CN103739732A - Method for extracting hollyhock seed polysaccharide - Google Patents
Method for extracting hollyhock seed polysaccharide Download PDFInfo
- Publication number
- CN103739732A CN103739732A CN201310735013.9A CN201310735013A CN103739732A CN 103739732 A CN103739732 A CN 103739732A CN 201310735013 A CN201310735013 A CN 201310735013A CN 103739732 A CN103739732 A CN 103739732A
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- China
- Prior art keywords
- polysaccharide
- althaeae roseae
- semen althaeae
- semen
- extracting
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- 239000005017 polysaccharide Substances 0.000 title claims abstract description 46
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 46
- 150000004676 glycans Chemical class 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 24
- 235000017334 Alcea rosea Nutrition 0.000 title abstract description 9
- 235000017303 Althaea rosea Nutrition 0.000 title abstract description 9
- 240000000530 Alcea rosea Species 0.000 title description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 58
- 238000001556 precipitation Methods 0.000 claims abstract description 22
- 238000005238 degreasing Methods 0.000 claims abstract description 20
- 238000000605 extraction Methods 0.000 claims abstract description 15
- 210000000582 semen Anatomy 0.000 claims description 47
- 239000006286 aqueous extract Substances 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 18
- 238000010992 reflux Methods 0.000 claims description 16
- 238000003809 water extraction Methods 0.000 claims description 11
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 10
- 229960001701 chloroform Drugs 0.000 claims description 10
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 9
- 238000002386 leaching Methods 0.000 claims description 8
- 239000011259 mixed solution Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 12
- 102000004169 proteins and genes Human genes 0.000 abstract description 2
- 108090000623 proteins and genes Proteins 0.000 abstract description 2
- 241000921356 Alcea Species 0.000 abstract 4
- 239000000243 solution Substances 0.000 description 20
- 239000000843 powder Substances 0.000 description 11
- 239000003153 chemical reaction reagent Substances 0.000 description 10
- 238000001914 filtration Methods 0.000 description 10
- 239000006228 supernatant Substances 0.000 description 10
- 239000000284 extract Substances 0.000 description 8
- 239000002904 solvent Substances 0.000 description 6
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 description 5
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 235000000346 sugar Nutrition 0.000 description 4
- MYKOKMFESWKQRX-UHFFFAOYSA-N 10h-anthracen-9-one;sulfuric acid Chemical compound OS(O)(=O)=O.C1=CC=C2C(=O)C3=CC=CC=C3CC2=C1 MYKOKMFESWKQRX-UHFFFAOYSA-N 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- 239000012488 sample solution Substances 0.000 description 3
- 244000208874 Althaea officinalis Species 0.000 description 2
- 235000006576 Althaea officinalis Nutrition 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 208000025865 Ulcer Diseases 0.000 description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 231100000397 ulcer Toxicity 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- 235000007926 Craterellus fallax Nutrition 0.000 description 1
- 240000007175 Datura inoxia Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000219071 Malvaceae Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 102000035195 Peptidases Human genes 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 208000006568 Urinary Bladder Calculi Diseases 0.000 description 1
- 208000009911 Urinary Calculi Diseases 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- LPQOADBMXVRBNX-UHFFFAOYSA-N ac1ldcw0 Chemical compound Cl.C1CN(C)CCN1C1=C(F)C=C2C(=O)C(C(O)=O)=CN3CCSC1=C32 LPQOADBMXVRBNX-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000000202 analgesic effect Effects 0.000 description 1
- 210000004102 animal cell Anatomy 0.000 description 1
- 230000000954 anitussive effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 229940124584 antitussives Drugs 0.000 description 1
- 210000000941 bile Anatomy 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 201000001421 hyperglycemia Diseases 0.000 description 1
- 208000033065 inborn errors of immunity Diseases 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- -1 polysaccharide compound Chemical class 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 208000028529 primary immunodeficiency disease Diseases 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310735013.9A CN103739732B (en) | 2013-12-27 | 2013-12-27 | A kind of method of extracting seed of hollyhock polysaccharide |
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CN201310735013.9A CN103739732B (en) | 2013-12-27 | 2013-12-27 | A kind of method of extracting seed of hollyhock polysaccharide |
Publications (2)
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CN103739732A true CN103739732A (en) | 2014-04-23 |
CN103739732B CN103739732B (en) | 2016-05-04 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103976466A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Abelmoschus manilhot seed extractive and application in cigarette |
CN104087422A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of hollyhock root/stem water extract |
CN104082846A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Application of althaea rosa seed extractive to cigarettes |
CN105859907A (en) * | 2016-06-12 | 2016-08-17 | 南京中医药大学 | Abelmoschus manihot stem leaf polysaccharide sulfating modified product having immune activity improving function and preparation method thereof |
CN105859906A (en) * | 2016-06-12 | 2016-08-17 | 南京中医药大学 | Abelmoschus manihot stem and leaf polysaccharide acetylation modification product with immunocompetence improving function and preparation method thereof |
CN105968221A (en) * | 2016-06-28 | 2016-09-28 | 南京中医药大学 | Immunological competence improving acid degradation product of polysaccharides of stems and leaves of abelmoschus esculentus and method for preparing immunological competence improving acid degradation product |
CN106008729A (en) * | 2016-04-14 | 2016-10-12 | 南京中医药大学 | Abelmoschus manihot stem and leaf polysaccharide and preparation method and application thereof |
CN106046187A (en) * | 2016-06-28 | 2016-10-26 | 南京中医药大学 | Free radical degradation product of abelmoschus manilhot stem leaf polysaccharide capable of improving immunocompetence and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102964466A (en) * | 2012-12-18 | 2013-03-13 | 江苏省中医院 | Abelmoschus manihot polysaccharide with anti-tumor activity and preparation method thereof |
CN103087213A (en) * | 2013-02-01 | 2013-05-08 | 李育材 | Preparation method of polysaccharide of tree peony seeds |
CN103435711A (en) * | 2013-07-17 | 2013-12-11 | 新乡医学院 | Extraction method of ipomoea nil polysaccharide |
-
2013
- 2013-12-27 CN CN201310735013.9A patent/CN103739732B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102964466A (en) * | 2012-12-18 | 2013-03-13 | 江苏省中医院 | Abelmoschus manihot polysaccharide with anti-tumor activity and preparation method thereof |
CN103087213A (en) * | 2013-02-01 | 2013-05-08 | 李育材 | Preparation method of polysaccharide of tree peony seeds |
CN103435711A (en) * | 2013-07-17 | 2013-12-11 | 新乡医学院 | Extraction method of ipomoea nil polysaccharide |
Non-Patent Citations (3)
Title |
---|
徐怀德: "《天然产物提取工艺学》", 30 June 2008, 北京:中国轻工业出版社 * |
赵焕焕 等: "黄秋葵粗多糖体外抗氧化活性测定", 《郑州大学学报(医学版)》 * |
高素莲 等: "黄蜀葵多糖的分析", 《分析测试学报》 * |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103976466A (en) * | 2014-05-20 | 2014-08-13 | 河南中烟工业有限责任公司 | Abelmoschus manilhot seed extractive and application in cigarette |
CN104087422A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of hollyhock root/stem water extract |
CN104082846A (en) * | 2014-07-24 | 2014-10-08 | 中国烟草总公司郑州烟草研究院 | Application of althaea rosa seed extractive to cigarettes |
CN104082846B (en) * | 2014-07-24 | 2016-02-24 | 中国烟草总公司郑州烟草研究院 | The application of a kind of hollyhock seed extract in cigarette |
CN104087422B (en) * | 2014-07-24 | 2016-03-16 | 中国烟草总公司郑州烟草研究院 | A kind of preparation method of hollyhock rhizome Aqueous extracts and application thereof |
CN106008729A (en) * | 2016-04-14 | 2016-10-12 | 南京中医药大学 | Abelmoschus manihot stem and leaf polysaccharide and preparation method and application thereof |
CN106008729B (en) * | 2016-04-14 | 2018-05-25 | 南京中医药大学 | A kind of sunset abelmoschus stem or bark leaf polyose and preparation method and application |
CN105859906A (en) * | 2016-06-12 | 2016-08-17 | 南京中医药大学 | Abelmoschus manihot stem and leaf polysaccharide acetylation modification product with immunocompetence improving function and preparation method thereof |
CN105859907A (en) * | 2016-06-12 | 2016-08-17 | 南京中医药大学 | Abelmoschus manihot stem leaf polysaccharide sulfating modified product having immune activity improving function and preparation method thereof |
CN105859907B (en) * | 2016-06-12 | 2018-06-19 | 南京中医药大学 | With immunocompetent sunset abelmoschus stem or bark leaf polyose sulphation modification product of raising and preparation method thereof |
CN105968221A (en) * | 2016-06-28 | 2016-09-28 | 南京中医药大学 | Immunological competence improving acid degradation product of polysaccharides of stems and leaves of abelmoschus esculentus and method for preparing immunological competence improving acid degradation product |
CN106046187A (en) * | 2016-06-28 | 2016-10-26 | 南京中医药大学 | Free radical degradation product of abelmoschus manilhot stem leaf polysaccharide capable of improving immunocompetence and preparation method thereof |
CN106046187B (en) * | 2016-06-28 | 2018-06-19 | 南京中医药大学 | With free radical cracking product for improving immunocompetent sunset abelmoschus stem or bark leaf polyose and preparation method thereof |
CN105968221B (en) * | 2016-06-28 | 2018-08-14 | 南京中医药大学 | With the acid system catabolite and preparation method thereof for improving immunocompetent sunset abelmoschus stem or bark leaf polyose |
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CN103739732B (en) | 2016-05-04 |
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Address after: 830000 No. 625 Yingbin Road, the Xinjiang Uygur Autonomous Region, Urumqi Applicant after: XINJIANG QIKANG HABO UIGHUR MEDICINE CO.,LTD. Address before: 830000 No. 625 Yingbin Road, the Xinjiang Uygur Autonomous Region, Urumqi Applicant before: QIKANGHABO UGGR MEDICINE Co.,Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: QIKANGHABO UYGUR MEDICINE CO., LTD., XINJIANG TO: XINJIANG QIKANG HABO UIGUR MEDICINE CO., LTD. |
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Address after: 830000 the Xinjiang Uygur Autonomous Region Urumqi hi tech Industrial Development Zone (new urban area) 1375 Patentee after: New Qikang Pharmaceutical Co.,Ltd. Address before: 830000 Yingbin Road, Urumqi, the Xinjiang Uygur Autonomous Region 625 Patentee before: XINJIANG QIKANG HABO UIGHUR MEDICINE CO.,LTD. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Method for Extracting Polysaccharides from Shukui Seeds Effective date of registration: 20230324 Granted publication date: 20160504 Pledgee: China Construction Bank Corporation Urumqi Youhao North Road Branch Pledgor: New Qikang Pharmaceutical Co.,Ltd. Registration number: Y2023980036259 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |