CN104263037A - Water-based radon-proof interior wall paint - Google Patents
Water-based radon-proof interior wall paint Download PDFInfo
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- CN104263037A CN104263037A CN201410544851.2A CN201410544851A CN104263037A CN 104263037 A CN104263037 A CN 104263037A CN 201410544851 A CN201410544851 A CN 201410544851A CN 104263037 A CN104263037 A CN 104263037A
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Abstract
The invention discloses water-based radon-proof interior wall paint. The paint comprises raw materials in parts by weight as follows: 0.6-1 part of 5-hydroxy-2-adamantanone, 0.7-2 parts of hydroxyl silicone oil, 2-4 parts of zinc oxide, 1-2 parts of polysorbate-80, 0.7-1 part of calcium acetylacetone, 2-4 parts of ethylene glycol monoethyl ether acetate, 0.7-1 part of sodium carboxymethyl cellulose, 0.4-1 part of a cross-linking agent TAC, 3-5 parts of bamboo charcoal powder, 2-3 parts of polyisoprene, 10-14 parts of wollastonite powder, 70-100 parts of tetravinyl tetramethylcyelo tetrasiloxane, 120-160 parts of butyl methacrylate, 130-200 parts of 2-ethylhexyl acrylate, 500-600 parts of deionized water, 2-4 parts of sodium persulfate, 3-4 parts of op-10 and 4-5 parts of a binder. The paint has very good anti-radiation capacity, and a paint film is good in stability and compactness and can shield damage caused by radon in a wall to the human body lastingly.
Description
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Technical field
The present invention relates generally to paint field, particularly relates to a kind of water-based radon-proof interior wall coating.
Background technology
Be applied to body surface can be formed there is protection, the class I liquid I of solid-state film of decoration or property (as insulation, anticorrosion, mark etc.) or the general name of solid material, comprise oil (property) paint, water-miscible paint, powder coating.Paint is flowable liquid coating, comprises oil (property) paint and water-miscible paint.Paint take organic solvent as medium or high solid, solvent-free oil-base paint.Water-miscible paint is used water dissolving or the coating with water-dispersion.Coating is as one of the main material of house decoration, and the large percentage accounted in decorations, buys the whether qualified environment directly having influence on overall finishing effect and room of coating, sometimes even can produce harm greatly to the health of human body.At present along with the generation of various coating, the quality requirements of coating is also improved constantly, and improve constantly coating quality and can play very large help for building, life.
Summary of the invention
The object of the invention is just to provide a kind of water-based radon-proof interior wall coating.
The present invention is achieved by the following technical solutions:
A kind of water-based radon-proof interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
5-hydroxyl-2-diamantane ketone 0.6-1, hydroxy silicon oil 0.7-2, zinc borate 2-4, Polysorbate 80 1-2, calcium acetylacetonate 0.7-1, ethylene glycol ether acetate 2-4, Xylo-Mucine 0.7-1, linking agent TAC0.4-1, bamboo charcoal powder 3-5, polyisoprene 2-3, wollastonite powder 10-14, t etram-ethyltetravinylcyclotetrasiloxane 70-100, butyl methacrylate 120-160, Isooctyl acrylate monomer 130-200, deionized water 500-600, Sodium Persulfate 2-4, op-10 3-4, adhesive aid 4-5,
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 5-10, acrylate and vinyl acetate emulsion 20-25, aluminate coupling agent 2-3, Camphorwood micro mist 1-2, iso-borneol methacrylic ester 2-3, Potassium Persulphate 1-2, Sodium dodecylbenzene sulfonate 0.6-1, deionized water 13-20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester after stirring, insulated and stirred 3-5 minute at 50-60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 300-400 rev/min of dispersed with stirring 15-20 minute, obtains described adhesive aid.
A preparation method for water-based radon-proof interior wall coating, is characterized in that comprising the following steps:
(1) get the 50-60% mixing of the 50-60% of above-mentioned butyl methacrylate weight, Isooctyl acrylate monomer weight, stir, obtain monomer a;
(2) remaining butyl methacrylate, Isooctyl acrylate monomer are mixed with t etram-ethyltetravinylcyclotetrasiloxane, insulated and stirred 10-15 minute at 60-70 DEG C, is cooled to normal temperature, obtains monomer b;
(3) get Sodium Persulfate, add the 10-20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with the 10-20% of residue deionized water weight, add Xylo-Mucine, at 50-60 DEG C, be uniformly mixed 10-15 minute, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 60-70 DEG C, insulated and stirred 20-30 minute, drips above-mentioned monomer a, drips off, be incubated 20-30 minute at the temperature disclosed above after dropwising, obtain seed emulsion in 2-4 hour;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 100-120 minute, after dropwising, at 70-80 DEG C, is incubated 1-2 hour, cooling, filters discharging with 200-250 eye mesh screen;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 800-1200 rev/min of dispersed with stirring 20-30 minute, obtains described water-based radon-proof interior wall coating.
Advantage of the present invention is:
Coating of the present invention has good radioprotective and penetrates ability, and paint film stability is good, and compactness is good, can in long-acting shielding body of wall radon gas to the harm of human body.The methyl methacrylate that adhesive aid of the present invention adds can form colloidal state in water, mixed and modified with iso-borneol methacrylic ester, Potassium Persulphate, acrylate and vinyl acetate emulsion etc., has very strong bond effect, can improve film coated surface cohesiveness and stability.
Embodiment
Embodiment 1
A kind of water-based radon-proof interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
5-hydroxyl-2-diamantane ketone 0.6, hydroxy silicon oil 0.7, zinc borate 2, Polysorbate 80 1, calcium acetylacetonate 0.7, ethylene glycol ether acetate 2, Xylo-Mucine 0.7, linking agent TAC0.4, bamboo charcoal powder 3, polyisoprene 2, wollastonite powder 14, t etram-ethyltetravinylcyclotetrasiloxane 100, butyl methacrylate 160, Isooctyl acrylate monomer 200, deionized water 600, Sodium Persulfate 4, op-10 4, adhesive aid 5;
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 10, acrylate and vinyl acetate emulsion 25, aluminate coupling agent 3, Camphorwood micro mist 1, iso-borneol methacrylic ester 3, Potassium Persulphate 1, Sodium dodecylbenzene sulfonate 0.6, deionized water 20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, after stirring, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester, insulated and stirred 3 minutes at 60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 400 revs/min of dispersed with stirring 20 minutes, obtain described adhesive aid.
A preparation method for water-based radon-proof interior wall coating, is characterized in that comprising the following steps:
(1) get 60% of above-mentioned butyl methacrylate weight, 60% mixing of Isooctyl acrylate monomer weight, stir, obtain monomer a;
(2) remaining butyl methacrylate, Isooctyl acrylate monomer are mixed with t etram-ethyltetravinylcyclotetrasiloxane, insulated and stirred 10-15 minute at 60-70 DEG C, is cooled to normal temperature, obtains monomer b;
(3) get Sodium Persulfate, add 20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with 20% of residue deionized water weight, add Xylo-Mucine, at 60 DEG C, be uniformly mixed 15 minutes, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 70 DEG C, and insulated and stirred 30 minutes drips above-mentioned monomer a, dripped off in 4 hours, is incubated 30 minutes at the temperature disclosed above, obtains seed emulsion after dropwising;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 120 minutes, after dropwising, at 80 DEG C, be incubated 2 hours, and cooling filters discharging with 250 eye mesh screens;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 1200 revs/min of dispersed with stirring 30 minutes, obtain described water-based radon-proof interior wall coating.
Performance test:
Unit elongation: >=300%;
Watertightness: 0.3MPa (one hour waterproof).
Claims (2)
1. a water-based radon-proof interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
5-hydroxyl-2-diamantane ketone 0.6-1, hydroxy silicon oil 0.7-2, zinc borate 2-4, Polysorbate 80 1-2, calcium acetylacetonate 0.7-1, ethylene glycol ether acetate 2-4, Xylo-Mucine 0.7-1, linking agent TAC0.4-1, bamboo charcoal powder 3-5, polyisoprene 2-3, wollastonite powder 10-14, t etram-ethyltetravinylcyclotetrasiloxane 70-100, butyl methacrylate 120-160, Isooctyl acrylate monomer 130-200, deionized water 500-600, Sodium Persulfate 2-4, op-10 3-4, adhesive aid 4-5,
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 5-10, acrylate and vinyl acetate emulsion 20-25, aluminate coupling agent 2-3, Camphorwood micro mist 1-2, iso-borneol methacrylic ester 2-3, Potassium Persulphate 1-2, Sodium dodecylbenzene sulfonate 0.6-1, deionized water 13-20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester after stirring, insulated and stirred 3-5 minute at 50-60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 300-400 rev/min of dispersed with stirring 15-20 minute, obtains described adhesive aid.
2. a preparation method for water-based radon-proof interior wall coating as claimed in claim 1, is characterized in that comprising the following steps:
(1) get the 50-60% mixing of the 50-60% of above-mentioned butyl methacrylate weight, Isooctyl acrylate monomer weight, stir, obtain monomer a;
(2) remaining butyl methacrylate, Isooctyl acrylate monomer are mixed with t etram-ethyltetravinylcyclotetrasiloxane, insulated and stirred 10-15 minute at 60-70 DEG C, is cooled to normal temperature, obtains monomer b;
(3) get Sodium Persulfate, add the 10-20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with the 10-20% of residue deionized water weight, add Xylo-Mucine, at 50-60 DEG C, be uniformly mixed 10-15 minute, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 60-70 DEG C, insulated and stirred 20-30 minute, drips above-mentioned monomer a, drips off, be incubated 20-30 minute at the temperature disclosed above after dropwising, obtain seed emulsion in 2-4 hour;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 100-120 minute, after dropwising, at 70-80 DEG C, is incubated 1-2 hour, cooling, filters discharging with 200-250 eye mesh screen;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 800-1200 rev/min of dispersed with stirring 20-30 minute, obtains described water-based radon-proof interior wall coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410544851.2A CN104263037A (en) | 2014-10-15 | 2014-10-15 | Water-based radon-proof interior wall paint |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410544851.2A CN104263037A (en) | 2014-10-15 | 2014-10-15 | Water-based radon-proof interior wall paint |
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| CN104263037A true CN104263037A (en) | 2015-01-07 |
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| CN201410544851.2A Pending CN104263037A (en) | 2014-10-15 | 2014-10-15 | Water-based radon-proof interior wall paint |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105885618A (en) * | 2015-11-26 | 2016-08-24 | 无锡英普林纳米科技有限公司 | Anti-radon gas coating material |
Citations (5)
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| CN101096400A (en) * | 2006-06-30 | 2008-01-02 | 天津市振东涂料有限公司 | Synthesizing method for confecting inner-outer wall coating water-proof stain-resistant latex |
| CN101649153A (en) * | 2009-09-07 | 2010-02-17 | 大连工业大学 | Organic silicon modified acrylic ester aqueous wood lacquer latex and synthesizing method thereof |
| CN102643385A (en) * | 2012-05-10 | 2012-08-22 | 西北师范大学 | Organic silicon-acrylic ester copolymer emulsion and preparation and application thereof |
| CN103351671A (en) * | 2013-06-20 | 2013-10-16 | 滁州麦斯特新型建材有限公司 | High-efficiency antifouling antibacterial exterior wall coating and preparation method thereof |
| CN103725141A (en) * | 2013-12-17 | 2014-04-16 | 江苏苏博特新材料股份有限公司 | Water-based emulsion for protecting external wall of building and preparation method for water-based emulsion |
-
2014
- 2014-10-15 CN CN201410544851.2A patent/CN104263037A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101096400A (en) * | 2006-06-30 | 2008-01-02 | 天津市振东涂料有限公司 | Synthesizing method for confecting inner-outer wall coating water-proof stain-resistant latex |
| CN101649153A (en) * | 2009-09-07 | 2010-02-17 | 大连工业大学 | Organic silicon modified acrylic ester aqueous wood lacquer latex and synthesizing method thereof |
| CN102643385A (en) * | 2012-05-10 | 2012-08-22 | 西北师范大学 | Organic silicon-acrylic ester copolymer emulsion and preparation and application thereof |
| CN103351671A (en) * | 2013-06-20 | 2013-10-16 | 滁州麦斯特新型建材有限公司 | High-efficiency antifouling antibacterial exterior wall coating and preparation method thereof |
| CN103725141A (en) * | 2013-12-17 | 2014-04-16 | 江苏苏博特新材料股份有限公司 | Water-based emulsion for protecting external wall of building and preparation method for water-based emulsion |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105885618A (en) * | 2015-11-26 | 2016-08-24 | 无锡英普林纳米科技有限公司 | Anti-radon gas coating material |
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Application publication date: 20150107 |
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