CN104496416B - The manufacture method of the transparent pea green starved glaze of your porcelain - Google Patents
The manufacture method of the transparent pea green starved glaze of your porcelain Download PDFInfo
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- CN104496416B CN104496416B CN201410700559.5A CN201410700559A CN104496416B CN 104496416 B CN104496416 B CN 104496416B CN 201410700559 A CN201410700559 A CN 201410700559A CN 104496416 B CN104496416 B CN 104496416B
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- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 229910052925 anhydrite Inorganic materials 0.000 claims abstract description 32
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims abstract description 32
- 235000015895 biscuits Nutrition 0.000 claims abstract description 26
- 238000001238 wet grinding Methods 0.000 claims abstract description 20
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 16
- 229910001719 melilite Inorganic materials 0.000 claims abstract description 16
- 239000010453 quartz Substances 0.000 claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims abstract description 11
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 230000001590 oxidative effect Effects 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 13
- 238000010792 warming Methods 0.000 claims description 13
- 239000011505 plaster Substances 0.000 claims description 4
- 239000010803 wood ash Substances 0.000 claims description 2
- 239000003638 chemical reducing agent Substances 0.000 claims 1
- 239000003513 alkali Substances 0.000 abstract description 5
- 239000003795 chemical substances by application Substances 0.000 abstract description 5
- 238000009413 insulation Methods 0.000 abstract description 3
- 235000019628 coolness Nutrition 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 11
- 239000002585 base Substances 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 244000025254 Cannabis sativa Species 0.000 description 2
- 210000003298 dental enamel Anatomy 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 101100002917 Caenorhabditis elegans ash-2 gene Proteins 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000931705 Cicada Species 0.000 description 1
- 241000371997 Eriocheir sinensis Species 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 208000031481 Pathologic Constriction Diseases 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 210000001215 vagina Anatomy 0.000 description 1
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- Adornments (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The manufacture method of the transparent pea green starved glaze of your porcelain, takes melilite 5% 10%, calcite 10% 20%, white Anhydrite 45% 65%, black Anhydrite 15% 22%, quartz 5% 10%, plant ash 1% 3% make glaze, and the glaze powder chosen is broken to 40 mesh respectively；Mill, remove the ferrum that swims in glaze slip with bar magnet, prepare glaze.Take Kaolin as blank, add the water of weight 45% 50% and 0.3% 0.5% aqueous alkali agent wet grinding 8 13 hours after, slip makes blank, burns to 800 DEG C of 900 DEG C of natural coolings and obtains biscuit, after glazing bottom finishing, the glaze layer on surface and uneven part；Load kiln, oxidizing atmosphere is gradually warmed up to 1040 DEG C, change reducing atmosphere into and be to slowly warm up to 1250 DEG C of insulations 10 minutes, cease fire；Cooling i.e. completes.
Description
Technical field
The present invention relates to the processing technology of a kind of porcelain, the manufacture method of the transparent pea green glaze of your porcelain a kind of.
Background technology
Your porcelain is one of our five your name's porcelain, and the Ruyao in later stage in the Northern Song Dynasty aims at imperial palace and burns and make hired porcelain, i.e. " official you porcelain "
It is called for short your porcelain.Its glaze colours is characterized as characteristic glaze such as " green grass or young crops such as sky, faces such as jade, cicada's wings stricture of vagina, stars at dawn are dilute, Ungula Eriocheir sinensis, Pericarpium Pyri, Flos Sesami indici "
Color, your porcelain mostly makes with form modelled after an antique and produces at present.And your enamel common is thicker.Conventional traditional handicraft is being fired
During, temperature is the highest usually more than 1250 DEG C, and the rate of burning till is relatively low. energy resource consumption great efforts.
Summary of the invention
The technical problem to be solved is to provide the manufacture method of the transparent pea green starved glaze of your porcelain a kind of, make you
Enamel is thin, the gentle exquisiteness in surface, it can be seen that exquisite pattern, grace attractive in appearance on base substrate.
The present invention be the technical scheme is that by above-mentioned technical problem
The manufacture method of the transparent pea green starved glaze of your porcelain, comprises the following steps:
Step one: choose melilite, calcite, white Anhydrite, black Anhydrite, quartz, plant ash respectively as glaze raw material, by weight
Amount ratio is melilite 5%-10%, calcite 10%-16%, white Anhydrite 45%-64%, black Anhydrite 15%-22%, quartz 5%-10%, grass
Wood ash 1%-3%；The raw material chosen is crushed to respectively 40 mesh, standby；
Step 2: the glaze raw material mixing such as melilite, calcite, white Anhydrite, black Anhydrite and plant ash that step one is chosen,
Being mixed glaze and add ball mill, be subsequently adding the water that mixed material weight is 45-58% and carry out wet grinding, the wet grinding time is 12-
20 hours, the glaze slip after wet grinding crossed 150 mesh sieves, removed the ferrum that swims in glaze slip with Magnet, standby；
Step 3: choose Kaolin as base raw material, puts into ball mill after being broken into pieces, add billet weight 45-50%'s
The aqueous alkali agent of water and 0.3%-0.5%, wet grinding 8-13 hour, pug was starched 120 mesh sieves, and was removed foreign material and remove mud with bar magnet
Take out after the ferrum that swims in slip, standby；
Step 4: the mud that step 3 prepares is adjusted its concentration at 48 °-52 °, the mud that mix up is injected in plaster mold half
Individual about many hours overfalls, make blank, and blank is cool to be repaired to partial desiccation, then fully parching rear biscuiting 5 hours,
Biscuit is taken out to obtain after natural cooling, standby；
Step 5: glaze concentration step 2 prepared out is adjusted to Baume degrees 58 °-62 °, then step 4 is prepared
Surface dirt cleared up by biscuit, then is dipped into by biscuit in glaze slip, and the glaze thickness waiting its biscuit face to adhere to reaches 0.2-
Take out after 0.3mm, the bubble bottom finishing base, on surface glaze layer and uneven part；
Step 6: put into the kiln putting up rack-layer, in oxidizing atmosphere after step 5 is trimmed the biscuit airing of glaze layer
In be gradually heating to 1040 DEG C, wherein, in kiln, room temperature is warming up to 300 DEG C, and the time is 1 hour, is warming up to 900 DEG C from 300 DEG C,
Time is 4 hours, and 1040-1050 DEG C of steady fire reduces by force 30 minutes；The most gradually being to slowly warm up to 1250-1255 DEG C, the time is
6-7 hour, after having heated up, it is incubated 10 minutes again；Cease fire, natural cooling, completing of the transparent pea green starved glaze of your porcelain.
The medicine have the advantages that the present invention uses special process and glaze, will have your porcelain of milkiness sense and transparent feel
Glaze presents pea green transparent river starved glaze state, and color and luster is gentle, simple and elegant, elegant, simple and easy, thus produces a kind of brand-new vision
Impact and artistic effect, innovate in tradition, makes the breakthrough of your solid existing tradition innovation, enriches your culture of porcelain intension, carry
The high artistry of your porcelain products, added value, market share and impulsive force.
Detailed description of the invention
The present invention is further simply analysed below in conjunction with specific embodiment.Involved method step in following embodiment, as
Without special instruction, it is convenient source or commercially available.
Embodiment 1
The manufacture method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose respectively melilite, calcite, white Anhydrite, black Anhydrite, quartz, plant ash, as glaze raw material, press
Part by weight melilite 5%, calcite 10%, white Anhydrite 64%, black Anhydrite 15%, quartz 5%, plant ash 1%, divide the raw material chosen
It is not crushed to 40 mesh, standby；
Step 2: the glaze raw material mixing such as melilite, calcite, white Anhydrite, black Anhydrite and plant ash that step one is chosen
Glaze adds ball mill, is subsequently adding the water that mixed material part by weight is 50% and carries out wet grinding, and the wet grinding time is 18 hours, wet
Glaze slip after mill crosses 150 mesh sieves, removes the ferrum that swims in glaze slip with bar magnet, standby；
Step 3: choose Kaolin as base raw material, puts into ball mill after being broken into pieces by blank, add billet weight 50%
Water and the aqueous alkali agent wet grinding 12 hours of 0.5%, pug starched 120 mesh sieves, remove foreign material and with bar magnet remove in pug slurry floating
Take out after trip ferrum, standby；
Step 4: the mud that step 3 prepares is modulated concentration at 50 °, its mud is injected in plaster mold half an hour
Overfall, makes blank, repairs after blank partial desiccation, then the blank biscuiting after fully parching 6 hours, after natural cooling
Out obtain biscuit, standby；
Step 5: glaze concentration step 2 prepared out is adjusted to Baume degrees 58 °, the biscuit then step 4 prepared
Having cleared up surface dirt and foreign material etc., be dipped in glaze slip by biscuit, the glaze thickness waiting its biscuit face to adhere to reaches
Take out after 0.2mm, the bubble bottom finishing base, on surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer after the biscuit airing of glaze layer being trimmed, in oxidizing atmosphere gradually
Being warming up to 1040 DEG C, being wherein warming up to 300 DEG C of times is 1 hour, and being warming up to 900 DEG C from 300 DEG C is 3 hours, from 900 DEG C of intensifications
It is 1 hour to 1040 DEG C of times, is passed directly into carbon monoxide unsteady state operation after 1050 DEG C and becomes reducing atmosphere (by force reduction), and gradually
Being to slowly warm up to 1250 DEG C, the time is 7 hours, steady fire insulation 10 minutes after having heated up；Cease fire；Natural cooling；Your porcelain is saturating
Completing of bright pea green starved glaze.
Embodiment 2
The manufacture method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose melilite, calcite, white Anhydrite, black Anhydrite, quartz, plant ash respectively as glaze raw material, by weight
Amount ratio melilite 10%, calcite 16%, white Anhydrite 45%, black Anhydrite 22%, quartz 5%, plant ash 2%, divide the raw material chosen
It is not crushed to 40 mesh, standby；
Step 2: the melilite that step one is chosen, the glaze raw material mixing such as calcite, white Anhydrite, black Anhydrite and plant ash
Glaze adds ball mill, is subsequently adding the water that mixed material part by weight is 45% and carries out wet grinding, and the wet grinding time is 20 hours,
Glaze slip after wet grinding crosses 150 mesh sieves, and the ferrum that swims removed in glaze slip with bar magnet takes out in holding bucket, standby；
Step 3: choose Kaolin as base raw material, puts into ball mill after being broken into pieces by blank, add billet weight 45%
Water and the aqueous alkali agent of 0.45%, wet grinding 10 hours, pug was starched 120 mesh sieves, and was removed foreign material and remove in pug slurry with bar magnet
Swim ferrum, standby；
Step 4: the mud that step 3 prepares is modulated concentration at 52 °, its mud is injected in plaster mold 35 minutes and returns
Slurry, makes blank, and blank is cool to be repaired to partial desiccation, then fully parching rear biscuiting 5 hours, prepares after natural cooling
Biscuit, standby；
Step 5: glaze concentration step 2 prepared out is adjusted to Baume degrees 58 °, the biscuit then step 4 prepared
Having cleared up surface dirt and foreign material etc., be dipped in glaze slip by biscuit, the glaze thickness waiting its biscuit face to adhere to reaches
Take out after 0.25mm, the bubble on finishing base lower surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer after the biscuit airing of glaze layer being trimmed, in oxidizing atmosphere gradually
Heating up, being warming up to 300 DEG C of times is 1 hour, and it is 3 hours that clump 300 DEG C is warming up to 900 DEG C of times, is warming up to 1050 DEG C from 900 DEG C
Time is 1 hour, is converted into reducing atmosphere after 1050 DEG C, and the time is 6 hours, and is gradually to slowly warm up to 1255 DEG C, has heated up
It is incubated 10 minutes after one-tenth, ceases fire；Natural cooling；Completing of the transparent pea green starved glaze of your porcelain.
Embodiment 3
The manufacture method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose melilite respectively, calcite, white Anhydrite, black Anhydrite, quartz, plant ash make glaze raw material, by weight
Ratio is melilite 8%, calcite 14%, white Anhydrite 50%, black Anhydrite 15%, quartz 10%, plant ash 3%, is divided by the raw material chosen
It is not crushed to 40 mesh, standby；
Step 2: the glaze raw material mixing such as melilite, calcite, white Anhydrite, black Anhydrite and plant ash that step one is chosen
Glaze adds ball mill, is subsequently adding the water that mixed material weight is 50% and carries out wet grinding, and the wet grinding time is 15 hours, wet grinding
After glair cross 150 mesh sieves, remove the ferrum that swims in glaze slip with bar magnet, standby；
Step 3: choose Kaolin as base raw material, puts into ball mill after being broken into pieces by blank, add billet weight 45%
Water and the aqueous alkali agent of 0.3%, wet grinding 10 hours, pug, by 120 mesh sieves, removes foreign material and removes in mud slip with bar magnet
The ferrum that swims after take out, filter moisture with filter, standby；
Step 4: mud step 3 prepared is refined through pug mill, sequences the inside air；, walk is put on Blank drawing machine
Making blank, blank is cool to be repaired to partial desiccation, and finishing impression is bonding etc.；Then little for the blank biscuiting 6 after fully parching
Time, out biscuit after natural cooling, standby；
Step 5: glaze concentration step 2 prepared out is adjusted to Baume degrees 62 °, the biscuit then step 4 prepared
Clear up surface dirt and foreign material etc., the most again biscuit has been dipped in glaze slip, wait the glaze thickness of its biscuit surface attachment
Take out after reaching 0.2mm, the bubble bottom finishing base, on surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer after the biscuit airing of glaze layer being trimmed, in oxidizing atmosphere gradually
Heating up, be warming up to 900 DEG C ° from normal temperature laboratory, its time is 4 hours, and 900 DEG C are warming up to 1040 DEG C, and the time is 1 hour, 1040
Being converted into reducing atmosphere, strong reductase 12 0-30 minute after DEG C, and be gradually to slowly warm up to 1260 DEG C, the time is 7 hours, heats up
Insulation 15 minutes after completing；Cease fire；Natural cooling；Completing of the transparent pea green glaze of your porcelain.
Claims (1)
1. the manufacture method of the transparent pea green starved glaze of your porcelain, it is characterised in that:
Step one, choose melilite, calcite, white Anhydrite, black Anhydrite, quartz, plant ash as glaze raw material respectively, by weight
Example is melilite 5%-10%, calcite 10%-16%, white Anhydrite 45%-64%, black Anhydrite 15%-22%, quartz 5%-10%, plant ash
1%-3%；The raw material chosen is crushed to respectively 40 mesh, standby；
Step 2, the melilite that step one is chosen, calcite, white Anhydrite, black Anhydrite, quartz and the mixing of wood ash glaze raw material,
Being mixed glaze and add ball mill, be subsequently adding the water that mixed material weight is 45-58% and carry out wet grinding, the wet grinding time is 12-
20 hours, the glaze slip after wet grinding crossed 150 mesh sieves, removed the ferrum that swims in glaze slip with Magnet, standby；
Step 3, choose Kaolin as base raw material, after being broken into pieces, put into ball mill, add billet weight 45-50% water and
The water reducer of 0.3%-0.5%, wet grinding 8-13 hour, pug was starched 120 mesh sieves, and was removed foreign material and remove mud slip with bar magnet
Take out after the interior ferrum that swims, standby；
Step 4, the mud that step 3 prepares being adjusted its concentration at 48 °-52 °, the mud that will mix up injects in plaster mold half
Many hours overfalls, make blank, and blank is cool to be repaired to partial desiccation, then fully parching rear biscuiting 5 hours, the coldest
Take out to obtain biscuit the most afterwards, standby；
Step 5, glaze concentration step 2 prepared out are adjusted to Baume degrees 58 °-62 °, the biscuit then step 4 prepared
Clear up surface dirt, then biscuit has been dipped in glaze slip, after the glaze thickness waiting its biscuit face to adhere to reaches 0.2-0.3mm
Take out, the bubble bottom finishing base, on surface glaze layer and uneven part；
Step 6, step 5 is trimmed the biscuit airing of glaze layer after put into the kiln putting up rack-layer, in oxidizing atmosphere by
Gradually being warming up to 1040 DEG C, wherein, in kiln, room temperature is warming up to 300 DEG C, and the time is 1 hour, is warming up to 900 DEG C from 300 DEG C, the time
Being 4 hours, 1040-1050 DEG C of steady fire reduces by force 30 minutes；The most gradually being to slowly warm up to 1250-1255 DEG C, the time is 6-7
Hour, it is incubated 10 minutes after having heated up again；Cease fire, natural cooling, completing of the transparent pea green starved glaze of your porcelain.
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104860725A (en) * | 2015-04-24 | 2015-08-26 | 长沙市望城区盛唐工艺陶瓷有限公司 | Green glaze ceramic artware preparation method |
| CN107162564A (en) * | 2017-05-22 | 2017-09-15 | 苏州太湖窑陶瓷有限公司 | A kind of clear mud porcelain and its preparation technology |
| CN108483918A (en) * | 2018-06-19 | 2018-09-04 | 刘冬青 | Pseudo-classic glaze of your a kind of porcelain and preparation method thereof |
| CN110156437B (en) * | 2019-05-29 | 2021-11-30 | 王晟鸣 | Pink-green glaze Ru porcelain and preparation method thereof |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
| CN111704360B (en) * | 2020-07-13 | 2022-04-22 | 张玉凤 | Antique Ru porcelain green glaze and manufacturing method thereof |
| CN112939464B (en) * | 2021-04-29 | 2022-06-10 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN113387577B (en) * | 2021-07-19 | 2023-02-17 | 河南弘宝汝瓷坊有限公司 | Green glaze for Ru porcelain and preparation method of green glaze Ru porcelain |
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| CN102391018A (en) * | 2011-08-10 | 2012-03-28 | 刘冬青 | Method for making archaistic semimatte thin glaze for Ru porcelain |
| CN102503574A (en) * | 2011-11-01 | 2012-06-20 | 姚瑞平 | Manufacture craft for pale yellowish green colored glaze of Ru porcelain |
| CN102503573A (en) * | 2011-11-01 | 2012-06-20 | 姚瑞平 | Manufacturing technology for Ru porcelain thin-tire thin-glaze |
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2014
- 2014-11-28 CN CN201410700559.5A patent/CN104496416B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102391018A (en) * | 2011-08-10 | 2012-03-28 | 刘冬青 | Method for making archaistic semimatte thin glaze for Ru porcelain |
| CN102503574A (en) * | 2011-11-01 | 2012-06-20 | 姚瑞平 | Manufacture craft for pale yellowish green colored glaze of Ru porcelain |
| CN102503573A (en) * | 2011-11-01 | 2012-06-20 | 姚瑞平 | Manufacturing technology for Ru porcelain thin-tire thin-glaze |
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Effective date of registration: 20170628 Address after: Ruzhou porcelain industry in Pingdingshan city in Henan province 467500 area Patentee after: Henan Hong you Culture & Art Co., Ltd. Address before: Ruzhou City, Pingdingshan City, Henan Province, 467500 riding Ling Fan Ji village 5 groups Patentee before: Feng Yanqin |
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