CN104496416A - Manufacturing method of transparent pea green-color thin glaze of Ru porcelain - Google Patents
Manufacturing method of transparent pea green-color thin glaze of Ru porcelain Download PDFInfo
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- CN104496416A CN104496416A CN201410700559.5A CN201410700559A CN104496416A CN 104496416 A CN104496416 A CN 104496416A CN 201410700559 A CN201410700559 A CN 201410700559A CN 104496416 A CN104496416 A CN 104496416A
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- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 239000010433 feldspar Substances 0.000 claims abstract description 32
- 235000015895 biscuits Nutrition 0.000 claims abstract description 28
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000001238 wet grinding Methods 0.000 claims abstract description 21
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 16
- 238000001816 cooling Methods 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052742 iron Inorganic materials 0.000 claims abstract description 11
- 239000010453 quartz Substances 0.000 claims abstract description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims description 20
- 238000010792 warming Methods 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 239000011505 plaster Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 238000009413 insulation Methods 0.000 abstract description 4
- 239000002002 slurry Substances 0.000 abstract description 4
- 238000005245 sintering Methods 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract 3
- 238000000227 grinding Methods 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 241000196324 Embryophyta Species 0.000 description 12
- 210000003298 dental enamel Anatomy 0.000 description 3
- 238000009966 trimming Methods 0.000 description 3
- 239000003086 colorant Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000479 mixture part Substances 0.000 description 2
- 101100002917 Caenorhabditis elegans ash-2 gene Proteins 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000931705 Cicada Species 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 210000000078 claw Anatomy 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
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- Adornments (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a manufacturing method of transparent pea green-color thin glaze of Ru porcelain. The manufacturing method comprises the following steps of respectively taking 5-10% of melilith, 10-20% of calcite, 45-65% of white feldspar, 15-22% of black feldspar, 5-10% of quartz and 1-3% of plant ash as glaze materials, crushing the glaze materials to powder of 40 meshes, carrying out grinding, removing floating iron in the glaze slurry by a magnet rod so that glaze is obtained, taking kaolin as a blank material, adding 45-50wt% of water and 0.3-0.5wt% of an alkaline water aqua into the blank material, carrying out wet grinding for 8-13h, preparing a blank from the slurry, sintering the blank to a temperature of 800-900 DEG C, carrying out natural cooling to obtain a biscuit, carrying out glazing on the biscuit, finishing the bottom, the surface glaze layer and a nonuniform part, putting the finished biscuit into a kiln, carrying out gradual heating to a temperature of 1040 DEG C in an oxidation atmosphere, carrying out slow heating to a temperature of 1250 DEG C in a reduction atmosphere, carrying out thermal insulation for 10min, stopping heating and carrying out cooling.
Description
Technical field
The present invention relates to a kind of manufacture craft of porcelain, specifically the making method of the transparent pea green glaze of your porcelain a kind of.
Background technology
Your porcelain is one of our five your name's porcelain, and Ruyao in later stage in the Northern Song Dynasty aims at imperial palace and burns and make hired porcelain, and namely " official you porcelain " is called for short your porcelain.Its glaze colours is characterized as characteristic glaze colours such as " blue or green as sky, look like beautiful, cicada's wings line, stars at dawn are rare, crab claw, pears skin, Flos Sesami indici ", your porcelain makes production mainly with form modelled after an antique greatly at present.And your enamel common is thicker.Conventional traditional technology is in sintering procedure, and temperature is also higher is generally more than 1250 DEG C, and rate of burning till is also relatively low. energy consumption great efforts.
Summary of the invention
Technical problem to be solved by this invention is to provide the making method of the transparent pea green starved glaze of your porcelain a kind of, and your enamel made is thin, and surperficial gentle exquisiteness can see exquisite pattern on base substrate, grace attractive in appearance.
The technical scheme that the present invention adopts for above-mentioned technical problem is:
The making method of the transparent pea green starved glaze of your porcelain, comprises the following steps:
Step one: choose melilith, calcite, white feldspar, black feldspar, quartz, plant ash respectively as glaze raw material is melilith 5%-10%, calcite 10%-16%, white feldspar 45%-64%, black feldspar 15%-22%, quartzy 5%-10%, plant ash 1%-3% by weight proportion; The raw material chosen is crushed to 40 orders respectively, for subsequent use;
Step 2: the glaze raw material mixing such as the melilith that step one is chosen, calcite, white feldspar, black feldspar and plant ash, mixed glaze and added ball mill, then adding mixture weight is that the water of 45-58% carries out wet-milling, the wet-milling time is 12-20 hour, glaze slip after wet-milling crosses 150 mesh sieves, with the iron that swims in magnet removing glaze slip, for subsequent use;
Step 3: choose kaolin as base raw material, put into ball mill after being broken into pieces, adds the water of billet weight 45-50% and the buck agent of 0.3%-0.5%, wet-milling 8-13 hour, pug starched 120 mesh sieves, removed foreign material and took out with after the iron that swims in bar magnet removing mud slip, for subsequent use;
Step 4: adjust its concentration at 48 °-52 ° in mud obtained for step 3, to inject in plaster mould overfall about more than half a hour, makes blank by the mud mixed up, blank is cool to be repaired to partial desiccation, then fully parching rear biscuiting 5 hours, biscuit after naturally cooling, is taken out to obtain, for subsequent use;
Step 5: glaze concentration step 2 obtained out is adjusted to degree Beaume 58 °-62 °, then the biscuit that step 4 is obtained has been cleared up surface dirt, again biscuit is dipped in glaze slip, Deng the glaze thickness of its biscuit face attachment reach 0.2-0.3mm after take out, bottom finishing base, bubble on surface glaze layer and uneven part;
Step 6: put into the kiln putting up rack-layer after step 5 being trimmed the biscuit airing of glaze layer, 1040 DEG C are warming up to gradually in oxidizing atmosphere, wherein, in kiln, normal temperature is warming up to 300 DEG C, time is 1 hour, be warming up to 900 DEG C from 300 DEG C, the time is 4 hours, and 1040-1050 DEG C of steady fire reduces 30 minutes by force; Slowly be warming up to 1250-1255 DEG C gradually afterwards, the time is 6-7 hour, is incubated 10 minutes again after having heated up; Cease fire, naturally cooling, completing of the transparent pea green starved glaze of your porcelain.
Beneficial effect of the present invention is: the present invention adopts special process and glaze, your enamel with milkiness sense and transparent feel is presented pea green transparent river starved glaze state, color and luster is gentle, simple and elegant, elegant, simple and easy, thus produce a kind of brand-new visual impact and artistic effect, innovate in tradition, what your solid existing tradition was innovated is breakthrough, has enriched your culture of porcelain intension, has improve the artistry of your porcelain products, added value, share of market and surging force.
Embodiment
The present invention is simply analysed further again below in conjunction with specific embodiment.Involved method steps in following embodiment, if no special instructions, is convenient source or commercially available.
Embodiment 1
The making method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose respectively melilith, calcite, white feldspar, black feldspar, quartz, plant ash, as glaze raw material, melilith 5%, calcite 10%, white feldspar 64%, black feldspar 15%, quartz 5%, plant ash 1% by weight proportion, the raw material chosen is crushed to 40 orders respectively, for subsequent use;
Step 2: the glaze raw material mixing glaze such as melilith step one chosen, calcite, white feldspar, black feldspar and plant ash add ball mill, then add mixture part by weight be 50% water carry out wet-milling, the wet-milling time is 18 hours, glaze slip after wet-milling crosses 150 mesh sieves, with the iron that swims in bar magnet removing glaze slip, for subsequent use;
Step 3: choose kaolin as base raw material, put into ball mill after being broken into pieces by blank, add the water of billet weight 50% and the buck agent wet-milling 12 hours of 0.5%, pug starched 120 mesh sieves, remove foreign material and take out with after the iron that swims in bar magnet removing pug slurry, for subsequent use;
Step 4: mud obtained for step 3 is modulated concentration at 50 °, its mud to be injected in plaster mould half hour overfall, makes blank, repair after blank partial desiccation, then the blank biscuiting after fully parching 6 hours, after naturally cooling, out biscuit is obtained, for subsequent use;
Step 5: glaze concentration step 2 obtained out is adjusted to degree Beaume 58 °, then the biscuit that step 4 is obtained surface dirt and foreign material etc. have been cleared up, and then biscuit is dipped in glaze slip, Deng the glaze thickness of its biscuit face attachment reach 0.2mm after take out, bottom finishing base, bubble on surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer by after the biscuit airing trimming glaze layer, 1040 DEG C are warming up to gradually in oxidizing atmosphere, wherein being warming up to 300 DEG C of times is 1 hour, being warming up to 900 DEG C from 300 DEG C is 3 hours, being warming up to 1040 DEG C of times from 900 DEG C is 1 hour, directly passes into carbon monoxide unsteady state operation and becomes reducing atmosphere (reducing by force), and be slowly warming up to 1250 DEG C gradually after 1050 DEG C, time is 7 hours, and heated up rear steady fire insulation 10 minutes; Cease fire; Naturally cooling; Completing of the transparent pea green starved glaze of your porcelain.
Embodiment 2
The making method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose melilith, calcite, white feldspar, black feldspar, quartz, plant ash respectively as glaze raw material, melilith 10%, calcite 16%, white feldspar 45%, black feldspar 22%, quartz 5%, plant ash 2% by weight proportion, the raw material chosen is crushed to 40 orders respectively, for subsequent use;
Step 2: the melilith that step one is chosen,, calcite, the glaze raw material mixing glaze such as white feldspar, black feldspar and plant ash add ball mill, then add mixture part by weight be 45% water carry out wet-milling, the wet-milling time is 20 hours, glaze slip after wet-milling crosses 150 mesh sieves, take out in holding bucket with the iron that swims in bar magnet removing glaze slip, for subsequent use;
Step 3: choose kaolin as base raw material, put into ball mill after being broken into pieces by blank, adds the water of billet weight 45% and the buck agent of 0.45%, wet-milling 10 hours, pug starched 120 mesh sieves, removed foreign material and removed the iron that swims in pug slurry with bar magnet, for subsequent use;
Step 4: mud obtained for step 3 is modulated concentration at 52 °, its mud is injected 35 minutes overfalls in plaster mould, and make blank, blank is cool to be repaired to partial desiccation, and then fully parching rear biscuiting 5 hours, after naturally cooling, obtained biscuit, for subsequent use;
Step 5: glaze concentration step 2 obtained out is adjusted to degree Beaume 58 °, then the biscuit that step 4 is obtained surface dirt and foreign material etc. have been cleared up, and then biscuit is dipped in glaze slip, Deng the glaze thickness of its biscuit face attachment reach 0.25mm after take out, the bubble on finishing base lower surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer by after the biscuit airing trimming glaze layer, heat up gradually in oxidizing atmosphere, being warming up to 300 DEG C of times is 1 hour, it is 3 hours that clump 300 DEG C is warming up to 900 DEG C of times, and being warming up to 1050 DEG C of times from 900 DEG C is 1 hour, converts reducing atmosphere to after 1050 DEG C, time is 6 hours, and be slowly warming up to 1255 DEG C gradually, heated up rear insulation 10 minutes, ceases fire; Naturally cooling; Completing of the transparent pea green starved glaze of your porcelain.
Embodiment 3
The making method of the transparent pea green starved glaze of your porcelain, making step is:
Step one: choose melilith respectively, calcite, in vain feldspar, black feldspar, quartz, plant ash make glaze raw material, be melilith 8%, calcite 14%, white feldspar 50%, black feldspar 15%, quartz 10%, plant ash 3% by weight proportion, the raw material chosen is crushed to 40 orders respectively, for subsequent use;
Step 2: the glaze raw material mixing glaze such as melilith step one chosen, calcite, white feldspar, black feldspar and plant ash add ball mill, then add mixture weight be 50% water carry out wet-milling, the wet-milling time is 15 hours, glair after wet-milling crosses 150 mesh sieves, with the iron that swims in bar magnet removing glaze slip, for subsequent use;
Step 3: choose kaolin as base raw material, ball mill is put into after being broken into pieces by blank, add the water of billet weight 45% and the buck agent of 0.3%, wet-milling 10 hours, pug is by 120 mesh sieves, remove foreign material and take out with after the iron that swims in bar magnet removing mud slip, filtering moisture with filter, for subsequent use;
Step 4: the mud that step 3 is obtained is refined through pug mill, sequences the inside air; , put by walk on Blank drawing machine and make blank, blank is cool to be repaired to partial desiccation, and finishing impression is bonding etc.; Then the blank biscuiting after fully parching 6 hours, out biscuit after naturally cooling, for subsequent use;
Step 5: glaze concentration step 2 obtained out is adjusted to degree Beaume 62 °, then the biscuit that step 4 is obtained surface dirt and foreign material etc. have been cleared up, and then biscuit is dipped in glaze slip, Deng the glaze thickness of its biscuit surface attachment reach 0.2mm after take out, the bubble bottom finishing base, on surface glaze layer and uneven part.
Step 6: put into the kiln putting up rack-layer by after the biscuit airing trimming glaze layer, heat up gradually in oxidizing atmosphere, normal temperature is warming up to 900 DEG C ° indoor, and its time is 4 hours, and 900 DEG C are warming up to 1040 DEG C, time is 1 hour, convert reducing atmosphere to after 1040 DEG C, strong reductase 12 0-30 minute, and be slowly warming up to 1260 DEG C gradually, time is 7 hours, insulation 15 minutes after having heated up; Cease fire; Naturally cooling; Completing of the transparent pea green glaze of your porcelain.
Claims (1)
1. the making method of the transparent pea green starved glaze of your porcelain, is characterized in that:
Step one, choosing melilith, calcite, white feldspar, black feldspar, quartz, plant ash as glaze raw material respectively, be melilith 5%-10%, calcite 10%-16%, in vain feldspar 45%-64%, black feldspar 15%-22%, quartzy 5%-10%, plant ash 1%-3% by weight proportion; The raw material chosen is crushed to 40 orders respectively, for subsequent use;
The glaze raw material mixing such as step 2, the melilith that step one is chosen, calcite, white feldspar, black feldspar and plant ash, mixed glaze and added ball mill, then adding mixture weight is that the water of 45-58% carries out wet-milling, the wet-milling time is 12-20 hour, glaze slip after wet-milling crosses 150 mesh sieves, with the iron that swims in magnet removing glaze slip, for subsequent use;
Step 3, choose kaolin as base raw material, put into ball mill after being broken into pieces, add the water of billet weight 45-50% and the buck agent of 0.3%-0.5%, wet-milling 8-13 hour, pug starched 120 mesh sieves, removed foreign material and took out with after the iron that swims in bar magnet removing mud slip, for subsequent use;
Step 4, adjust its concentration at 48 °-52 ° in mud obtained for step 3, the mud mixed up to be injected in plaster mould overfall about more than half a hour, make blank, blank is cool to be repaired to partial desiccation, then fully parching rear biscuiting 5 hours, biscuit after naturally cooling, is taken out to obtain, for subsequent use;
Step 5, glaze concentration step 2 obtained out are adjusted to degree Beaume 58 °-62 °, then the biscuit that step 4 is obtained has been cleared up surface dirt, again biscuit is dipped in glaze slip, Deng the glaze thickness of its biscuit face attachment reach 0.2-0.3mm after take out, bottom finishing base, bubble on surface glaze layer and uneven part;
Step 6, step 5 is trimmed glaze layer biscuit airing after put into the kiln putting up rack-layer, 1040 DEG C are warming up to gradually in oxidizing atmosphere, wherein, in kiln, normal temperature is warming up to 300 DEG C, time is 1 hour, be warming up to 900 DEG C from 300 DEG C, the time is 4 hours, and 1040-1050 DEG C of steady fire reduces 30 minutes by force; Slowly be warming up to 1250-1255 DEG C gradually afterwards, the time is 6-7 hour, is incubated 10 minutes again after having heated up; Cease fire, naturally cooling, completing of the transparent pea green starved glaze of your porcelain.
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Cited By (8)
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| CN104860725A (en) * | 2015-04-24 | 2015-08-26 | 长沙市望城区盛唐工艺陶瓷有限公司 | Green glaze ceramic artware preparation method |
| CN107162564A (en) * | 2017-05-22 | 2017-09-15 | 苏州太湖窑陶瓷有限公司 | A kind of clear mud porcelain and its preparation technology |
| CN108483918A (en) * | 2018-06-19 | 2018-09-04 | 刘冬青 | Pseudo-classic glaze of your a kind of porcelain and preparation method thereof |
| CN110156437A (en) * | 2019-05-29 | 2019-08-23 | 王晟鸣 | A kind of your porcelain of lavender grey glaze and preparation method thereof |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
| CN111704360A (en) * | 2020-07-13 | 2020-09-25 | 张玉凤 | Antique Ru porcelain green glaze and manufacturing method thereof |
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| CN104860725A (en) * | 2015-04-24 | 2015-08-26 | 长沙市望城区盛唐工艺陶瓷有限公司 | Green glaze ceramic artware preparation method |
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| CN110156437A (en) * | 2019-05-29 | 2019-08-23 | 王晟鸣 | A kind of your porcelain of lavender grey glaze and preparation method thereof |
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| CN111704360A (en) * | 2020-07-13 | 2020-09-25 | 张玉凤 | Antique Ru porcelain green glaze and manufacturing method thereof |
| CN112939464A (en) * | 2021-04-29 | 2021-06-11 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN112939464B (en) * | 2021-04-29 | 2022-06-10 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN113387577A (en) * | 2021-07-19 | 2021-09-14 | 河南弘宝汝瓷坊有限公司 | Green glaze for Ru porcelain and preparation method of green glaze Ru porcelain |
| CN113387577B (en) * | 2021-07-19 | 2023-02-17 | 河南弘宝汝瓷坊有限公司 | Green glaze for Ru porcelain and preparation method of green glaze Ru porcelain |
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Effective date of registration: 20170628 Address after: Ruzhou porcelain industry in Pingdingshan city in Henan province 467500 area Patentee after: Henan Hong you Culture & Art Co., Ltd. Address before: Ruzhou City, Pingdingshan City, Henan Province, 467500 riding Ling Fan Ji village 5 groups Patentee before: Feng Yanqin |