physical index
Table 2 furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core cigarette and contrast filter stick cigarette smoking result
Table 3 furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core cigarette and control sample flue gas amino acid content
Application Example 2
Apply the natural product powder composite particle with flavouring effect of the present invention, the particle feeding equipment in filter stick formation process is utilized to produce the fine filter stick of the vinegar loading natural product powder composite particle, then by filter stick equipment complex, fine to this filter stick and groove vinegar filter stick is connected for furrowfilter rod-composite particles/vinegar fibre-furrowfilter rod Three-element composite filter core, the addition often propping up nanometer natural product powder composite particle in the ternary composite filter tip of cigarette is 20mg, and the structure of filter stick as shown in Figure 4.Contrast filter stick is the furrowfilter rod-particle/vinegar fibre-furrowfilter rod ternary composite filter stick with launder adding the particle that 20mg uses merely porous-starch to prepare through microwave treatment.Utilize above-mentioned two kinds of filter stick setting-outs to produce cigarette, except filter stick, the cigarette material used in cigarette process is all identical with tobacco leaf formulation three.The physical index of two kinds of cigarette filter rods is in table 4, and the cigarette sample smoking result that setting-out is produced is in table 5.
Table 4 furrowfilter rod-composite particles/vinegar fibre-furrowfilter rod Three-element composite filter core and contrast filter stick physical index
Table 5 furrowfilter rod-composite particles/vinegar fibre-furrowfilter rod Three-element composite filter core cigarette and control sample smoking result
Application Example 3
Apply the natural product powder composite particle with flavouring effect of the present invention, adopt Simultaneous distillation to extract volatile and semi-volatile compounds in sample particle, extract is through anhydrous sodium sulfate process and concentrate, and GC-MS analysis is carried out in sampling.Utilize WILEY spectrum storehouse and NIST to compose storehouse and carry out signals assigned.Areas of peak normalization method is adopted to calculate the relative amount of each composition.The total particle flow graph of sample is shown in Fig. 2, and volatility semi-volatility component analytical table is in table 6.
Table 6, the natural product powder composite particle volatility with flavouring effect, semi-volatility component analytical table
Analytical applications embodiment 1 and Application Example 2 experimental result can be found out, the natural product powder composite particle with flavouring effect is added to after in cigarette filter tip, compare with the cigarette that contrasts using porous-starch to prepare particle through microwave treatment merely, in cigarette smoke, amino acid content has obvious rising.Cigarette sensory evaluating smoking show, adds natural product powder composite particle in mouth rod, can increase cigarette smoke perfume quantity, improves aroma quality and harmony, reduces assorted gas and excitant, increase sweet sense, the interior quality of Integral lifting cigarette.
Analytical applications embodiment 3 experimental result can be found out: volatility and the semi-volatility component of natural coffee powder mainly contain: furfuryl alcohol; palmitic acid; furfural; 5 methyl furfural; 2-acetyl pyrrole; to vinyl guaiacol etc., wherein main component palmitic acid composition is generally no more than 20%, constitutes the characteristic perfume of coffee.And the volatile and semi-volatile compounds with the natural product powder composite particle of flavouring effect prepared by mode of the present invention, contain most characteristic flavor compounds of natural coffee, wherein the ratio natural coffee of principal character flavor component palmitic acid also has significantly increases, display particle can retain and the odor characteristic of partial reinforment coffee, this should be after natural product powder composite particle makes an addition to filter tip, can to a certain degree increase cigarette perfume (or spice), improve the material base of mouthfeel.
Claims (14)
1. one kind has the natural product powder composite particle of flavouring effect, it is characterized in that, raw material is with parts by weight, composed as follows: 8-30 part ground coffee, 1.5-5 part increase sweet natural vegetable powder, 0.3-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 80-100 part reduced sugar deionized water solutions; The sweet natural vegetable powder of described increasing is licorice powder, dark plum powder, sweetleaf inulin or its mixture; Described reduced sugar is glucose, fructose, maltose or its mixture, and described reduced sugar deionized water solution concentration is 2%-20%.
2. a kind of natural product powder composite particle with flavouring effect according to claim 1, it is characterized in that, raw material is with parts by weight, composed as follows: 10-25 part ground coffee, 2-5 part increase sweet natural vegetable powder, 0.5-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 90-100 part reduced sugar deionized water solutions.
3. a kind of natural product powder composite particle with flavouring effect according to claim 1, it is characterized in that, raw material is with parts by weight, composed as follows: 15-20 part ground coffee, 2-3 part increase sweet natural vegetable powder, 1-1.5 part pearl powder, 100 parts of Corn Porous Starchs, 100 parts of reduced sugar deionized water solutions.
4. a kind of natural product powder composite particle with flavouring effect according to any one of claim 1-3, is characterized in that: described ground coffee is broken into fine powder by coffee bean powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill.
5. a kind of natural product powder composite particle with flavouring effect according to any one of claim 1-3, it is characterized in that: the sweet natural vegetable powder of described increasing is broken into fine powder by former Plant Powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill.
6. a kind of natural product powder composite particle with flavouring effect according to any one of claim 1-3, is characterized in that: described pearl powder is broken into fine powder by pearl powder, and be prepared into the powder of particle diameter 100-500nm through nanon ball-mill.
7. a kind of natural product powder composite particle with flavouring effect according to claim 1, is characterized in that: described reduced sugar deionized water solution concentration is 3%-15%.
8. a kind of natural product powder composite particle with flavouring effect according to claim 7, is characterized in that: described reduced sugar deionized water solution concentration is 5%-10%.
9. a kind of preparation method with the natural product powder composite particle of flavouring effect according to any one of claim 1-3, it is characterized in that: by ground coffee, increase sweet natural vegetable powder, pearl powder adds among porous-starch in proportion, mix, the deionized water solution slowly adding reduced sugar soaks, then by the ground coffee after wetting, increase sweet natural vegetable powder, pearl powder, the screen cloth that porous-starch mixture passes certain order number by pressing method is prepared into particle, particle is put into micro-wave oven being no more than at 100 DEG C and is carried out microwave gelation sizing, dry, then sieve, obtain the compound porous starch crystalline particles of natural product powder.
10. there is the preparation method of the natural product powder composite particle of flavouring effect according to claim 9, it is characterized in that: described microwave gelation sizing is under not dehumidifier state, with 20 kilowatts/m
2the compound porous starch granules of Microwave Power Density discontinuity process natural product powder amount to 4-6 minute; Described microwave drying is under dehumidifier state, with 20 kilowatts/m
2the compound porous starch granules of Microwave Power Density discontinuity process natural product powder amount to 6 ~ 9 minutes.
The application of composite particles in cigarette filter that 11. a kind of preparation methods with the natural product powder composite particle of flavouring effect any one of claim 9-10 described in claim prepare, it is characterized in that: in filter stick formation process, the natural product powder composite particle of 80 ~ 120mg is added, the fine Three-element composite filter core of obtained vinegar fibre-composite particles-vinegar in cavity reserved between the fine filter core of the conventional vinegar of two-section; Or in filter stick formation process, in cavity reserved between the fine filter core of two-section groove vinegar, add the natural product powder composite particle of 80 ~ 120mg, obtained furrowfilter rod-composite particles-furrowfilter rod Three-element composite filter core.
The application of composite particles in cigarette filter that 12. a kind of preparation methods with the natural product powder composite particle of flavouring effect any one of claim 9-10 described in claim prepare, it is characterized in that: natural product powder composite particle being fallen apart is spread across on the tow of cigarette filter rod, the fine filter stick of obtained loading natural product powder composite particle vinegar; Again fine for loading natural product powder composite particle vinegar filter stick is connected with the fine filter stick of conventional vinegar or furrowfilter rod, obtained binary or Three-element composite filter core.
13. application according to claim 12, it is characterized in that: be spread across on cigarette filter rod tow by loose for described natural product powder composite particle, refer in vinegar fibre filter stick formation process, described natural product powder composite particle is sprinkled upon on filter stick tow by the addition of 10 ~ 25mg/10mm tow is loose equably.
14. application according to claim 13; it is characterized in that: the most characteristic flavor compounds containing the nutritional labelings such as the peculiar amino acid of pearl powder and natural coffee in particle volatility semi-volatility component; wherein the ratio natural coffee of principal character flavor component palmitic acid also has significantly increases; described natural product powder composite particle is made an addition to after cigarette filter rod is applied to cigarette; cigarette smoke perfume quantity can be increased; improve aroma quality and harmony; reduce assorted gas and excitant; increase sweet sense, the interior quality of Integral lifting cigarette.
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| CN103704881A (en) * | 2013-12-31 | 2014-04-09 | 广西中烟工业有限责任公司 | Preparing and application of natural product powder composite particle with harm reducing effect in cigarette filter |
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| CN103704881A (en) * | 2013-12-31 | 2014-04-09 | 广西中烟工业有限责任公司 | Preparing and application of natural product powder composite particle with harm reducing effect in cigarette filter |
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