CN1045636C - Equipment and process for injection deposition - Google Patents

Equipment and process for injection deposition Download PDF

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Publication number
CN1045636C
CN1045636C CN95110862A CN95110862A CN1045636C CN 1045636 C CN1045636 C CN 1045636C CN 95110862 A CN95110862 A CN 95110862A CN 95110862 A CN95110862 A CN 95110862A CN 1045636 C CN1045636 C CN 1045636C
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China
Prior art keywords
cooling
nozzle
matrix
crucible
jet
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CN95110862A
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CN1140767A (en
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陈振华
蒋向阳
杨伏良
周多三
张豪
陈刚
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Central South University
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Central South University
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Abstract

The present invention relates to a device and technology for spray deposition. Compared with the traditional devices, the device of the present invention is additionally provided with a motion control device, an external intensive cooling device and a connecting plate; a crucible, a nozzle and the external intensive cooling device are fixed on the connecting plate of which the motion is controlled by the motion control device; a cooling medium is liquid nitrogen or inert gas; a plain nozzle can be used for completing the production of large blanks; the superheating temperature of molten metal is selected from 100 to 200 DEG C, the spraying distance is from 150 to 200mm, atomization air pressure is from 1.0 to 1.2MPa and the outlet aperture of the nozzle is from 2.8 to 3.0mm. The present invention has the advantages of great increase of sediment cooling speed which is increased from 10 to 10<2>k/s to 10<3> to 10<5>k/s, large dimensions of spray deposition blanks and high precision.

Description

Jet deposition equipment
The present invention relates to the production unit of a kind of alloy or matrix material, particularly jet deposition equipment.
At present, spray deposition technology has been widely used for the production of alloys such as various pipes, slab, excellent base and matrix material, all be the jet deposition principle that has adopted Britain Asinger professor to propose the seventies on this technological essence: being about to that molten metal or alloy atomize in inert atmosphere is that particle jetting liquid flows, inject directly on the colder matrix, through moving to and froly hit, coalescent, be frozen into settling, its common feature is that settling forms through the matrix deposition by spray liquid flow is disposable." Arms Material scientific and engineering " the 17th volume has been introduced the equipment and the technological process of this technology the 2nd phase (in March, 1994).Compare with common casting one press working and powder metallurgy, its apparatus and process is simple, can reduce many manufacturing procedures, the using rate of metal height, and can save a large amount of energy consumptions.Traditional splashing device generally adopts equipment as shown in Figure 1 and Figure 2, comprising crucible 1, nozzle 2, base stop 3, atomizing space 4, vapor pipe 5, transmission mechanism 6, interior device for cooling 7, though its atomization process speed of cooling is higher, reach 10 3-10 5K/t, but deposits cool speed generally only is 10-10 2K/s, simultaneously when the bigger pipe of preparation diameter, heavy-walled tube base, wide and thick slab, finish size often difficulty reaches requirement, because if solve by improving injection density, because condensing rate is unhappy, causes sedimental segregation, grain coarsening, pyrocondensation hole defect, as adopting v type nozzle, shaking scan nozzle or a plurality of nozzle, technology is very complicated again, and sedimental like this size is very limited.
The new installation that the purpose of this invention is to provide a kind of jet deposition to accelerate speed of cooling, increases the size of jet sediment, improves and sprays large-scale blank quality, does not make equipment, process complications simultaneously again.
Jet deposition equipment of the present invention has increased motion control device 8, outer strong device for cooling 9 and web plate 10, the nozzle 2 and the outer conduit 11 of device for cooling 9 by force that fuse with crucible all pass web plate 10, and be fastened on the web plate 10, with the web plate 10 common crucible systems of forming, web plate 10 is promptly as the loam cake of spray chamber 4, motion control device 8 acts on the web plate 10, the motion of control crucible system, and the size and Orientation of its speed all can be regulated.Outer strong device for cooling 9 comprises air feed bottle, switch-valve and conduit 11, and its effect is: after spray liquid flow 13 was sprayed onto on the matrix 3, outer strong device for cooling 9 conduit jet orifices 12 are the shower cooling medium immediately, and settling 14 is carried out external cooling, and its heat-eliminating medium is liquid nitrogen or rare gas element.According to the difference of spraying blank, the movement locus of crucible system and outer strong device for cooling 9 are also inequality, when spraying tubing, as shown in Figure 3, the conduit jet orifice 12 of outer strong external cooler 9 is positioned at matrix 3 belows, and is relative with nozzle 2, and crucible system is made approximate linear uniform motion along the bus of matrix 3, matrix 3 buses are done uniform rotation around its axis again simultaneously, and the deposition track that metal jet liquid is injected on the matrix 3 is a circular helix; When spraying slab, as shown in Figure 4, outer strong device for cooling 9 respectively has a conduit jet orifice 12 in the nozzle both sides, different motion direction according to crucible system, open corresponding conduit jet orifice respectively and close an other conduit jet orifice, heat-eliminating medium is sprayed into after every layer of spray liquid flow 13 depositions just, every surface sediments 14 is carried out external cooling, crucible system is reciprocating along 3 liang of parallel edges of plane tabular matrix, matrix 3 is simultaneously reciprocating perpendicular to crucible system direction of motion, and the deposition track that metal jet liquid is injected on the matrix 3 is a sinusoidal curve.In the moving process, the conduit jet orifice 12 of conduit 11 is constant all the time with the relative position of nozzle.Settling 14 each layers that make so all are the results of crucible system and more than 3 motion of matrix; The homogeneity of alloy or matrix material, planarization all improve greatly than the one-sided motion of matrix.According to different deposit preform sizes, can adjust the move distance of corresponding crucible system, matrix 3, and adjust the movement velocity of crucible system, matrix 3, can satisfy the different performance requirement of deposit preform.
When utilizing aforesaid device to produce alloy or matrix material, the optimum deposition condition of multilayer spray depends on temperature of superheat, gas and mass ratio, jet length and the matrix 3 of metal injection liquid stream of metal liquid, the movement velocity of crucible system.But because matrix 3 to-and-fro movements, in the multi-level jet deposition, a back settling of same position arrives apart from the timed interval that last settling arrives long, last surface sediments ratio is easier to sputter and solidifies, form the sputter border easily, the quality of blank is sprayed in influence, for guaranteeing that back one deck jet sediment arrives the incomplete sputter of last surface sediments before and solidifies, eliminate the sputter border, realize optimum deposition condition, in the processing parameter of production process, the temperature of superheat of molten metal is chosen 100-200 ℃, jet length is with 150~200mm, atomization air pressure is 1~1.21MPa, jet exit footpath 28~30mm, the frequency that matrix 3 rotates or moves (all numbers that the unit time endobasal-body rotates or round mobile number of times) avoids selecting for use the multiple relation with the travel frequency of crucible 1, the general available 1/10~1/6Hz of the motion frequency of crucible, the motion frequency of matrix can be with 1/40~1/30Hz, when needs are made long tube and slab spare, also can use many group crucibles simultaneously, nozzle and conduit jet orifice satisfy optimum deposition condition.In addition, with different crucibles put different molten metals respectively, when strengthening producing matrix material mutually, the homogeneity of matrix material improves greatly.
Owing to adopted above-mentioned technology, accelerated sedimental speed of cooling greatly, make sedimental sedimentation velocity by 10~10 2K/s brings up to 10 3-10 4K/s, when spraying large-scale blank, realize optimum deposition condition easily, increased the size of spraying blank, can produce Φ 270 * 350mm, wall thickness is 30kg for the 80mm quality so that bigger alloy aluminum ingot is compared with crucible or the one-sided motion of matrix, improved the precision of deposition blank greatly, made blank smooth, even.Simultaneously, the uniform distribution of strengthening phase for matrix material again provides a kind of novel method.
Fig. 1 is conventional spray deposition pipe production unit synoptic diagram;
Garden 2 is conventional spray deposition slab production unit synoptic diagram;
Fig. 3 is a jet deposition pipe production unit synoptic diagram of the present invention;
Fig. 4 is a jet deposition slab production unit synoptic diagram of the present invention.
Embodiment 1 usefulness aluminium-iron-alum-silicon is raw material, with its fusing, temperature of superheat is chosen 200 ℃, jet length 153mm in crucible 1, atomization gas pressure 1.2MPa, jet exit footpath 2.9mm, the frequency that matrix rotates is 80 rev/mins, it is 7 times/minute that crucible 1 comes and goes frequency, producing size internal diameter Φ is 124mm, external diameter Φ is 290mm, and long L is 300mm, and weight is the aluminium alloy pipe of 30Kg.The heat-eliminating medium that outer strong device for cooling 9 uses is rare gas element, crucible system is by the driven by motor rotating disk of motion control device 8, by the connecting rod transmission belt plate 10 that is dynamically connected, the motion of control crucible system, make crucible system do the average rate to-and-fro movement along the matrix bus, move distance is 250mm.Its deposits cool speed reaches 10 4K/s.

Claims (6)

1. jet deposition equipment, comprise crucible, nozzle, matrix, spray chamber, vapor pipe, transmission mechanism, interior device for cooling, it is characterized in that: the sedimental outer strong device for cooling of motion control device, cooling that also has the motion of web plate and control linkage plate, the nozzle and the outer conduit of device for cooling by force that fuse with crucible all pass web plate, and are fastened on the web plate.
2. jet deposition equipment according to claim 1, it is characterized in that: the jet length of nozzle and matrix is 150~200mm, atomization air pressure is 1.0~1.2MPa, jet exit footpath 2.8~3.0mm, the motion frequency 1/10-1/6Hz of crucible, the matrix motion frequency is with 1/40~1/30Hz, and the frequency that crucible can not move the multiple relation with the matrix motion frequency.
3. jet deposition equipment according to claim 1 and 2 is characterized in that: the heat-eliminating medium in the outer strong device for cooling is liquid nitrogen or rare gas element.
4. jet deposition equipment according to claim 1 and 2 is characterized in that: crucible does reciprocating linear motion along the matrix bus, and the catheter nozzle of outer strong device for cooling is opened in the matrix below, over against nozzle.
5. jet deposition equipment according to claim 1 and 2, it is characterized in that: crucible is made complex line along the matrix parallel edges and is moved, the pipe inspection mouth of outer strong device for cooling is positioned at the nozzle both sides, and in the moving process, the conduit jet orifice of outer strong device for cooling and the relative position of nozzle become down.
6. jet deposition equipment according to claim 1 and 2 is characterized in that: the conduit jet orifice that many group crucibles, nozzle and outer strong device for cooling are arranged on the web plate.
CN95110862A 1995-07-17 1995-07-17 Equipment and process for injection deposition Expired - Fee Related CN1045636C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN95110862A CN1045636C (en) 1995-07-17 1995-07-17 Equipment and process for injection deposition

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Application Number Priority Date Filing Date Title
CN95110862A CN1045636C (en) 1995-07-17 1995-07-17 Equipment and process for injection deposition

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CN1140767A CN1140767A (en) 1997-01-22
CN1045636C true CN1045636C (en) 1999-10-13

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CN102151828A (en) * 2011-03-18 2011-08-17 西南交通大学 Method for preparing gradient materials through multi-crucible and multi-nozzle spray forming
CN102277132A (en) * 2011-06-11 2011-12-14 山东理工大学 Structural form control method for preparing magnetic grinding materials by air atomization quick-setting process
CN102626843A (en) * 2012-02-17 2012-08-08 汤汉良 Manufacturing method for automobile parts made of aluminum-based composite material through spray deposition
CN103510033B (en) * 2012-06-28 2017-07-28 富瑞精密组件(昆山)有限公司 The preparation method of metal works
CN102909328B (en) * 2012-10-25 2016-02-03 苏州金江铜业有限公司 A kind of Apparatus for () and method therefor of jet deposition manufactured copper alloy strip
CN103785833B (en) * 2014-01-24 2016-01-20 江苏理工学院 Multi-nozzle 3D printing device for aluminum alloy plates
CN104607642B (en) * 2015-01-29 2017-10-27 天津百恩威新材料科技有限公司 Spray chamber down cycles system and the method cooled using the system to spray chamber
CN105671474B (en) * 2016-03-18 2018-11-30 李光武 The method and apparatus for manufacturing semiconductor chip
CN107460426A (en) * 2017-09-19 2017-12-12 湖南三泰新材料股份有限公司 A kind of device of jet deposition billet surface composite
CN110965011B (en) * 2019-12-30 2022-05-17 格林美股份有限公司 Motor rotor collecting ring repairing device
CN115007867B (en) * 2022-06-30 2024-01-19 东北大学 Method for preparing metal material by spray forming and spray forming device

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0151511A1 (en) * 1984-01-11 1985-08-14 National Research Development Corporation Spray deposition of metal
EP0163776A2 (en) * 1984-01-18 1985-12-11 James A. Browning Highly concentrated supersonic flame spray method and apparatus with improved material feed
US4804034A (en) * 1985-03-25 1989-02-14 Osprey Metals Limited Method of manufacture of a thixotropic deposit
US4926923A (en) * 1985-03-25 1990-05-22 Osprey Metals Ltd. Deposition of metallic products using relatively cold solid particles
US5401539A (en) * 1985-11-12 1995-03-28 Osprey Metals Limited Production of metal spray deposits

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0151511A1 (en) * 1984-01-11 1985-08-14 National Research Development Corporation Spray deposition of metal
EP0163776A2 (en) * 1984-01-18 1985-12-11 James A. Browning Highly concentrated supersonic flame spray method and apparatus with improved material feed
US4804034A (en) * 1985-03-25 1989-02-14 Osprey Metals Limited Method of manufacture of a thixotropic deposit
US4926923A (en) * 1985-03-25 1990-05-22 Osprey Metals Ltd. Deposition of metallic products using relatively cold solid particles
US5401539A (en) * 1985-11-12 1995-03-28 Osprey Metals Limited Production of metal spray deposits

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