CN104650264A - Method for extracting inulin - Google Patents
Method for extracting inulin Download PDFInfo
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- CN104650264A CN104650264A CN201410291754.7A CN201410291754A CN104650264A CN 104650264 A CN104650264 A CN 104650264A CN 201410291754 A CN201410291754 A CN 201410291754A CN 104650264 A CN104650264 A CN 104650264A
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- inulin
- minutes
- jerusalem artichoke
- extracting
- dry powder
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Abstract
The invention discloses a method for extracting inulin, and belongs to the technical field of chemical extraction. The method comprises the following specific steps: cleaning jerusalem artichoke; peeling off; slicing; drying; crushing; adding water to be dissolved; extracting through microwave; digesting through hot water to obtain coarse extracted liquid; feeding the coarse extracted liquid into an ionic exchange resin tower to discolor so as to obtain a refined inulin solution; concentrating by pressure reduction; freezing and drying to obtain inulin. The method is short in extraction time; the extracted inulin is high in purity and degree of polymerization.
Description
Technical field
The present invention relates to chemical industry extractive technique field, especially a kind of extracting method of inulin.
Background technology
Inulin, has another name called synanthrin, is the mixture of a class natural fruit glycan, is mainly derived from the Liliaceae in 11 sections such as the composite family in dicotyledons, campanulaceae, Gentianaceae and monocotyledons, grass tree section.Inulin is very good functional food ingredient, is also the raw material producing the products such as oligofructose, polyfructosan, high fructose syrup, crystal diabetin simultaneously.At present, the extraction of inulin mainly with jerusalem artichoke, witloof and Folium Agaves variegatae for raw material, adopt organic solvent lixiviate, the method for hot water extraction or biological enzyme lixiviate extracts inulin, the problems such as it is lower that these methods exist extraction efficiency, and gained inulin purity is low, the polymerization degree is low.
Summary of the invention
The object of this invention is to provide a kind of extracting method of inulin, this method can solve the problem that extraction efficiency is lower and gained inulin purity is low, the polymerization degree is low.
In order to solve the problem, the technical solution used in the present invention is: a kind of extracting method of inulin, comprises the following steps:
The impurity of A, removing jerusalem artichoke, use clear water wash clean, peeling, section, dry, pulverize, obtain 70 order ~ 100 order dry powder;
B, described dry powder to be dissolved in water, then to adopt microwave extracting to extract; Wherein, the mass ratio of described water and described dry powder is 9 ~ 10:1, and described microwave extracting power is 500 watts ~ 550 watts, and the microwave extracting time is 3 minutes ~ 5 minutes;
C, hot water extraction 40 minutes ~ 60 minutes, obtain crude extract; Wherein, the temperature of described hot water is 70 DEG C ~ 90 DEG C;
D, described crude extract is passed into exchange resin tower carry out desolventing technology, obtain the jerusalem artichoke solution refined; Wherein, bleaching time is 2 hours ~ 2.5 hours;
E, described refining jerusalem artichoke solution is carried out concentrating under reduced pressure, lyophilize, obtain inulin.
Owing to have employed technique scheme, the present invention compared with prior art has following beneficial effect:
This technique adopts the method for microwave technology assisted extraction,
1, the present invention adopts microwave extracting in conjunction with the method for hot water extraction, shorten extraction time, improve the extraction efficiency of inulin, and the biological activity extracting the inulin of gained is good, solubleness is high.
2, energy-conservation, efficient, the non-secondary pollution of the present invention, and easily manipulate, products obtained therefrom stable in properties, purity are high, the polymerization degree is high.
3, the present invention adopts ion exchange resin to carry out desolventing technology, and decolorizing effect is better.
Embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
Get 9.85 kilograms of fresh jerusalem artichokes, removing surface impurity, then uses clear water wash clean, peeling, and section, dry, pulverize, obtain 1 kilogram, 70 order ~ 100 order dry powder; Joined in 9 kilograms of pure water, stirring and dissolving, proceeds to Microwave Extraction Apparatus, and under the power of 500 watts, extract 5 minutes, proceed in water-bath, be heated to 70 DEG C, hot water extraction 40 minutes, obtains crude extract; Crude extract is passed into exchange resin tower and carry out desolventing technology 2 hours, obtain the jerusalem artichoke solution refined; Refining jerusalem artichoke solution is carried out concentrating under reduced pressure, lyophilize, obtains inulin.
Measure the purity of the inulin that this enforcement is extracted and the polymerization degree, purity is 83.4%, and the polymerization degree is 35; Purity and the polymerization degree of the inulin prepared by employing the present embodiment method are all higher.
Embodiment 2
Get 9.69 kilograms of fresh jerusalem artichokes, removing surface impurity, then uses clear water wash clean, peeling, and section, dry, pulverize, obtain 1 kilogram, 70 order ~ 100 order dry powder; Joined in 9.5 kilograms of pure water, stirring and dissolving, proceeds to Microwave Extraction Apparatus, and under the power of 550 watts, extract 4 minutes, proceed in water-bath, be heated to 90 DEG C, hot water extraction 50 minutes, obtains crude extract; Crude extract is passed into exchange resin tower and carry out desolventing technology 2.5 hours, obtain the jerusalem artichoke solution refined; Refining jerusalem artichoke solution is carried out concentrating under reduced pressure, lyophilize, obtains inulin.
Measure the purity of the inulin that this enforcement is extracted and the polymerization degree, purity is 84.2%, and mean polymerisation degree is 32; Purity and the polymerization degree of the inulin prepared by employing the present embodiment method are all higher.
Embodiment 3
Get 10.02 kilograms of fresh jerusalem artichokes, removing surface impurity, then uses clear water wash clean, peeling, and section, dry, pulverize, obtain 1 kilogram, 70 order ~ 100 order dry powder; Joined in 10 kilograms of pure water, stirring and dissolving, proceeds to Microwave Extraction Apparatus, and under the power of 525 watts, extract 3 minutes, proceed in water-bath, be heated to 80 DEG C, hot water extraction 60 minutes, obtains crude extract; Crude extract is passed into exchange resin tower and carry out desolventing technology 2.25 hours, obtain the jerusalem artichoke solution refined; Refining jerusalem artichoke solution is carried out concentrating under reduced pressure, lyophilize, obtains inulin.
Measure the purity of the inulin that this enforcement is extracted and the polymerization degree, purity is 83.5%, and mean polymerisation degree is 33; Purity and the polymerization degree of the inulin prepared by employing the present embodiment method are all higher.
Claims (1)
1. an extracting method for inulin, is characterized in that comprising the following steps:
The impurity of A, removing jerusalem artichoke, use clear water wash clean, peeling, section, dry, pulverize, obtain 70 order ~ 100 order dry powder;
B, described dry powder to be dissolved in water, then to adopt microwave extracting to extract; Wherein, the mass ratio of described water and described dry powder is 9 ~ 10:1, and described microwave extracting power is 500 watts ~ 550 watts, and the microwave extracting time is 3 minutes ~ 5 minutes;
C, hot water extraction 40 minutes ~ 60 minutes, obtain crude extract; Wherein, the temperature of described hot water is 70 DEG C ~ 90 DEG C;
D, described crude extract is passed into exchange resin tower carry out desolventing technology, obtain the jerusalem artichoke solution refined; Wherein, bleaching time is 2 hours ~ 2.5 hours;
E, described refining jerusalem artichoke solution is carried out concentrating under reduced pressure, lyophilize, obtain inulin.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410291754.7A CN104650264A (en) | 2014-06-26 | 2014-06-26 | Method for extracting inulin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410291754.7A CN104650264A (en) | 2014-06-26 | 2014-06-26 | Method for extracting inulin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104650264A true CN104650264A (en) | 2015-05-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410291754.7A Pending CN104650264A (en) | 2014-06-26 | 2014-06-26 | Method for extracting inulin |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105661507A (en) * | 2016-01-15 | 2016-06-15 | 王军 | Method for producing inulin, natto and enzyme powder through solid state fermentation |
| CN106674383A (en) * | 2016-12-30 | 2017-05-17 | 晨光生物科技集团股份有限公司 | Industrial method for rapidly and efficiently producing inulin |
| CN109384858A (en) * | 2018-12-12 | 2019-02-26 | 安徽师范大学 | A kind of extraction preparation method of selenium-rich jerusalem artichoke selenium polysaccharide |
| CN110423292A (en) * | 2019-03-13 | 2019-11-08 | 陕西森弗天然制品有限公司 | It is a kind of to continue to exceed filtering method for what inulin extracted |
| CN111019017A (en) * | 2019-12-26 | 2020-04-17 | 陕西森弗天然制品有限公司 | Inulin production circulating concentration method |
Citations (4)
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| CN1919855A (en) * | 2006-09-21 | 2007-02-28 | 贵州大学 | Method of extracting inulin assisted with microwave technique |
| CN101402984A (en) * | 2008-11-12 | 2009-04-08 | 南京泛成生物化工有限公司 | Method for extracting inulin with assistance of biological enzyme |
| US20110081449A1 (en) * | 2008-06-12 | 2011-04-07 | Lena De Leenheer | Fructooligosaccharide composition, process for its production and use |
| CN102180995A (en) * | 2011-04-21 | 2011-09-14 | 山东省科学院能源研究所 | Method for extracting synanthrin from jerusalem artichoke |
-
2014
- 2014-06-26 CN CN201410291754.7A patent/CN104650264A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1919855A (en) * | 2006-09-21 | 2007-02-28 | 贵州大学 | Method of extracting inulin assisted with microwave technique |
| US20110081449A1 (en) * | 2008-06-12 | 2011-04-07 | Lena De Leenheer | Fructooligosaccharide composition, process for its production and use |
| CN101402984A (en) * | 2008-11-12 | 2009-04-08 | 南京泛成生物化工有限公司 | Method for extracting inulin with assistance of biological enzyme |
| CN102180995A (en) * | 2011-04-21 | 2011-09-14 | 山东省科学院能源研究所 | Method for extracting synanthrin from jerusalem artichoke |
Non-Patent Citations (2)
| Title |
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| 肖仔君等: ""菊芋中菊粉提取工艺的研究"", 《现代食品科技》 * |
| 胡秀沂等: ""新鲜菊芋的预处理及微波辅助提取菊粉的研究"", 《食品工业科技》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105661507A (en) * | 2016-01-15 | 2016-06-15 | 王军 | Method for producing inulin, natto and enzyme powder through solid state fermentation |
| CN106674383A (en) * | 2016-12-30 | 2017-05-17 | 晨光生物科技集团股份有限公司 | Industrial method for rapidly and efficiently producing inulin |
| CN106674383B (en) * | 2016-12-30 | 2019-05-14 | 晨光生物科技集团股份有限公司 | A kind of industrial method quickly, efficiently producing inulin |
| CN109384858A (en) * | 2018-12-12 | 2019-02-26 | 安徽师范大学 | A kind of extraction preparation method of selenium-rich jerusalem artichoke selenium polysaccharide |
| CN110423292A (en) * | 2019-03-13 | 2019-11-08 | 陕西森弗天然制品有限公司 | It is a kind of to continue to exceed filtering method for what inulin extracted |
| CN111019017A (en) * | 2019-12-26 | 2020-04-17 | 陕西森弗天然制品有限公司 | Inulin production circulating concentration method |
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Application publication date: 20150527 |