CN104264496A - 一种服装用合成革及其生产方法 - Google Patents

一种服装用合成革及其生产方法 Download PDF

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CN104264496A
CN104264496A CN201410448326.0A CN201410448326A CN104264496A CN 104264496 A CN104264496 A CN 104264496A CN 201410448326 A CN201410448326 A CN 201410448326A CN 104264496 A CN104264496 A CN 104264496A
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许月莲
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LIUAN SANXI LEATHER PRODUCTS Co Ltd
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Abstract

本发明公开了一种服装用合成革，包括基布层、PVC发泡层和PU面层，其面层由下述重量份的原料制得：水性聚氨酯树脂80-100，椰子油脂肪酸二乙醇酰胺0.2-1，月桂醇硫酸酯钠0.2-0.5，留兰香油0.5-1.5，油酸聚乙二醇酯2-6，山梨醇0.2-1，β-环糊精3-8，花生壳粉1-3，木粉1-2，微晶纤维素1-2，改性助剂1-3，色料1-2；本发明的合成革外观、柔软度及手感良好，温和无害，且具有持久的清新香味，适用于服装面料。

Description

一种服装用合成革及其生产方法
技术领域
本发明涉及合成革加工技术领域，具体涉及一种服装用合成革及其生产方法。
背景技术
聚氨酯(PU)合成革具有耐寒、手感及外观质量好、强度高、吸湿透气性好、无聚氯乙烯（PVC）人造革冬硬夏软且粘手的现象等特点，成为替代天然皮革的最佳选择。
发明内容
本发明的目的是提供一种服装用合成革。
本发明是通过以下技术方案实现的：
一种服装用合成革，包括基布层、PVC发泡层和PU面层，其中：
PU面层由下述重量份的原料制得：
水性聚氨酯树脂80-100，椰子油脂肪酸二乙醇酰胺0.2-1，月桂醇硫酸酯钠0.2-0.5，留兰香油0.5-1.5，油酸聚乙二醇酯2-6，山梨醇0.2-1，β-环糊精3-8，花生壳粉1-3，木粉1-2，微晶纤维素1-2，改性助剂1-3，色料1-2；
PVC发泡层由下述重量份的原料制得：
PVC SG-1 30-60，PVC SG-5 20-40，乙酰柠檬酸三丁酯50-80，棕榈油3-8，亚麻籽油2-4，尿素0.2-1，琥珀酸钠0.5-1，轻质碳酸钙20-40，沸石粉10-20，木薯淀粉5-10，水镁石纤维1-2，壬基酚聚氧乙烯醚0.2-0.5，吐温80 0.1-0.3，鲸蜡硬脂醇4-8，AC发泡剂2-5，液体钡锌稳定剂1-3；
其中改性助剂由下列重量份的原料制成：
羽毛粉10-20，高岭土10-20，甘露醇1-2，柠檬酸0.2-1，氯化铵2-4，钛酸酯偶联剂0.5-1，油酸2-6；
改性助剂的制备方法是：
将羽毛粉与高岭土混合均匀，500-600℃煅烧1-2h后加入适量水和氯化铵，搅拌均匀后过滤，加入丙二醇和柠檬酸，再加适量水研磨15-30min，干燥后加入钛酸酯偶联剂，100-150℃、200-400r/min搅拌10-20min，加入油酸，同样条件下搅拌30-60min，干燥后研磨至600-800目，即得；
一种服装用合成革的生产方法，包括以下步骤：
（1）称取PU面层原料，先将留兰香油溶于少量乙醇，在50-60℃、600-800r/min条件下滴加入10-15%β-环糊***溶液搅拌30-60min，加入油酸聚乙二醇酯和山梨醇同样条件下搅拌10-15min，喷雾干燥后得活性粉体；将活性粉体与其余面层原料混合，1000-1500r/min搅拌10-20min后均匀涂覆在离型纸上，100-150℃烘干后形成面；
（2）称取PVC发泡层原料，先将轻质碳酸钙、沸石粉、木薯淀粉与棕榈油、亚麻籽油混合并200-400r/min、50-60℃搅拌30-60min，再与其余原料混合，1000-1500r/min搅拌30-60min，得PVC发泡浆料；再将配制好的PVC发泡浆料均匀涂覆在聚氨酯面层上，于160-200℃下发泡形成PVC发泡层；
（3）在发泡层上涂覆水性聚氨酯粘结浆料，与基布层粘接后130-160℃烘干；
（4）去除离型纸，得到合成革成品。
本发明的优点是：
本发明的合成革外观、柔软度及手感良好，温和无害，且含有天然香料留兰香油，具有持久的清新香味，适用于服装面料。
具体实施方式
本发明非限定实施例如下：
实施例1
一种服装用合成革，包括基布层、PU面层和PVC发泡层，其中：
PU面层由下述重量份的原料制得：
水性聚氨酯树脂90，椰子油脂肪酸二乙醇酰胺0.5，月桂醇硫酸酯钠0.4，留兰香油1，油酸聚乙二醇酯4，山梨醇0.6，β-环糊精6，花生壳粉2，木粉1.5，微晶纤维素1.5，改性助剂2，色料1.5；
PVC发泡层由下述重量份的原料制得：
PVC SG-1 40，PVC SG-5 30，乙酰柠檬酸三丁酯65，棕榈油6，亚麻籽油3，尿素0.5，琥珀酸钠0.6，轻质碳酸钙30，沸石粉15，木薯淀粉7，水镁石纤维1，壬基酚聚氧乙烯醚0.4，吐温80 0.2，鲸蜡硬脂醇6，AC发泡剂3，液体钡锌稳定剂2；
其中改性助剂由下列重量份的原料制成：
羽毛粉15，高岭土10，甘露醇2，柠檬酸0.5，氯化铵3，钛酸酯偶联剂0.8，油酸4；
改性助剂的制备方法是：
将羽毛粉与高岭土混合均匀，600℃煅烧1h后加入适量水和氯化铵，搅拌均匀后过滤，加入丙二醇和柠檬酸，再加适量水研磨15min，干燥后加入钛酸酯偶联剂，120℃、200r/min搅拌10min，加入油酸，同样条件下搅拌30min，干燥后研磨至600目，即得；
一种服装用合成革的生产方法，包括以下步骤：
（1）称取PU面层原料，先将留兰香油溶于少量乙醇，在55℃、800r/min条件下滴加入15%β-环糊***溶液搅拌45min，加入油酸聚乙二醇酯和山梨醇同样条件下搅拌10min，喷雾干燥后得活性粉体；将活性粉体与其余面层原料混合，1200r/min搅拌10min后均匀涂覆在离型纸上，120℃烘干后形成面；
（2）称取PVC发泡层原料，先将轻质碳酸钙、沸石粉、木薯淀粉与棕榈油、亚麻籽油混合并400r/min、60℃搅拌50min，再与其余原料混合，1300r/min搅拌40min，得PVC发泡浆料；再将配制好的PVC发泡浆料均匀涂覆在聚氨酯面层上，于180℃下发泡形成PVC发泡层；
（3）在发泡层上涂覆水性聚氨酯粘结浆料，与基布层粘接后150℃烘干；
（4）去除离型纸，得到合成革成品。
经产品性能测试，经向撕裂负荷为18N，纬向撕裂负荷为15N，符合实际应用的要求。

Claims (2)

1.一种服装用合成革，包括基布层、PVC发泡层和PU面层，其特征在于：
所述的PU面层由下述重量份的原料制得：
水性聚氨酯树脂80-100，椰子油脂肪酸二乙醇酰胺0.2-1，月桂醇硫酸酯钠0.2-0.5，留兰香油0.5-1.5，油酸聚乙二醇酯2-6，山梨醇0.2-1，β-环糊精3-8，花生壳粉1-3，木粉1-2，微晶纤维素1-2，改性助剂1-3，色料1-2；
所述的PVC发泡层由下述重量份的原料制得：
PVC SG-1 30-60，PVC SG-5 20-40，乙酰柠檬酸三丁酯50-80，棕榈油3-8，亚麻籽油2-4，尿素0.2-1，琥珀酸钠0.5-1，轻质碳酸钙20-40，沸石粉10-20，木薯淀粉5-10，水镁石纤维1-2，壬基酚聚氧乙烯醚0.2-0.5，吐温80 0.1-0.3，鲸蜡硬脂醇4-8，AC发泡剂2-5，液体钡锌稳定剂1-3；
所述改性助剂由下列重量份的原料制成：
羽毛粉10-20，高岭土10-20，甘露醇1-2，柠檬酸0.2-1，氯化铵2-4，钛酸酯偶联剂0.5-1，油酸2-6；
所述改性助剂的制备方法是：
将羽毛粉与高岭土混合均匀，500-600℃煅烧1-2h后加入适量水和氯化铵，搅拌均匀后过滤，加入丙二醇和柠檬酸，再加适量水研磨15-30min，干燥后加入钛酸酯偶联剂，100-150℃、200-400r/min搅拌10-20min，加入油酸，同样条件下搅拌30-60min，干燥后研磨至600-800目，即得。
2.根据权利要求1所述的一种服装用合成革的制备方法，其特征在于，包括以下步骤：
（1）称取PU面层原料，先将留兰香油溶于少量乙醇，在50-60℃、600-800r/min条件下滴加入10-15%β-环糊***溶液搅拌30-60min，加入油酸聚乙二醇酯和山梨醇同样条件下搅拌10-15min，喷雾干燥后得活性粉体；将活性粉体与其余面层原料混合，1000-1500r/min搅拌10-20min后均匀涂覆在离型纸上，100-150℃烘干后形成面层；
（2）称取PVC发泡层原料，先将轻质碳酸钙、沸石粉、木薯淀粉与棕榈油、亚麻籽油混合并200-400r/min、50-60℃搅拌30-60min，再与其余原料混合，1000-1500r/min搅拌30-60min，得PVC发泡浆料；再将配制好的PVC发泡浆料均匀涂覆在聚氨酯面层上，于160-200℃下发泡形成PVC发泡层；
（3）在发泡层上涂覆水性聚氨酯粘结浆料，与基布层粘接后130-160℃烘干；
（4）去除离型纸，得到合成革成品。
CN201410448326.0A 2014-09-04 2014-09-04 一种服装用合成革及其生产方法 Pending CN104264496A (zh)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104594061A (zh) * 2015-01-12 2015-05-06 安徽玉堂雨具有限公司 一种节能环保型pu合成革及其生产方法
CN104594063A (zh) * 2015-01-12 2015-05-06 安徽玉堂雨具有限公司 一种高性能pu沙发革及其生产方法
CN105239415A (zh) * 2015-08-26 2016-01-13 安徽冠宜箱包有限公司 一种自带清香的人造皮革箱包及其制备方法
CN105297468A (zh) * 2015-10-27 2016-02-03 芜湖市鸿坤汽车零部件有限公司 一种清香型合成革及其生产方法
CN105862446A (zh) * 2016-06-22 2016-08-17 程志刚 一种抗菌防霉pu合成革及其生产方法
CN105887504A (zh) * 2016-06-22 2016-08-24 程志刚 一种仿真pu合成革及其生产方法
CN107099125A (zh) * 2017-06-23 2017-08-29 安徽金钻智能科技有限公司 一种合成革加工用柔软增强剂及其制备方法
CN107435248A (zh) * 2016-05-27 2017-12-05 丰田纺织株式会社 合成皮革
CN109235053A (zh) * 2018-11-30 2019-01-18 重庆长安汽车股份有限公司 一种芳香人造革及其制备方法和应用
CN109577020A (zh) * 2018-12-05 2019-04-05 东台市吉中汽车内饰件有限公司 一种带香味面套的生产工艺

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CN104594061A (zh) * 2015-01-12 2015-05-06 安徽玉堂雨具有限公司 一种节能环保型pu合成革及其生产方法
CN104594063A (zh) * 2015-01-12 2015-05-06 安徽玉堂雨具有限公司 一种高性能pu沙发革及其生产方法
CN105239415A (zh) * 2015-08-26 2016-01-13 安徽冠宜箱包有限公司 一种自带清香的人造皮革箱包及其制备方法
CN105297468A (zh) * 2015-10-27 2016-02-03 芜湖市鸿坤汽车零部件有限公司 一种清香型合成革及其生产方法
CN107435248A (zh) * 2016-05-27 2017-12-05 丰田纺织株式会社 合成皮革
CN105862446A (zh) * 2016-06-22 2016-08-17 程志刚 一种抗菌防霉pu合成革及其生产方法
CN105887504A (zh) * 2016-06-22 2016-08-24 程志刚 一种仿真pu合成革及其生产方法
CN107099125A (zh) * 2017-06-23 2017-08-29 安徽金钻智能科技有限公司 一种合成革加工用柔软增强剂及其制备方法
CN107099125B (zh) * 2017-06-23 2019-04-09 安徽金钻智能科技有限公司 一种合成革加工用柔软增强剂及其制备方法
CN109235053A (zh) * 2018-11-30 2019-01-18 重庆长安汽车股份有限公司 一种芳香人造革及其制备方法和应用
CN109577020A (zh) * 2018-12-05 2019-04-05 东台市吉中汽车内饰件有限公司 一种带香味面套的生产工艺

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