CN104231695A - Green antibacterial coating for interior wall - Google Patents

Green antibacterial coating for interior wall Download PDF

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Publication number
CN104231695A
CN104231695A CN201410544844.2A CN201410544844A CN104231695A CN 104231695 A CN104231695 A CN 104231695A CN 201410544844 A CN201410544844 A CN 201410544844A CN 104231695 A CN104231695 A CN 104231695A
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China
Prior art keywords
parts
minute
coating
mentioned
interior wall
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Pending
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CN201410544844.2A
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Chinese (zh)
Inventor
王贵东
宋睿
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Hefei Ring Macromolecular Material Factory
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Hefei Ring Macromolecular Material Factory
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Application filed by Hefei Ring Macromolecular Material Factory filed Critical Hefei Ring Macromolecular Material Factory
Priority to CN201410544844.2A priority Critical patent/CN104231695A/en
Publication of CN104231695A publication Critical patent/CN104231695A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a green antibacterial coating for interior wall, and the green antibacterial coating for interior wall is composed of the raw material in parts by weight: 2-3 parts of aloe vera gel, 1-2 parts of aloe extract liquid, 1-2 parts of ferrous sulfate, 2-3 parts of calcium aluminate, 0.6-1 parts of dimethylimidazole, 2-4 parts of polytetrafluoroethylene wax, 1-3 parts of propylene glycol monomethyl ether acetate, 0.1-0.4 parts of ascorbic acid, 1-2 parts of sodium sulphide, 10-12 parts of potassium feldspar powder, 2-4 parts of aluminium nitride, 70-100 parts of tetramethyl vinyl tetrasiloxane, 120-160 parts of butyl methacrylate, 140-200 parts of crylic acid ester, 2-3 parts of mannitol, 500-600 parts of deionized water, 2-4 parts of potassium persulfate, 3-4 parts of op-10 and 4-5 parts of bonding agent; the coating has good antibacterial effect for the aloe vera gel and aloe extract liquid, the consistency of the materials can be effectively improved, the bonding strength of the coating is improved, the adhesive force of the coating to the base material is enhanced, the coating is safe and environment friendly especially suitable for interior wall.

Description

A kind of antibacterial green interior wall coating
?
Technical field
The present invention relates generally to paint field, particularly relates to a kind of antibacterial green interior wall coating.
Background technology
Be applied to body surface can be formed there is protection, the class I liquid I of solid-state film of decoration or property (as insulation, anticorrosion, mark etc.) or the general name of solid material, comprise oil (property) paint, water-miscible paint, powder coating.Paint is flowable liquid coating, comprises oil (property) paint and water-miscible paint.Paint take organic solvent as medium or high solid, solvent-free oil-base paint.Water-miscible paint is used water dissolving or the coating with water-dispersion.Coating is as one of the main material of house decoration, and the large percentage accounted in decorations, buys the whether qualified environment directly having influence on overall finishing effect and room of coating, sometimes even can produce harm greatly to the health of human body.At present along with the generation of various coating, the quality requirements of coating is also improved constantly, and improve constantly coating quality and can play very large help for building, life.
Summary of the invention
The object of the invention is just to provide a kind of antibacterial green interior wall coating.
The present invention is achieved by the following technical solutions:
A kind of antibacterial green interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
Reed fragrant plant glue 2-3, extract solution from aloe 1-2, ferrous sulfate 1-2, calcium aluminate 2-3, methylimidazole 0.6-1, tetrafluoroethylene wax 2-4,1-Methoxy-2-propyl acetate 1-3, xitix 0.1-0.4, sodium sulphite 1-2, feldspar in powder 10-12, aluminium nitride 2-4, t etram-ethyltetravinylcyclotetrasiloxane 70-100, butyl methacrylate 120-160, Ethyl acrylate 140-200, N.F,USP MANNITOL 2-3, deionized water 500-600, Potassium Persulphate 2-4, op-10 3-4, adhesive aid 4-5;
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 5-10, acrylate and vinyl acetate emulsion 20-25, aluminate coupling agent 2-3, Camphorwood micro mist 1-2, iso-borneol methacrylic ester 2-3, Potassium Persulphate 1-2, Sodium dodecylbenzene sulfonate 0.6-1, deionized water 13-20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester after stirring, insulated and stirred 3-5 minute at 50-60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 300-400 rev/min of dispersed with stirring 15-20 minute, obtains described adhesive aid.
2, a preparation method for antibacterial green interior wall coating as claimed in claim 1, is characterized in that comprising the following steps:
(1) get the 50-60% mixing of the 50-60% of above-mentioned butyl methacrylate weight, Ethyl acrylate weight, add N.F,USP MANNITOL after stirring, insulated and stirred 3-5 minute at 50-60 DEG C, is cooled to normal temperature, obtains monomer a;
(2) remaining butyl methacrylate, Ethyl acrylate are mixed with t etram-ethyltetravinylcyclotetrasiloxane, insulated and stirred 10-15 minute at 60-70 DEG C, is cooled to normal temperature, obtains monomer b;
(3) get Potassium Persulphate, add the 10-20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with the 10-20% of residue deionized water weight, add reed fragrant plant glue, extract solution from aloe, at 50-60 DEG C, be uniformly mixed 10-15 minute, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 60-70 DEG C, insulated and stirred 20-30 minute, drips above-mentioned monomer a, drips off, be incubated 20-30 minute at the temperature disclosed above after dropwising, obtain seed emulsion in 2-4 hour;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 100-120 minute, after dropwising, at 70-80 DEG C, is incubated 1-2 hour, cooling, filters discharging with 200-250 eye mesh screen;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 800-1200 rev/min of dispersed with stirring 20-30 minute, obtains described antibacterial green interior wall coating.
Advantage of the present invention is:
Reed fragrant plant glue, extract solution from aloe etc. that coating of the present invention adds have good antibacterial effect, and effectively can improve the consistency of each storeroom, improve the cohesive strength of coating, strengthen the sticking power to base material, coating safety and environmental protection of the present invention, is particularly suitable for making interior wall coating.The methyl methacrylate that adhesive aid of the present invention adds can form colloidal state in water, mixed and modified with iso-borneol methacrylic ester, Potassium Persulphate, acrylate and vinyl acetate emulsion etc., has very strong bond effect, can improve film coated surface cohesiveness and stability.
Embodiment
Embodiment 1
A kind of antibacterial green interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
Reed fragrant plant glue 2, extract solution from aloe 1, ferrous sulfate 2, calcium aluminate 2, methylimidazole 0.6, tetrafluoroethylene wax 2,1-Methoxy-2-propyl acetate 1, xitix 0.4, sodium sulphite 2, feldspar in powder 12, aluminium nitride 2, t etram-ethyltetravinylcyclotetrasiloxane 100, butyl methacrylate 160, Ethyl acrylate 200, N.F,USP MANNITOL 2, deionized water 600, Potassium Persulphate 2, op-10 4, adhesive aid 5;
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 10, acrylate and vinyl acetate emulsion 25, aluminate coupling agent 3, Camphorwood micro mist 2, iso-borneol methacrylic ester 3, Potassium Persulphate 2, Sodium dodecylbenzene sulfonate 0.6, deionized water 20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, after stirring, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester, insulated and stirred 5 minutes at 60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 400 revs/min of dispersed with stirring 20 minutes, obtain described adhesive aid.
A preparation method for antibacterial green interior wall coating, is characterized in that comprising the following steps:
(1) get 50% of above-mentioned butyl methacrylate weight, 60% mixing of Ethyl acrylate weight, add N.F,USP MANNITOL after stirring, at 60 DEG C, insulated and stirred 5 minutes, is cooled to normal temperature, obtains monomer a;
(2) remaining butyl methacrylate, Ethyl acrylate are mixed with t etram-ethyltetravinylcyclotetrasiloxane, at 70 DEG C, insulated and stirred 15 minutes, is cooled to normal temperature, obtains monomer b;
(3) get Potassium Persulphate, add 20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with 20% of residue deionized water weight, add reed fragrant plant glue, extract solution from aloe, at 60 DEG C, be uniformly mixed 15 minutes, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 70 DEG C, and insulated and stirred 30 minutes drips above-mentioned monomer a, dripped off in 4 hours, is incubated 30 minutes at the temperature disclosed above, obtains seed emulsion after dropwising;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 120 minutes, after dropwising, at 80 DEG C, be incubated 1-2 hour, cooling, filters discharging with 250 eye mesh screens;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 1200 revs/min of dispersed with stirring 30 minutes, obtain described antibacterial green interior wall coating.
Performance test:
Unit elongation: >=300%;
Watertightness: 0.3MPa (one hour waterproof).

Claims (2)

1. an antibacterial green interior wall coating, is characterized in that what it was made up of the raw material of following weight parts:
Reed fragrant plant glue 2-3, extract solution from aloe 1-2, ferrous sulfate 1-2, calcium aluminate 2-3, methylimidazole 0.6-1, tetrafluoroethylene wax 2-4,1-Methoxy-2-propyl acetate 1-3, xitix 0.1-0.4, sodium sulphite 1-2, feldspar in powder 10-12, aluminium nitride 2-4, t etram-ethyltetravinylcyclotetrasiloxane 70-100, butyl methacrylate 120-160, Ethyl acrylate 140-200, N.F,USP MANNITOL 2-3, deionized water 500-600, Potassium Persulphate 2-4, op-10 3-4, adhesive aid 4-5;
Described adhesive aid is made up of each raw material of following weight parts:
Methyl methacrylate 5-10, acrylate and vinyl acetate emulsion 20-25, aluminate coupling agent 2-3, Camphorwood micro mist 1-2, iso-borneol methacrylic ester 2-3, Potassium Persulphate 1-2, Sodium dodecylbenzene sulfonate 0.6-1, deionized water 13-20;
Above-mentioned methyl methacrylate is mixed with aluminate coupling agent, adds Sodium dodecylbenzene sulfonate, iso-borneol methacrylic ester after stirring, insulated and stirred 3-5 minute at 50-60 DEG C;
Camphorwood micro mist is joined in deionized water, after stirring, adds Potassium Persulphate, stir;
By each raw material mixing after above-mentioned process, join in acrylate and vinyl acetate emulsion, 300-400 rev/min of dispersed with stirring 15-20 minute, obtains described adhesive aid.
2. a preparation method for antibacterial green interior wall coating as claimed in claim 1, is characterized in that comprising the following steps:
(1) get the 50-60% mixing of the 50-60% of above-mentioned butyl methacrylate weight, Ethyl acrylate weight, add N.F,USP MANNITOL after stirring, insulated and stirred 3-5 minute at 50-60 DEG C, is cooled to normal temperature, obtains monomer a;
(2) remaining butyl methacrylate, Ethyl acrylate are mixed with t etram-ethyltetravinylcyclotetrasiloxane, insulated and stirred 10-15 minute at 60-70 DEG C, is cooled to normal temperature, obtains monomer b;
(3) get Potassium Persulphate, add the 10-20% of above-mentioned deionized water weight, stir, obtain initiator solution;
(4) get op-10 to mix with the 10-20% of residue deionized water weight, add reed fragrant plant glue, extract solution from aloe, at 50-60 DEG C, be uniformly mixed 10-15 minute, obtain emulsion;
(5) in above-mentioned emulsion, add initiator solution, being increased to temperature is 60-70 DEG C, insulated and stirred 20-30 minute, drips above-mentioned monomer a, drips off, be incubated 20-30 minute at the temperature disclosed above after dropwising, obtain seed emulsion in 2-4 hour;
(6) in above-mentioned seed emulsion, drip monomer b, time for adding is 100-120 minute, after dropwising, at 70-80 DEG C, is incubated 1-2 hour, cooling, filters discharging with 200-250 eye mesh screen;
(7) material above-mentioned steps (6) obtained mixes with each raw material of residue, and 800-1200 rev/min of dispersed with stirring 20-30 minute, obtains described antibacterial green interior wall coating.
CN201410544844.2A 2014-10-15 2014-10-15 Green antibacterial coating for interior wall Pending CN104231695A (en)

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CN201410544844.2A CN104231695A (en) 2014-10-15 2014-10-15 Green antibacterial coating for interior wall

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Application Number Priority Date Filing Date Title
CN201410544844.2A CN104231695A (en) 2014-10-15 2014-10-15 Green antibacterial coating for interior wall

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105111893A (en) * 2015-08-14 2015-12-02 安徽艳阳电气集团有限公司 Heat-dissipating and insulating coating material for led (light emitting diode) and preparation method therefor
CN106084949A (en) * 2016-06-17 2016-11-09 枞阳县新天地高新材料有限公司 A kind of environmental protection antibiotic paint
CN107760126A (en) * 2017-10-24 2018-03-06 沈阳顺风新材料有限公司 A kind of environment-friendly antibacterial emulsion paint and preparation method thereof
CN109054555A (en) * 2018-07-11 2018-12-21 合肥广民建材有限公司 A kind of inner wall heat-preservation coating and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101096400A (en) * 2006-06-30 2008-01-02 天津市振东涂料有限公司 Synthesizing method for confecting inner-outer wall coating water-proof stain-resistant latex
CN101649153A (en) * 2009-09-07 2010-02-17 大连工业大学 Organic silicon modified acrylic ester aqueous wood lacquer latex and synthesizing method thereof
CN102643385A (en) * 2012-05-10 2012-08-22 西北师范大学 Organic silicon-acrylic ester copolymer emulsion and preparation and application thereof
CN103351671A (en) * 2013-06-20 2013-10-16 滁州麦斯特新型建材有限公司 High-efficiency antifouling antibacterial exterior wall coating and preparation method thereof
CN103725141A (en) * 2013-12-17 2014-04-16 江苏苏博特新材料股份有限公司 Water-based emulsion for protecting external wall of building and preparation method for water-based emulsion

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101096400A (en) * 2006-06-30 2008-01-02 天津市振东涂料有限公司 Synthesizing method for confecting inner-outer wall coating water-proof stain-resistant latex
CN101649153A (en) * 2009-09-07 2010-02-17 大连工业大学 Organic silicon modified acrylic ester aqueous wood lacquer latex and synthesizing method thereof
CN102643385A (en) * 2012-05-10 2012-08-22 西北师范大学 Organic silicon-acrylic ester copolymer emulsion and preparation and application thereof
CN103351671A (en) * 2013-06-20 2013-10-16 滁州麦斯特新型建材有限公司 High-efficiency antifouling antibacterial exterior wall coating and preparation method thereof
CN103725141A (en) * 2013-12-17 2014-04-16 江苏苏博特新材料股份有限公司 Water-based emulsion for protecting external wall of building and preparation method for water-based emulsion

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105111893A (en) * 2015-08-14 2015-12-02 安徽艳阳电气集团有限公司 Heat-dissipating and insulating coating material for led (light emitting diode) and preparation method therefor
CN106084949A (en) * 2016-06-17 2016-11-09 枞阳县新天地高新材料有限公司 A kind of environmental protection antibiotic paint
CN107760126A (en) * 2017-10-24 2018-03-06 沈阳顺风新材料有限公司 A kind of environment-friendly antibacterial emulsion paint and preparation method thereof
CN109054555A (en) * 2018-07-11 2018-12-21 合肥广民建材有限公司 A kind of inner wall heat-preservation coating and preparation method thereof

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Application publication date: 20141224

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