CN103922785B - A kind of high temperature insulation fire-retardant material - Google Patents
A kind of high temperature insulation fire-retardant material Download PDFInfo
- Publication number
- CN103922785B CN103922785B CN201310015985.0A CN201310015985A CN103922785B CN 103922785 B CN103922785 B CN 103922785B CN 201310015985 A CN201310015985 A CN 201310015985A CN 103922785 B CN103922785 B CN 103922785B
- Authority
- CN
- China
- Prior art keywords
- black mud
- fire
- retardant material
- parts
- high temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
A kind of high temperature insulation fire-retardant material, it is characterized in that: the following starting material comprising parts by weight: black mud powder or black mud particle 20-25 part, hollow glass microbead 7-10 part, industrial hex-ammoniate 7-10 part, sepiolite 7-10 part, high-alumina cement 7-10 part, carbon fiber 1-4 part, fibrous magnesium silicate element 3-5 part, whipping agent 1-3 part, AES promoting agent 1-3 part.This kind material fire insulation performance is good, cost is low, density is little, can be used for preparing fireproof brickwork etc.
Description
Technical field
The present invention relates to the manufacture method of a kind of high temperature insulation fire-retardant material and this fire-retardant material, this material can be used for preparing fireproof brickwork.
Background technology
Fire-retardant material just refers to the construction or art work with the above fire resistance of certain grade, can be divided into following three kinds according to Building technology rule: (one) non-fire material: as concrete, brick or hollow brick, watt, building stones, iron and steel, aluminium, glass, glass fibre, mineral wool, pottery, mortar, lime and other is not because intimately causing burning, fusing, failure by rupture and producing the material of obnoxious flavour; (2) refractory slab: as materials such as wood cement board, the plates of resistance to calcined plaster; (3) flame resistant material: as materials such as the plywood of resistance to combustion, the fiberboard of resistance to combustion, the plastic plate of resistance to combustion, plasterboards.
The energy and material are the bases of Chinese national economy, are also the bottlenecks of Chinese national economy development simultaneously, the energy-conservation fundamental state policy having become China.30% of the about total national total energy consumption of building energy consumption of China, in today of Building Trade in China develop rapidly, if do not note the use of energy-conserving product, the increase along with buildings increases by building energy consumption ratio.Lightweight, insulation, heat insulation material of construction is used to be one of effective measure reducing energy consumption.Firmly build portion and the Ministry of Public Security must install and use heat insulating fire prevention in No. 46 and the Fire-Fighting Bureau under the Ministry of Public Security 65 all skins of literary composition regulation in 2011 in 2009 and reach the finishing material that A level requires.Existing market only adopts the finishing material of national standard B level, so the heat insulating fire-retardant material of research and development national standard A level level is extremely urgent.
Meanwhile, the major issue that refractory materials cost Ye Shi enterprise considers is reduced.Use stalk material to prepare fireproof brickwork etc. although have on the market, cost is lower, and their heat-proof quality is poor, and fire resistance period is short, can not meet the requirement of national standard and " Code for fire protection design of buildings ".
Summary of the invention
Object of the present invention is just to provide the fire-retardant material that a kind of heat-proof quality is good, cost is low, density is low, intensity is high, and the manufacture method of this material; It can be used for making fireproof brickwork.
For achieving the above object, technical scheme of the present invention is:
A kind of high temperature insulation fire-retardant material, it is characterized in that: the following starting material comprising parts by weight: black mud powder or black mud particle 20-25 part, hollow glass microbead 7-10 part, industrial hex-ammoniate 7-10 part, sepiolite 7-10 part, high-alumina cement 7-10 part, carbon fiber 1-4 part, fibrous magnesium silicate element 3-5 part, whipping agent 1-3 part, AES promoting agent 1-3 part.
Also comprise water in above-mentioned fire-retardant material, the amount of described water meets that the mixture of each raw material can be made to be formed is thick.
Described black mud powder or black mud particle are made up of the mud bottom fish pond or reservoir, and the granularity of described black mud powder is 20-200 order, and the mean diameter of described black mud particle is 1mm-5mm, and its main component is Al
2o
3, SiO
2and Fe
2o
3.
A kind of method preparing above-mentioned fire-retardant material, completed by following steps: (A), in stirrer, add black mud powder according to any one of claim 1-5 or black mud particle, hollow glass microbead, industrial hex-ammoniate, sepiolite stir, add high-alumina cement and carbon fiber again, fibrous magnesium silicate element, AES promoting agent be uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Adopt technique scheme, wherein muck soil and slag etc. are waste material, the rubbish in people's eye, peter out, current era that energy day is becoming tight in resource, and our country advocates especially and builds a conservation-minded society.They use by the present invention, and on the one hand production cost is low, and change waste material, rubbish are again recycled into secondary resource on the other hand, this meets national environmental protection policy.Muck soil is also well natural bonding agent simultaneously.
Produce the rapid foaming and intumescing of chemical reaction after the mixing such as hollow glass microbead, possess heat insulating fire protection flame retarding function.First external wall thermal insulation material will have good flame retardant resistance, and we are with naked light directly to testpieces burning, and after 20 minutes, testpieces still stands intact, and has not both melted also non-deliquescing, only occurs carbonization point.
And add whipping agent and extrudate density can be reduced to below 0.35g/cm3, goods are made to reach 180kg/cm3-260kg/cm3, thus making goods reduce thermal conductivity, its thermal conductivity reaches 0.048w/m.k-0.08w/m.k. and has higher intensity to meet shaping and construction needs.
Blending carbon fiber improves anti-folding and the ultimate compression strength of goods, prevents shrinkage crack, improves intensity.And add the intensity that carbon fiber can reduce material weight, strongthener.
Fibrous magnesium silicate element does not produce chemical reaction with other materials, is serviceability and the mechanical property of being improved goods by physical action completely, plays fine effect to the stability of goods.
Promoting agent adopts AES promoting agent, can remove smell, increases flow effect.
Through inspection, fire-retardant material of the present invention all can be up to state standards the standard of heat insulating fire-retardant material of A level level.
Embodiment
Black mud powder of the present invention is made up of pond muck soil or reservoir muck soil.Muck soil, through screening, filters, and dries, screening, the techniques such as grinding, deep processing elaborate powder or particle, and wherein the granularity of black mud powder is 20 order to 200 orders, and the mean diameter of black mud particle is 1-5mm, and muck soil chemistry major ingredient is: Al
2o
3>=34%, SiO
2≤ 50.5%, Fe
2o
3≤ 1.35%.
The particle diameter of hollow glass microbead is micron order.
Embodiment 1
20 parts, black mud powder, hollow glass microbead 10 parts, industrial hex-ammoniate 7 parts, sepiolite 10 parts is added in stirrer, stir, add high-alumina cement 10 parts, 1 part, carbon fiber, fibrous magnesium silicate element 5 parts again, AES promoting agent 1 part is uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent 3 parts to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Embodiment 2
In stirrer, add black mud particle 25 parts, hollow glass microbead 7 parts, industrial hex-ammoniate 10 parts, sepiolite 7 parts, stir, add high-alumina cement 7 parts, 4 parts, carbon fiber, fibrous magnesium silicate element 3 parts again, AES promoting agent 3 parts is uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent 1 part to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Embodiment 3
In stirrer, add black mud particle 20 parts, hollow glass microbead 8 parts, industrial hex-ammoniate 10 parts, sepiolite 7 parts, stir, add high-alumina cement 10 parts, 1 part, carbon fiber, fibrous magnesium silicate element 5 parts again, AES promoting agent 1 part is uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent 3 parts to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Embodiment 4
In stirrer, add 25 parts, black mud powder, hollow glass microbead 7 parts, industrial hex-ammoniate 7 parts, sepiolite 10 parts, stir, add high-alumina cement 7 parts, 4 parts, carbon fiber, fibrous magnesium silicate element 3 parts again, AES promoting agent 3 parts is uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent 1 part to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Embodiment 5
In stirrer, add black mud particle 20 parts, hollow glass microbead 8 parts, industrial hex-ammoniate 9 parts, sepiolite 7 parts, stir, add high-alumina cement 7 parts, 1 part, carbon fiber, fibrous magnesium silicate element 5 parts again, AES promoting agent 1 part is uniformly mixed, then it is thick for adding water and being stirred to mixture, and (B) utilizes foaming machine the aqueous solution of whipping agent 3 parts to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
Claims (2)
1. a high temperature insulation fire-retardant material, is characterized in that: the following starting material comprising parts by weight: black mud powder or black mud particle 20-25 part, hollow glass microbead 7-10 part, industrial hex-ammoniate 7-10 part, sepiolite 7-10 part, high-alumina cement 7-10 part, carbon fiber 1-4 part, fibrous magnesium silicate element 3-5 part, whipping agent 1-3 part and AES promoting agent 1-3 part; Wherein, described high temperature insulation fire-retardant material also comprises water, and the amount of described water meets that the mixture of each raw material can be made to be formed is thick; Described black mud powder or black mud particle are made up of the mud bottom fish pond or reservoir, and the granularity of described black mud powder is 20-200 order, and the mean diameter of described black mud particle is 1mm-5mm, and the main component of described black mud powder or black mud particle is Al
2o
3, SiO
2and Fe
2o
3wherein, described high temperature insulation fire-retardant material is completed by following steps: (A), in stirrer, add described black mud powder or black mud particle, hollow glass microbead, industrial hex-ammoniate, sepiolite stir, add high-alumina cement and carbon fiber again, fibrous magnesium silicate element, AES promoting agent be uniformly mixed, then it is thick for adding water and being stirred to mixture
(B) foaming machine is utilized the aqueous solution of whipping agent to be made foam slurry; Then this foam slurry is added in the mixture of step (A), be uniformly mixed and obtain fire-retardant material.
2. a purposes for fire-retardant material described in claim 1, is characterized in that: for the preparation of fireproof brickwork.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310015985.0A CN103922785B (en) | 2013-01-15 | 2013-01-15 | A kind of high temperature insulation fire-retardant material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310015985.0A CN103922785B (en) | 2013-01-15 | 2013-01-15 | A kind of high temperature insulation fire-retardant material |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103922785A CN103922785A (en) | 2014-07-16 |
| CN103922785B true CN103922785B (en) | 2016-03-02 |
Family
ID=51141214
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310015985.0A Active CN103922785B (en) | 2013-01-15 | 2013-01-15 | A kind of high temperature insulation fire-retardant material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103922785B (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106099663B (en) * | 2016-06-03 | 2018-05-04 | 宋海涛 | A kind of intelligent electric power switchgear |
| CN106699075A (en) * | 2016-11-28 | 2017-05-24 | 江苏东钢新材料有限公司 | Low-cost fireproof material |
| CN106630918A (en) * | 2016-12-15 | 2017-05-10 | 南京市消防工程有限公司宜兴安装分公司 | Incombustible fireproof material |
| CN107417167A (en) * | 2017-06-20 | 2017-12-01 | 合肥博之泰电子科技有限公司 | A kind of Novel fireproof material and preparation method thereof |
| CN107200499A (en) * | 2017-07-17 | 2017-09-26 | 苏州伟安杰工程技术有限公司 | The engineering material of multifunctional fire-proof environmental protection |
| CN107521431A (en) * | 2017-08-16 | 2017-12-29 | 合肥东凯智控科技有限公司 | A kind of new-energy automobile feature heat-insulating fire-proofing material |
| CN109422511A (en) * | 2017-08-31 | 2019-03-05 | 天源华威集团有限公司 | A kind of high temperature resistant heat insulation fire proofing material |
| CN108162118B (en) * | 2017-12-07 | 2020-05-19 | 淮安子婷门窗有限公司 | Preparation method of fireproof door core board |
| CN108373310A (en) * | 2018-03-01 | 2018-08-07 | 合肥达户电线电缆科技有限公司 | A kind of fiber composite enhancing thermal insulation board and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
-
2013
- 2013-01-15 CN CN201310015985.0A patent/CN103922785B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103922785A (en) | 2014-07-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103922785B (en) | A kind of high temperature insulation fire-retardant material | |
| CN103992091B (en) | A kind of light-high-strength aerated bricks and preparation method thereof | |
| CN104876471A (en) | Inorganic composite insulation board | |
| CN101514089B (en) | Self-insulation external wallboard for buildings | |
| CN101767976B (en) | Fireproof door core material and application thereof in preparation of fireproof door | |
| CN102838375A (en) | Inorganic foam heat insulating material and preparation method thereof | |
| CN107032708A (en) | A kind of autoclaved aerated concrete slab and its manufacture method | |
| CN103992086A (en) | Fire and water resistant aerated brick and making method thereo f | |
| CN104446227A (en) | Concrete with high fire resistance | |
| CN104761189A (en) | High-performance thermal-insulation fire-proof sound-insulation material | |
| CN101585687A (en) | Insulation and fire-proof material and production method thereof | |
| CN105399380A (en) | Single-component efficient light external wall thermal insulation material and preparation method thereof | |
| KR20080103135A (en) | The dry mortar with soundproof and keeping warm and the noninflammable board therewith and light brick therewith | |
| CN104193387B (en) | A kind of suction ripple aerated bricks and preparation method thereof | |
| CN103992085B (en) | A kind of fireproof antibacterial mildew-resistant aerated bricks and preparation method thereof | |
| CN103880376B (en) | A kind of lightweight inorganic fireproof heat preservation plate material | |
| CN103992066A (en) | Stripping resistant aerated brick and making method thereof | |
| CN107140896A (en) | A kind of concrete and preparation method thereof | |
| CN107417167A (en) | A kind of Novel fireproof material and preparation method thereof | |
| CN103408322A (en) | Mine tailing-doped high-performance concrete and preparation method thereof | |
| CN102584121B (en) | Inorganic nonmetallic light fireproof thermal insulation board | |
| CN103922676A (en) | Novel thermal-insulation fireproof material | |
| CN108585615A (en) | A kind of resistance to compression light fire-proof plank and preparation method thereof | |
| CN101831980A (en) | Manganese slag lightweight aggregate wall block | |
| CN108558208A (en) | A kind of environment protection architecture ceramic glaze and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent for invention or patent application | ||
| CB02 | Change of applicant information |
Address after: 201302 Pudong New Area old port industrial zone, Le Le Road, No. 388, Shanghai Applicant after: Shanghai Waysmos Fine Chemical Co., Ltd. Address before: 201322 No. 388 happy road, old town, Shanghai, Pudong New Area Applicant before: Shanghai Waysmos Fine Chemical Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |