CN108517178A - A kind of environment-friendly type UV hands wipe filled coloring coating and preparation method thereof - Google Patents
A kind of environment-friendly type UV hands wipe filled coloring coating and preparation method thereof Download PDFInfo
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- CN108517178A CN108517178A CN201810387790.1A CN201810387790A CN108517178A CN 108517178 A CN108517178 A CN 108517178A CN 201810387790 A CN201810387790 A CN 201810387790A CN 108517178 A CN108517178 A CN 108517178A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/06—Unsaturated polyesters having carbon-to-carbon unsaturation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/06—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation
- B05D3/061—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation using U.V.
- B05D3/065—After-treatment
- B05D3/067—Curing or cross-linking the coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
- B05D7/06—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
- B05D7/24—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials for applying particular liquids or other fluent materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2502/00—Acrylic polymers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2601/00—Inorganic fillers
- B05D2601/02—Inorganic fillers used for pigmentation effect, e.g. metallic effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D2602/00—Organic fillers
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Macromonomer-Based Addition Polymer (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of environment-friendly type UV hands wiping filled coloring coating, is grouped as by the group of following parts by weight：15 25 parts of functional monomer；13 30 parts of aliphatic polyurethane acrylic resin；25 32 parts of polyether-modified polyester acrylate resin；15 25 parts of color stuffing；0.5 5 parts of wetting dispersing agent；0.1 1 parts of antifoaming agent；48 parts of photoinitiator；Wherein, the functional monomer is polyethylene glycol 400 diacrylate, one kind in glycerine methoxyl group mono acrylic ester or mixture；The photoinitiator is 2 hydroxyl, 2 methyl, 1 phenyl, 1 acetone, 2,4,6 trimethyl benzoyl diphenyl base phosphine oxides of collocation or bis- (2,4,6 trimethylbenzoyl) phosphine oxides of phenyl.Using low viscous UV resins, it arranges in pairs or groups special UV monomers, addition has the filler of higher smooth degree and the photoinitiator of different wave length in right amount, to reach good construction effect and have no stimulation to human skin, adhesive force between base material and upper layer paint film is good, color wiping can enter next procedure after completing, and construction efficiency is obviously improved.
Description
Technical field
The invention belongs to the coating material solidified technical fields of UV, and in particular to a kind of environment-friendly type UV hands wipe filled coloring coating and its
Preparation method.
Background technology
Furniture industry to make the painting effect that color is penetrating, well arranged, three-dimensional sense is strong, by the full head degree by material
Color is realized, and used coating is exactly filled coloring coating, be commonly called as filling out agent.Filled coloring coating used in industry now
Based on solvent based product, solvent type product one side smell is big, and VOC content is high, has sizable danger to health
It does harm to and has serious pollution to air, another aspect construction efficiency is extremely low, and color wiping will be in 15-25 DEG C of environment after completing
Next procedure could be entered after placing 12 hours, winter need to place the longer time since temperature is low.Conventional solvent type hand
Wiping filled coloring coating, there is also the problems bad with the adhesive force of upper coating.
Invention content
Big, high VOC emission, stimulation skin, low construction efficiency, paint film for conventional solvent type filled coloring coating smell
The problem of poor adhesive force, the present invention is intended to provide a kind of environment-friendly type UV hands wipe filled coloring coating, using the UV trees of low viscosity
Fat, special UV monomers of arranging in pairs or groups, addition has the filler of higher smooth degree and the photoinitiator of different wave length in right amount, fine to reach
Construction effect and have no stimulation to human skin, accomplish real environmental protection, with the attachment between base material and upper layer paint film
Power is good, and color wiping can enter next procedure after completing, and construction efficiency is obviously improved.
The present invention is achieved by the following technical solutions：
A kind of environment-friendly type UV hands wiping filled coloring coating, is grouped as by the group of following parts by weight：
Wherein, the functional monomer is in polyethylene glycol 400 diacrylate, glycerine methoxyl group mono acrylic ester
A kind of or mixture；The photoinitiator is 2- hydroxy-2-methyl -1- phenyl -1- acetone collocation 2,4,6- trimethylbenzoyls
Base-diphenyl phosphine oxide or bis- (2,4,6- trimethylbenzoyls) phosphine oxides of phenyl.
Further, the mixture is pressed by polyethylene glycol 400 diacrylate and glycerine methoxyl group mono acrylic ester
According to 4：The mass ratio of (1-5) forms.
Further, the mixture is pressed by polyethylene glycol 400 diacrylate and glycerine methoxyl group mono acrylic ester
According to 3:2 mass ratio composition.
Polyethylene glycol 400 diacrylate belongs to Large molecule active monomer, and curing rate is fast, and flexibility is good, but viscosity
Bigger than normal, glycerine methoxyl group mono acrylic ester, viscosity is relatively low, and dilution capacity is good, but rate of drying is slower, according to the above ratio
Mixing, can not only ensure curing rate, but also can provide suitable viscosity, could not only reach the physical property of paint film in this way, but also
It can guarantee preferable construction wiping properties.
Further, the accounting of 2- hydroxy-2-methyls -1- phenyl -1- acetone is 85-93wt% in the photoinitiator.
Further, the photoinitiator is selected from 2- hydroxy-2-methyl -1- phenyl -1- acetone, 2,4,6- trimethylbenzene first
At least one of bis- (2,4,6- trimethylbenzoyls) phosphine oxides of acyl group-diphenyl phosphine oxide, phenyl.2- hydroxyl -2- first
Base -1- phenyl -1- acetone, such as double bond company 1173；2,4,6- trimethylbenzoy-dipheny phosphine oxides, such as Hubei Gu Run
The GR-TPO of company；Bis- (2,4, the 6- trimethylbenzoyl) phosphine oxides of phenyl, such as the 819 of Ciba.
Further, the color stuffing is talcum powder, wax powder and aerosil, talcum powder, wax powder and gas phase dioxy
The mass ratio of SiClx is 30:1:2.
Above-mentioned environment-friendly type UV hands wipe the preparation method of filled coloring coating, by functional monomer, aliphatic urethane propylene
Acid resin, polyether-modified polyester acrylate resin, photoinitiator 2,4,6- trimethylbenzoy-diphenies phosphine oxide, defoaming
Agent, wetting dispersing agent, talcum powder, wax powder, aerosil are mixed, and after fully dispersed, photoinitiator 2- hydroxyls are added
Base -2- methyl-1s-phenyl -1- acetone, stirring is to fully dispersed uniformly without lump.
Above-mentioned environment-friendly type UV hands wipe the coating process of filled coloring coating, and oiliness color essence is disperseed in the coating
It is even, it is uniformly coated on wood surface with hairbrush, then with rag wiped clean, coating weight is 20~40g/ ㎡, is then carried out ultraviolet
Photocuring；Semi-solid preparation UV energy：800~120mj/cm2。
Advantageous effect：Environment-friendly type UV hands provided by the invention wipe filled coloring coating, and (1) low smell does not stimulate skin, ring
It protects；(2) adhesive force between base material and upper layer paint film is good；(3) quick solidifying, color wiping can enter lower road after completing
Process, construction efficiency are obviously improved；(4) preparation method is simple.
Specific implementation mode
The present invention is described in further details with reference to specific embodiment.
The aliphatic urethane acrylate that following embodiment uses inspires confidence in the product that the trade mark is CF-3301 for Shenzhen section is vertical；
Polyether-modified polyester acrylate is the product that the female grand trade mark in Jiangxi is HM-326；Wetting dispersing agent is that the Bi Ke companies trade mark is
The product of BYK-2009；Antifoaming agent is the product that the Ying Chuan companies trade mark is TEGO920.Photoinitiator be selected from double bond company 1173,
The GR-TPO of Hubei Gu Run companies, the 819 of Ciba.The KB-13-1 of talcum powder K boards company
Embodiment 1
Functional monomer is 15 kilograms of polyethylene glycol 400 diacrylate (PEG400DA), aliphatic urethane acrylic acid tree
13 kilograms of fat, 30 kilograms of polyether-modified polyester acrylate resin, photoinitiator are trimethylbenzoy-dipheny phosphine oxide
0.5 kilogram, 0.1 kilogram of antifoaming agent (TEGO920), 0.5 kilogram of wetting dispersing agent, 15 kilograms of talcum powder, 1 kilogram of wax powder, gas
2 kilograms of aerosil is mixed, and after fully dispersed, photoinitiator 2- hydroxy-2-methyl -1- phenyl -1- acetone is added
(1173) 5 kilograms, stirring is to fully dispersed uniformly without lump.The experimental result of this example is：Product viscosity is fitted substantially
In, paint film hardness is moderate, and deep cure reaches effect, and wiping is good.
Embodiment 2
Take 25 kilograms of functional monomer glycerine methoxyl group mono acrylic ester (TPGMEMA), aliphatic urethane acrylic acid tree
28 kilograms of fat, 32 kilograms of polyether-modified polyester acrylate resin, bis- (2,4, the 6- trimethylbenzoyl) oxygen of photoinitiator phenyl
Change (819) 0.5 kilograms of phosphine, 0.1 kilogram of antifoaming agent, 1 kilogram of dispersant, 15 kilograms of talcum powder, 0.5 kilogram of wax powder, gas phase two
1 kilogram of silica is mixed, and after fully dispersed, photoinitiator phenyl bis- (2,4,6- trimethylbenzoyls) is added and aoxidizes
7 kilograms of phosphine, stirring are fully dispersed uniformly without lump.The experimental result of this example is：Product viscosity is substantially moderate, paint film
Hardness is moderate, and deep cure reaches effect, and wiping is good.
Embodiment 3
Take 15 kilograms of functional monomer polyethylene glycol 400 diacrylate (PEG400DA), glycerine methoxyl group list propylene
5 kilograms of acid esters (TPGMEMA), 20 kilograms of aliphatic urethane acrylate resin, 25 kilograms of polyether-modified polyester acrylate resin,
Bis- (819) 0.5 kilograms of (2,4, the 6- trimethylbenzoyl) phosphine oxides of phenyl, 0.1 kilogram of antifoaming agent, 1 kilogram of dispersant, KB-
121 15 kilograms of talcum powder, 0.5 kilogram of wax powder, 1 kilogram of mixing of aerosil after fully dispersed, are added light-initiated
(1173) 5 kilograms of agent 2- hydroxy-2-methyl -1- phenyl -1- acetone, stirring are fully dispersed uniformly without lump.This example
Experimental result is：Product viscosity is substantially moderate, and paint film hardness is moderate, and deep cure reaches effect, and wiping is good.
Embodiment 4
Take 15 kilograms of functional monomer polyethylene glycol 400 diacrylate (PEG400DA), glycerine methoxyl group list propylene
10 kilograms of acid esters (TPGMEMA), 15 kilograms of aliphatic urethane acrylate resin, polyether-modified polyester acrylate resin 25,000
Gram, bis- (819) 0.5 kilograms of (2,4, the 6- trimethylbenzoyl) phosphine oxides of phenyl, 0.1 kilogram of antifoaming agent, 1 kilogram of dispersant,
15 kilograms of talcum powder, 0.5 kilogram of wax powder, 1 kilogram of aerosil are mixed, and after fully dispersed, photoinitiator is added
(1173) 5 kilograms of 2- hydroxy-2-methyl -1- phenyl -1- acetone, stirring are fully dispersed uniformly without lump.The reality of this example
Testing result is：Product viscosity is substantially moderate, and paint film hardness is moderate, and deep cure reaches effect, and wiping is good.
Embodiment 5
Take 15 kilograms of functional monomer polyethylene glycol 400 diacrylate (PEG400DA), glycerine methoxyl group list propylene
10 kilograms of acid esters (TPGMEMA), 13 kilograms of aliphatic urethane acrylate resin (CF-3301), polyether-modified polyester acrylic
28 kilograms of resin (HM-326), bis- (819) 0.5 kilograms of (2,4, the 6- trimethylbenzoyl) phosphine oxides of photoinitiator phenyl, disappears
0.1 kilogram of infusion, 1 kilogram of dispersant, 15 kilograms of talcum powder, 1 kilogram of wax powder, 1 kilogram of aerosil are mixed, fill
After dispersion, (1173) 5 kilograms of photoinitiator 2- hydroxy-2-methyl -1- phenyl -1- acetone is added, is stirred fully dispersed equal
Even no lump.The experimental result of this example is：Product viscosity is moderate, and paint film hardness is moderate, and deep cure reaches effect
Fruit, wiping is preferable, and overall performance is best.
The present invention environment-friendly type UV hands wipe filled coloring coating, be the translucent g., jelly-like liquid of milky, viscosity be 110~
120k μ (30 DEG C) paint solid content 98.5wt%~99wt%, extremely low smell.Ultraviolet light or the sun should be avoided in storage
Light direct irradiation, its bin stability (50 DEG C/7d), as a result without exception after tested.
When application, appropriate oiliness color essence is added, then scattered this product, wood surface is uniformly coated on hairbrush, then
With rag wiped clean, coating weight is 20~40g/ ㎡, then carries out ultraviolet light solidification.Semi-solid preparation UV energy：
80~120MJ/cm2.After tested, adhesive force (draw compartment away from 2mm)≤1 grade.When room temperature be less than 10 DEG C when, using water-bath by its
It constructs again after being heated to 20~35 DEG C.After color has wiped, ultraviolet photo-curing is carried out, UV is then directly carried out and sprays bottom
The application of paint.
The environment-friendly type UV hands wiping filled coloring coating of the present invention good, extremely low smell, production efficiency height, nothing with painting effect
The characteristics of human skin stimulates.
Embodiment described above is only that the preferred embodiment of the present invention is described, not to the scope of the present invention
It is defined, under the premise of not departing from design spirit of the present invention, those of ordinary skill in the art are to technical scheme of the present invention
The various modifications made and improvement should all be fallen into the protection domain of claims of the present invention determination.
Claims (7)
1. a kind of environment-friendly type UV hands wipe filled coloring coating, which is characterized in that be grouped as by the group of following parts by weight：
Wherein, the functional monomer is one kind in polyethylene glycol 400 diacrylate, glycerine methoxyl group mono acrylic ester
Or mixture；The photoinitiator is 2- hydroxy-2-methyl -1- phenyl -1- acetone collocation 2,4,6- trimethylbenzoyls-two
Phenyl phosphine oxide or bis- (2,4,6- trimethylbenzoyls) phosphine oxides of phenyl.
2. coating according to claim 1, which is characterized in that the mixture by polyethylene glycol 400 diacrylate with
Glycerine methoxyl group mono acrylic ester is according to 4：The mass ratio of (1-5) forms.
3. coating according to claim 1, which is characterized in that the mixture by polyethylene glycol 400 diacrylate with
Glycerine methoxyl group mono acrylic ester is according to 3:2 mass ratio composition.
4. coating according to claim 1, which is characterized in that 2- hydroxy-2-methyls -1- phenyl-in the photoinitiator
The accounting of 1- acetone is 85-93wt%.
5. coating according to claim 1, which is characterized in that the color stuffing is talcum powder, wax powder and gas phase titanium dioxide
The mass ratio of silicon, talcum powder, wax powder and aerosil is 30:1:2.
6. claim 1-5 any one of them environment-friendly type UV hands wipe the preparation method of filled coloring coating, which is characterized in that will
Functional monomer, aliphatic urethane acrylate resin, polyether-modified polyester acrylate resin, photoinitiator 2,4,6- trimethylbenzenes
Formoxyl-diphenyl phosphine oxide, antifoaming agent, wetting dispersing agent, talcum powder, wax powder, aerosil are mixed, fully
After dispersion, photoinitiator 2- hydroxy-2-methyl -1- phenyl -1- acetone is added, stirring is to fully dispersed uniformly without lump.
7. claim 1-5 any one of them environment-friendly type UV hands wipe the coating process of filled coloring coating, which is characterized in that will
Oiliness color essence is uniformly dispersed in the coating, and wood surface is uniformly coated on hairbrush, then with rag wiped clean, coating weight
For 20~40g/ ㎡, ultraviolet light solidification is then carried out；Semi-solid preparation UV energy：80~120MJ/cm2。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810387790.1A CN108517178B (en) | 2018-04-26 | 2018-04-26 | Environment-friendly UV (ultraviolet) hand-wiping filling coloring paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810387790.1A CN108517178B (en) | 2018-04-26 | 2018-04-26 | Environment-friendly UV (ultraviolet) hand-wiping filling coloring paint and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN108517178A true CN108517178A (en) | 2018-09-11 |
| CN108517178B CN108517178B (en) | 2020-05-12 |
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| CN201810387790.1A Active CN108517178B (en) | 2018-04-26 | 2018-04-26 | Environment-friendly UV (ultraviolet) hand-wiping filling coloring paint and preparation method thereof |
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| CN110256905A (en) * | 2019-06-13 | 2019-09-20 | 东莞大宝化工制品有限公司 | A kind of filled-type UV colorant and preparation method thereof |
| CN116063918A (en) * | 2022-11-24 | 2023-05-05 | 长沙广欣新材料科技有限公司 | Excimer skin-feel UV coating and preparation method and application thereof |
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|---|---|---|---|---|
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| CN116063918A (en) * | 2022-11-24 | 2023-05-05 | 长沙广欣新材料科技有限公司 | Excimer skin-feel UV coating and preparation method and application thereof |
| CN116063918B (en) * | 2022-11-24 | 2024-01-30 | 长沙广欣新材料科技有限公司 | Excimer skin-feel UV coating and preparation method and application thereof |
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| Publication number | Publication date |
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| CN108517178B (en) | 2020-05-12 |
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