CN104073040A - UV-cured white curtaining paint and preparation method thereof - Google Patents
UV-cured white curtaining paint and preparation method thereof Download PDFInfo
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- CN104073040A CN104073040A CN201410334383.6A CN201410334383A CN104073040A CN 104073040 A CN104073040 A CN 104073040A CN 201410334383 A CN201410334383 A CN 201410334383A CN 104073040 A CN104073040 A CN 104073040A
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Abstract
The invention discloses a UV-cured white curtaining paint and a preparation method thereof. The UV-cured white curtaining paint comprises the following raw materials by mass percentage: 30 to 50 percent of a UV cured oligomer, 20 to 40 percent of acrylate monomer, 4 to 8 percent of a photoinitiator, 0 to 10 percent of matting agent, 1 to 2 percent of additives and 5 to 15 percent of titanium dioxide, wherein the UV cured oligomer is one or mixture of several oligomers of aliphatic urethane acrylate, amino polyester acrylate and polyester acrylate; the photoinitiator is 1- hydroxy-cyclohexyl-phenyl-ketone. The method comprises the following steps: mixing of the oligomer and part of the acrylate monomer for resolving, stirring, adding of the additives, stirring, adding of the matting agent and the titanium dioxide, high-speed stirring, adding of the rest monomer after a dispersion fineness is reached, low-speed stirring for 10 to 20 minutes, vacuumizing for 30 min at 45 DEG C, and filtering to obtain the UV-cured white curtaining paint. The UV-cured white curtaining paint is high in adhesive attraction, excellent in hiding power, good in deep curing, and high in fullness, thereby being suitable for curtaining construction.
Description
Technical field
The invention belongs to UV (ultraviolet light polymerization) coating preparation field, the present invention be more particularly directed to the preparation method of coloured (white) ultraviolet-curing paint of a kind of showering painting form of construction work.
Background technology
Ultraviolet-curing paint is that colored paint is to grow up on the basis of ultraviolet light polymerization, solidify due to UV-light deep layer is a difficult problem of puzzlement industry always, current ultraviolet cured colored paint is all to rest in the roller coating of low glue spread substantially, although increased opacifying power because strengthen glue spread, can not deep layer solidify, do not reach such effect.The colored paint particularly with the showering of high fullness ratio is not easy to reach especially, and developing showering Color paint is a project that has very much technology content and prospect.In current coloured application, larger to white demand, the showering that particularly application such as kitchen guarding, wardrobe, office furniture has a high fullness ratio has very large market outlook.Exception is at present in white application, and the obstacle of the PU coating maximum of consumption maximum is exactly easy xanthochromia, so develop the UV of resistance to xanthochromia and solidify showering whitewash and both solved fullness ratio and the yellowing resistance of whitewash.Be a coating variety that has very large purposes, particularly in board-like white application, there is the unrivaled advantage of other coating, the curing energy-saving and environmental protection of UV in addition, efficient, white showering UV coating has wide market.
Summary of the invention
In order to solve the application of showering of the curing whitewash of existing ultraviolet light polymerization, mainly need to solve the application mode that is applicable to showering, solidify white showering coating so developed UV.
Technical scheme of the present invention is: a kind of UV solidifies white showering coating, and this white showering coating raw material by mass percentage, consists of: UV solidifies oligopolymer 30-50%; Acrylate monomer 20-40%; Light trigger 4-8%; Dumb light powder 0-10%; Auxiliary agent 1-2%; Titanium dioxide: 5-15%; It is the mixture of one or more oligopolymer in aliphatic urethane acrylate, Amino Polyester acrylate, polyester acrylate that UV solidifies oligopolymer; Described light trigger is 1-hydroxy-cyclohexyl phenyl ketone.
What described UV solidified oligopolymer is that described aliphatic urethane acrylate, polyester acrylate is the oligopolymer of 2 functional groups, and Amino Polyester acrylate is 3 functional groups.
Described acrylate monomer is one or more in hydroxyethyl methylacrylate, pentaerythritol triacrylate, Glycerin triacrylate, ethoxylation Glycerin triacrylate, ethoxylated neopentylglycol diacrylate, 1,6 hexanediyl ester, tripropylene glycol diacrylate.
Described dumb light powder is the silicon-dioxide flatting silica of vapor phase process or gel method.
Described auxiliary agent is any one or several in defoamer, dispersion agent, anti-settling agent, flow agent.
Described titanium dioxide is rutile titanium dioxide.
The method that the described UV of preparation solidifies white showering coating, UV is solidified to oligopolymer and the stirring of a part of acrylate monomer mixed dissolution, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual acrylic acid ester monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
Beneficial effect:
UV prepared by the present invention solidifies the application of white showering coating as an innovation of the inside, ultraviolet-curing paint field application, it is in the application that utilizes ultraviolet-curing paint in the application of furniture white, substitutes more environmental protection of conventional P U coating, more efficient, energy-conservation.Fullness ratio, the yellowing resistance of whitewash are greatly improved.Product sticking power of the present invention is good, opacifying power excellence, and deep layer is cured, and fullness ratio is good, is applicable to showering construction.UV of the present invention solidifies white showering coating and is adapted at plate fitment and floor application, particularly needs the resistance to xanthochromia white furniture application of high fullness ratio at the desk of some good decorative property, cabinet, wardrobe etc.
Embodiment
Preparation used in the present invention, as long as qualified industrial goods are not limited to producer, is all commercially available conventional products.
Below in conjunction with embodiment, the present invention is further illustrated.
UV solidifies oligopolymer 30-50%; Acrylate monomer 20-40%; Light trigger 4-8%; Dumb light powder 0-10%; Auxiliary agent 1-2%; Titanium dioxide: 5-15%.Preparation method of the present invention: oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
Described UV oligopolymer is the mixture of one or more oligopolymer in aliphatic urethane acrylate, amino acrylates, polyester acrylate.
Described acrylate monomer is for acrylate monomer is for containing one or more in HEMA (hydroxyethyl methylacrylate) and PETA (pentaerythritol triacrylate), TMPTA (Glycerin triacrylate), EO-TMPTA (ethoxylation Glycerin triacrylate), PO-NPGDA (ethoxylated neopentylglycol diacrylate), HDDA (1,6 hexanediyl ester), TPGDA (tripropylene glycol diacrylate).
It is the one 184 (1-hydroxy-cyclohexyl phenyl ketone) that must contain in acylphosphine oxide and alpha-hydroxyalkyl benzophenone class that described UV solidifies white showering coating initiator.
It is the silicon-dioxide flatting silica of vapor phase process or gel method that described UV solidifies white showering coating dumb light powder.
Described UV solidifies white showering coatings additive(s) and is divided into defoamer, dispersion agent, anti-settling agent, flow agent.Wherein defoamer is not containing organosilicon polymer solution, polyacrylic acid superpolymer or their mixture; Dispersion agent is high molecular weight block copolymer solution, modified acroleic acid block copolymer solution or their mixture; Anti-settling agent is polycarboxylic acid salt, modified urea solution or their mixture of aerosil, polyamine acid amides; Flow agent is acrylic ester compound or its solution of non-silicon class.
Described UV solidifies white showering coating, it is characterized in that type titanium dioxide is the good rutile titanium dioxide of weathering resistance opacifying power
Described UV solidifies white showering coating, its preparation technology is: oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
Embodiment 1
UV solidifies white showering formulation for coating material and comprises shown in following mass percent (in table one):
Wherein oligopolymer is mainly the 61B-85 that aliphatic urethane acrylate is Changxing company, amino acrylates; Monomer is TMPTA (Glycerin triacrylate) and the HDDA (1,6 hexanediyl ester) of HEMA (hydroxyethyl methylacrylate), acrylate; Light trigger is TPO (2,4,6-trimethylbenzoyl-diphenyl phosphine oxide), 184 (1-hydroxy-cyclohexyl phenyl ketone); Sub-powder is Grace 2105; Auxiliary agent is containing dispersant B YK164 and defoamer BYK055 and anti-settling agent BYK410, flow agent BYK358; Titanium dioxide be Du Pont's titanium dioxide r902+.
Table one UV solidifies the mass percent of white showering coating composition
By above-mentioned component, oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
This priming paint index of correlation: viscosity 300-450mpa.s/25 DEG C; Fineness≤25um; Curing speed is greater than 400mj/cm
2.; Showering 100g/m on sheet glass
2, 400mj/cm
2.after solidifying, gloss is 75-80 ° (60 record).Glue spread is that 100g/m2 reaches black and white lattice opacifying power, solidifies 20 △ E xanthochromia indexs be less than 1.0 at 800mj/cm2, illustrates that yellowing resistance is good..
Embodiment 2
UV solidifies white showering formulation for coating material and comprises shown in following mass percent (in table two):
Wherein oligopolymer is mainly the 61B-85 that aliphatic urethane acrylate is Changxing company, amino acrylates; Monomer is TMPTA (Glycerin triacrylate) and the HDDA (1,6 hexanediyl ester) of HEMA (hydroxyethyl methylacrylate), acrylate; Light trigger is 819 (two (2,4, the 6-trimethylbenzoyl) phosphine oxides of phenyl), 184 (1-hydroxy-cyclohexyl phenyl ketones); Auxiliary agent is containing dispersant B YK164 and defoamer BYK055 and anti-settling agent aerosil A200, flow agent BYK358; Titanium dioxide be Du Pont's titanium dioxide r902+.
Table two UV solidifies the mass percent of white showering coating composition
By above-mentioned component, oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
This priming paint index of correlation: viscosity 300-450mpa.s/25 DEG C; Fineness≤25um; Curing speed is greater than 400mj/cm
2.; Showering 100g/m on sheet glass
2, 400mj/cm
2.after solidifying, gloss is 95-100 ° (60 record).Glue spread is that 100g/m2 reaches black and white lattice opacifying power, solidifies 20 △ E xanthochromia indexs be less than 1.0 at 800mj/cm2, illustrates that yellowing resistance is good.
Embodiment 3
UV solidifies white showering formulation for coating material and comprises shown in following mass percent (in table three):
Wherein oligopolymer is mainly the 61B-85 that aliphatic urethane acrylate is Changxing company, and polyester acrylate is the 6333-100 of Changxing company; Monomer is TMPTA (Glycerin triacrylate) and TPGDA (tripropylene glycol diacrylate) and the HEMA (hydroxyethyl methylacrylate) of acrylate; Light trigger is that light trigger is 819 (two (2,4, the 6-trimethylbenzoyl) phosphine oxides of phenyl), 184 (1-hydroxy-cyclohexyl phenyl ketones); Sub-powder is Grace 2105; Auxiliary agent is containing dispersant B YK163 and defoamer BYK055 and anti-settling agent BYK410; Titanium dioxide be Du Pont's titanium dioxide r902+.
Table three UV solidifies the mass percent of white showering coating composition
By above-mentioned component, oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
This priming paint index of correlation: viscosity 300-450mpa.s/25 DEG C; Fineness≤25um; Curing speed is greater than 400mj/cm
2.; Showering 100g/m on sheet glass
2, 400mj/cm
2.after solidifying, gloss is 35-45 ° (60 record).Glue spread is that 100g/m2 reaches black and white lattice opacifying power, solidifies 20 △ E xanthochromia indexs be less than 1.0 at 800mj/cm2, illustrates that yellowing resistance is good.
Embodiment 4
UV solidifies white showering formulation for coating material and comprises shown in following mass percent (in table four):
Wherein oligopolymer is mainly the 61B-85 that aliphatic urethane acrylate is Changxing company, amino acrylates; ; Monomer is EO-TMPTA (ethoxylation Glycerin triacrylate) and TPGDA (tripropylene glycol diacrylate) and the HEMA (hydroxyethyl methylacrylate) of acrylate; Light trigger is that light trigger is 819 (two (2,4, the 6-trimethylbenzoyl) phosphine oxides of phenyl), 184 (1-hydroxy-cyclohexyl phenyl ketones); Sub-powder is Grace 2105; Auxiliary agent is containing dispersant B YK163 and defoamer BYK055 and anti-settling agent BYK410; Titanium dioxide be Du Pont's titanium dioxide r902+.
Table four UV solidifies the mass percent of white showering coating composition
By above-mentioned component, oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
This priming paint index of correlation: viscosity 300-450mpa.s/25 DEG C; Fineness≤25um; Curing speed is greater than 400mj/cm
2.; Showering 100g/m on sheet glass
2, 400mj/cm
2.after solidifying, gloss is that 95-100 ° of (60 record) glue spread is that 100g/m2 reaches black and white lattice opacifying power, solidifies 20 △ E xanthochromia indexs be less than 1.0 at 800mj/cm2, illustrates that yellowing resistance is good.
Embodiment 5
UV solidifies white showering formulation for coating material and comprises shown in following mass percent (in table five):
Wherein oligopolymer is mainly the 6333-100 of polyester acrylate Changxing company, amino acrylates; ; Monomer is EO-TMPTA (ethoxylation Glycerin triacrylate) and PO-NPGDA (ethoxylated neopentylglycol diacrylate) and the HEMA (hydroxyethyl methylacrylate) of acrylate; Light trigger is that light trigger is TPO (2,4,6-trimethylbenzoyl-diphenyl phosphine oxide), 184 (1-hydroxy-cyclohexyl phenyl ketone); Auxiliary agent is containing dispersant B YK164 and defoamer BYK055 and anti-settling agent BYK410; Titanium dioxide be Du Pont's titanium dioxide r902+.
Table five UV solidifies the mass percent of white showering coating composition
By above-mentioned component, oligopolymer and a part of acrylate monomer mixed dissolution are stirred, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
This priming paint index of correlation: viscosity 300-450mpa.s/25 DEG C; Fineness≤25um; Curing speed is greater than 300mj/cm
2.; Showering 100g/m on sheet glass
2, 300mj/cm
2.after solidifying, gloss is that 95-100 ° of (60 record) glue spread is that 100g/m2 reaches black and white lattice opacifying power, solidifies 20 △ E xanthochromia indexs be less than 0.6 at 800mj/cm2, illustrates that yellowing resistance is good.
Claims (7)
1. UV solidifies a white showering coating, it is characterized in that, this white showering coating raw material by mass percentage, consists of: UV solidifies oligopolymer 30-50%; Acrylate monomer 20-40%; Light trigger 4-8%; Dumb light powder 0-10%; Auxiliary agent 1-2%; Titanium dioxide: 5-15%; It is the mixture of one or more oligopolymer in aliphatic urethane acrylate, Amino Polyester acrylate, polyester acrylate that UV solidifies oligopolymer; Described light trigger is 1-hydroxy-cyclohexyl phenyl ketone.
2. UV according to claim 1 solidifies white showering coating, it is characterized in that, what described UV solidified oligopolymer is that described aliphatic urethane acrylate, polyester acrylate is the oligopolymer of 2 functional groups, and Amino Polyester acrylate is 3 functional groups.
3. UV according to claim 1 solidifies white showering coating, it is characterized in that, described acrylate monomer is one or more in hydroxyethyl methylacrylate, pentaerythritol triacrylate, Glycerin triacrylate, ethoxylation Glycerin triacrylate, ethoxylated neopentylglycol diacrylate, 1,6 hexanediyl ester, tripropylene glycol diacrylate.
4. UV according to claim 1 solidifies white showering coating, it is characterized in that, described dumb light powder is the silicon-dioxide flatting silica of vapor phase process or gel method.
5. UV according to claim 1 solidifies white showering coating, it is characterized in that, described auxiliary agent is any one or several in defoamer, dispersion agent, anti-settling agent, flow agent.
6. UV according to claim 1 solidifies white showering coating, it is characterized in that, described titanium dioxide is rutile titanium dioxide.
7. the method that the arbitrary described UV of preparation claim 1～6 solidifies white showering coating, it is characterized in that, UV is solidified to oligopolymer and the stirring of a part of acrylate monomer mixed dissolution, add again auxiliary agent to stir again, then add dumb light powder and titanium dioxide high-speed stirring, reach and add residual acrylic acid ester monomer stirring at low speed to vacuumize 30 minutes at 45 DEG C after 10-20 minute after fineness of dispersion to filter and get final product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410334383.6A CN104073040A (en) | 2014-07-15 | 2014-07-15 | UV-cured white curtaining paint and preparation method thereof |
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| CN201410334383.6A CN104073040A (en) | 2014-07-15 | 2014-07-15 | UV-cured white curtaining paint and preparation method thereof |
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Cited By (8)
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| CN104559698A (en) * | 2014-12-11 | 2015-04-29 | 惠州市长润发涂料有限公司 | Yellowing-resistant UV (ultraviolet) transparent primer for electrostatic spraying |
| CN104559740A (en) * | 2014-12-10 | 2015-04-29 | 惠州市长润发涂料有限公司 | Ultraviolet-curing spray bright white finish |
| CN104927632A (en) * | 2015-07-01 | 2015-09-23 | 卓达新材料科技集团有限公司 | Xanthochromia-resistant UV paint for external wall sheet material and preparation method of xanthochromia-resistant UV paint |
| CN104927633A (en) * | 2015-07-01 | 2015-09-23 | 卓达新材料科技集团有限公司 | UV paint for building external wall panel and preparation method of UV paint |
| CN107418296A (en) * | 2017-05-09 | 2017-12-01 | 惠州市至上新材料有限公司 | A kind of radium-shine transfer gloss oil of ultraviolet light solidification no-plate seam holographic and preparation method thereof |
| CN108517178A (en) * | 2018-04-26 | 2018-09-11 | 青岛展辰新材料有限公司 | A kind of environment-friendly type UV hands wipe filled coloring coating and preparation method thereof |
| CN115353803A (en) * | 2020-10-30 | 2022-11-18 | 中山市鑫峰光固化材料有限公司 | Preparation method of non-thickening water-based UV (ultraviolet) curing coating |
| CN116515381A (en) * | 2023-03-30 | 2023-08-01 | 濮阳展辰新材料有限公司 | Smell-removing and yellow-resisting UV vacuum spraying white matte finish paint and preparation method and application thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559740A (en) * | 2014-12-10 | 2015-04-29 | 惠州市长润发涂料有限公司 | Ultraviolet-curing spray bright white finish |
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| CN104927632A (en) * | 2015-07-01 | 2015-09-23 | 卓达新材料科技集团有限公司 | Xanthochromia-resistant UV paint for external wall sheet material and preparation method of xanthochromia-resistant UV paint |
| CN104927633A (en) * | 2015-07-01 | 2015-09-23 | 卓达新材料科技集团有限公司 | UV paint for building external wall panel and preparation method of UV paint |
| CN107418296A (en) * | 2017-05-09 | 2017-12-01 | 惠州市至上新材料有限公司 | A kind of radium-shine transfer gloss oil of ultraviolet light solidification no-plate seam holographic and preparation method thereof |
| CN108517178A (en) * | 2018-04-26 | 2018-09-11 | 青岛展辰新材料有限公司 | A kind of environment-friendly type UV hands wipe filled coloring coating and preparation method thereof |
| CN108517178B (en) * | 2018-04-26 | 2020-05-12 | 青岛展辰新材料有限公司 | Environment-friendly UV (ultraviolet) hand-wiping filling coloring paint and preparation method thereof |
| CN115353803A (en) * | 2020-10-30 | 2022-11-18 | 中山市鑫峰光固化材料有限公司 | Preparation method of non-thickening water-based UV (ultraviolet) curing coating |
| CN116515381A (en) * | 2023-03-30 | 2023-08-01 | 濮阳展辰新材料有限公司 | Smell-removing and yellow-resisting UV vacuum spraying white matte finish paint and preparation method and application thereof |
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Application publication date: 20141001 |