CN104651620B - 一种从镍基合金废料中再生高纯硫酸镍的方法 - Google Patents
一种从镍基合金废料中再生高纯硫酸镍的方法 Download PDFInfo
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- CN104651620B CN104651620B CN201510125711.6A CN201510125711A CN104651620B CN 104651620 B CN104651620 B CN 104651620B CN 201510125711 A CN201510125711 A CN 201510125711A CN 104651620 B CN104651620 B CN 104651620B
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- nickel
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- acid
- waste material
- sulphuric acid
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- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 199
- 238000000034 method Methods 0.000 title claims abstract description 140
- 229910052759 nickel Inorganic materials 0.000 title claims abstract description 93
- 239000000956 alloy Substances 0.000 title claims abstract description 75
- 229910045601 alloy Inorganic materials 0.000 title claims abstract description 71
- 239000002699 waste material Substances 0.000 title claims abstract description 49
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 title claims abstract description 44
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 title claims abstract description 44
- 230000001172 regenerating effect Effects 0.000 title abstract description 3
- 239000002253 acid Substances 0.000 claims abstract description 73
- 238000002386 leaching Methods 0.000 claims abstract description 71
- 238000000605 extraction Methods 0.000 claims abstract description 56
- 238000001556 precipitation Methods 0.000 claims abstract description 35
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000012535 impurity Substances 0.000 claims abstract description 29
- 238000000926 separation method Methods 0.000 claims abstract description 27
- 239000010941 cobalt Substances 0.000 claims abstract description 19
- 229910017052 cobalt Inorganic materials 0.000 claims abstract description 19
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims abstract description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract description 7
- 238000002425 crystallisation Methods 0.000 claims abstract description 7
- 230000008025 crystallization Effects 0.000 claims abstract description 7
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910001415 sodium ion Inorganic materials 0.000 claims abstract description 5
- -1 hydrogen ions Chemical class 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims description 91
- 238000006396 nitration reaction Methods 0.000 claims description 76
- 239000002585 base Substances 0.000 claims description 54
- 208000035126 Facies Diseases 0.000 claims description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 42
- HIRWGWMTAVZIPF-UHFFFAOYSA-N nickel;sulfuric acid Chemical compound [Ni].OS(O)(=O)=O HIRWGWMTAVZIPF-UHFFFAOYSA-N 0.000 claims description 41
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 31
- 239000007787 solid Substances 0.000 claims description 30
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 28
- 239000003085 diluting agent Substances 0.000 claims description 26
- 229920002401 polyacrylamide Polymers 0.000 claims description 26
- 239000001117 sulphuric acid Substances 0.000 claims description 26
- 235000011149 sulphuric acid Nutrition 0.000 claims description 26
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 24
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 22
- RPAJSBKBKSSMLJ-DFWYDOINSA-N (2s)-2-aminopentanedioic acid;hydrochloride Chemical compound Cl.OC(=O)[C@@H](N)CCC(O)=O RPAJSBKBKSSMLJ-DFWYDOINSA-N 0.000 claims description 18
- 239000003513 alkali Substances 0.000 claims description 18
- 239000011259 mixed solution Substances 0.000 claims description 18
- 238000005189 flocculation Methods 0.000 claims description 17
- 230000016615 flocculation Effects 0.000 claims description 17
- 239000000843 powder Substances 0.000 claims description 17
- 239000008367 deionised water Substances 0.000 claims description 16
- 229910021641 deionized water Inorganic materials 0.000 claims description 16
- 239000003350 kerosene Substances 0.000 claims description 16
- 239000002904 solvent Substances 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 14
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 13
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 claims description 13
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims description 13
- 239000001099 ammonium carbonate Substances 0.000 claims description 13
- QUXFOKCUIZCKGS-UHFFFAOYSA-N bis(2,4,4-trimethylpentyl)phosphinic acid Chemical compound CC(C)(C)CC(C)CP(O)(=O)CC(C)CC(C)(C)C QUXFOKCUIZCKGS-UHFFFAOYSA-N 0.000 claims description 13
- 229910000838 Al alloy Inorganic materials 0.000 claims description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 229910017604 nitric acid Inorganic materials 0.000 claims description 12
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 12
- 229910021529 ammonia Inorganic materials 0.000 claims description 11
- 238000000889 atomisation Methods 0.000 claims description 11
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 10
- 239000005518 polymer electrolyte Substances 0.000 claims description 7
- 238000012545 processing Methods 0.000 claims description 7
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 6
- 238000010521 absorption reaction Methods 0.000 claims description 6
- 239000003463 adsorbent Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- 230000006698 induction Effects 0.000 claims description 6
- 230000007935 neutral effect Effects 0.000 claims description 6
- 229910001453 nickel ion Inorganic materials 0.000 claims description 6
- 238000002844 melting Methods 0.000 claims description 5
- 230000008018 melting Effects 0.000 claims description 5
- 238000010891 electric arc Methods 0.000 claims description 4
- 238000009692 water atomization Methods 0.000 claims description 4
- 238000003723 Smelting Methods 0.000 claims description 3
- 238000012387 aerosolization Methods 0.000 claims description 3
- 239000002351 wastewater Substances 0.000 claims description 3
- 239000004743 Polypropylene Substances 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
- 125000000129 anionic group Chemical group 0.000 claims description 2
- 229920001155 polypropylene Polymers 0.000 claims description 2
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims 1
- 235000011941 Tilia x europaea Nutrition 0.000 claims 1
- 239000004571 lime Substances 0.000 claims 1
- 238000004064 recycling Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 4
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- 238000009713 electroplating Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 239000012071 phase Substances 0.000 description 20
- 239000000284 extract Substances 0.000 description 11
- 235000011121 sodium hydroxide Nutrition 0.000 description 10
- 239000003795 chemical substances by application Substances 0.000 description 8
- 239000007791 liquid phase Substances 0.000 description 8
- 230000008929 regeneration Effects 0.000 description 8
- 238000011069 regeneration method Methods 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 238000007747 plating Methods 0.000 description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 5
- 235000017550 sodium carbonate Nutrition 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- 239000011593 sulfur Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000010791 quenching Methods 0.000 description 2
- 230000000171 quenching effect Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 229910000906 Bronze Inorganic materials 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 239000010974 bronze Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 238000009856 non-ferrous metallurgy Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- 229910000406 trisodium phosphate Inorganic materials 0.000 description 1
- 235000019801 trisodium phosphate Nutrition 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Manufacture And Refinement Of Metals (AREA)
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Families Citing this family (9)
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CN107151739B (zh) * | 2017-07-07 | 2019-06-25 | 金川集团股份有限公司 | 一种低镍高铁合金粉的硝酸全浸方法 |
CN109179756B (zh) * | 2018-09-26 | 2022-02-11 | 衢州华友钴新材料有限公司 | 一种从湿法冶炼钴铜溶液中净化ss的处理工艺 |
CN109852794B (zh) * | 2019-03-11 | 2022-02-15 | 西安蓝晓科技新材料股份有限公司 | 一种用于制备电池级硫酸镍的方法 |
CN109750167A (zh) * | 2019-03-20 | 2019-05-14 | 东北大学 | 一种从镍基高温合金切削废料中回收镍的方法 |
CN110607439A (zh) * | 2019-09-12 | 2019-12-24 | 金川集团股份有限公司 | 一种球形氧化亚镍分段氧化酸浸处理方法 |
CN111304446A (zh) * | 2020-03-31 | 2020-06-19 | 中国科学院金属研究所 | 一种高温合金废料分段浸出综合利用的方法 |
CN112897598A (zh) * | 2021-02-07 | 2021-06-04 | 阳江市联邦金属化工有限公司 | 一种超细氧化亚镍的制备方法 |
CN113666437B (zh) * | 2021-07-15 | 2022-11-15 | 广东邦普循环科技有限公司 | 由镍铁铜合金制备硫酸镍的方法 |
CN114517263B (zh) * | 2022-02-21 | 2023-07-21 | 中南大学 | 一种从含镍废弃电容材料提取回收镍与制备镍产品的方法 |
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CN101195870A (zh) * | 2007-12-25 | 2008-06-11 | 金川集团有限公司 | 一种镍钴废合金的处理方法 |
CN101824540A (zh) * | 2009-12-10 | 2010-09-08 | 佛山市邦普镍钴技术有限公司 | 一种从含镍、锡废旧物料中分离回收金属镍、锡的方法 |
CN102417987A (zh) * | 2011-08-09 | 2012-04-18 | 朱小红 | 从电镀污泥中回收有价金属的方法 |
CN102925695A (zh) * | 2012-10-20 | 2013-02-13 | 贵研铂业股份有限公司 | 一种废旧高温合金物料的镍和钴浸出方法 |
CN103131859B (zh) * | 2013-03-06 | 2014-07-30 | 昆明理工大学 | 高温合金废料金属综合回收的方法 |
CN103334017A (zh) * | 2013-07-01 | 2013-10-02 | 贵研铂业股份有限公司 | 从废旧高温合金中制备高纯镍粉的方法 |
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Denomination of invention: Method for regenerating high-purity nickel sulfate from nickel-based alloy waste material Effective date of registration: 20200408 Granted publication date: 20170412 Pledgee: Xi'an Science and Technology Financial Service Center Co., Ltd. Pledgor: XI'AN RAREALLOYS Co.,Ltd. Registration number: Y2020610000036 |
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